Simple preparations of Pd6Cl12, Pt6Cl 12, and Qn[Pt2Cl8+n], n = 1, 2 (Q = TBA+, PPN+) and structural characterization of [TBA][Pt2Cl9] and [PPN]2[Pt2Cl 10]·C7H8

Inorganic Chemistry

Volumn 47, Issue 3, 2008, Pages 1237-1242

  Dell'Amico, Daniela Belli ^a   Calderazzo, Fausto ^a   Marchetti, Fabio ^a   Ramello, Stefano ^a,b   Samaritani, Simona ^a  

^a UNIVERSITY OF PISA   (Italy)

^b ENI S P A   (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 39749188796     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic701932u     Document Type: Article

References (54)

1. Bagnoli, F.; Belli Dell'Amico, D; Calderazzo, F; Englert, U.; Marchetti, F.; Merigo, A.; Ramello, S J. Organomet. Chem. 2001, 622, 180.
2. (a) Brodersen, K.; Thiele, G.; Schnering, H. G. Z. Anorg. Allg. Chem. 1965, 337, 120.
3. (b) Pilbrow, M. F. J. Chem. Soc., Dalton Trans. 1975, 2432.
4. (c) Schnering, H.G.; Chang, J.-H.; Peters, K.; Peters, E.-M.; Wagner, F. R.; Grin, Y.; Thiele, G. Z. Anorg. Allg. Chem. 2003, 629, 516.
5. (a) Schäfer, H.; Wiese, U.; Rinke, K.; Brendel, K. Angew. Chem. 1967, 79, 244;
6. Angew. Chem., Int. Ed Engl. 1967, 6, 253.
7. (b) Yatsimirski, A.; Ugo, R. Inorg. Chem. 1983, 2, 1395.
8. (c) Belli Dell'Amico, D.; Calderazzo, F.; Marchetti, F.; Ramello, S. Angew. Chem., Int. Ed. Engl. 1996, 35, 1331.
9. Wells, A. F. Z. Kristallogr. 1938, 100, 189.
10. Wiese, U.; Schäfer, H.; Schnering, H. G.; Brendel, C.; Rinke, K. Angew. Chem. 1970, 82, 135;
11. Angew. Chem., Int. Ed. Engl. 1970, 9, 158.
12. (a) Olmstead, M. M.; Ginwalla, A. S.; Noll, B. C.; Tinti, D. S.; Balch, A. L. J. Am. Chem. Soc. 1996, 118, 7737.
13. (b) Olmstead, M. M; Wei, P.; Balch, A. L. Chem. Eur. J. 1999, 5, 3136.
14. (c) Olmstead, M. M.; Wei, P.; Ginwalla, A. S.; Balch, A. L. Inorg. Chem. 2000, 39, 4555.
15. Kukushkin, V. Yu.; Tkachuk, V. M.;Vorobiov-Desiatovsky, N. V. Inorg. Syn. 1998, 32, 145, and references therein.
16. Dillamore, I. M.; Edwards, D. A. J. Inorg. Nucl. Chem. 1969, 31, 2427.
17. Pilbrow, M. F. J. Chem. Soc., Chem. Commun. 1972, 270.
18. Schnering, H. G.; Chang, J.-H.; Freiberg, M.; Peters, K.; Peters, E.-M.; Ormeci, A.; Schröder, L.; Thiele, G.; Röhr, C. Z. Anorg. Allg. Chem. 2004, 630, 109.
19. Belli Dell'Amico, D.; Calderazzo, F.; Dell'Amico, G. Gazz. Chim. Ital. 1977, 107, 101.
20. Sheldrick, G. M. SHELXTL-Plus, Rel. 5.1; Bruker AXS Inc.: Madison, WI, 1997.
21. Sheldrick, G. M. SHELX97, Programs for Crystal Structure Analysis (Release 97-2); University of Göttingen: Göttingen, Germany, 1998.
22. Altomare, A.; Cascarano, G.; Giacovazzo, C.; Guagliardi, A. J. Appl. Crystallogr. 1993, 26, 343.
23. Farrugia, L. J. J. Appl. Crystallogr. 1999, 32, 837.
24. Summerville, R. H.; Hoffmann, R. J. Am. Chem. Soc. 1979, 101, 3821.
25. Several data are reported in the literature; here only three papers are reported dealing with chromium, molybdenum, and tungsten derivatives, in that order. (a) Dyer, P. W.; Gibson, V. C.; Jeffery, J. C. Polyhedron 1995, 14, 3095.
26. (b) Stranger, R.; Smith, P. W.; Grey, I. E. Inorg. Chem. 1989, 28, 1271.
27. (c) Dunbar, K. R.; Pence, L. E. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1991, 47, 23.
28. Selected papers on titanium, zirconium, and hafnium compounds are, respectively. (a) Solari, E.; Floriani, C.; Schenk, K.; Chiesi-Villa, A.; Rizzoli, C.; Rosi, M.; Sgamellotti, A. Inorg. Chem. 1994, 33, 2018.
29. (b) Schormann, M.; Garratt, S.; Hughes, D. L.; Green, J. C.; Bochmann, M. J. Am. Chem. Soc. 2002, 124, 11266.
30. (c) Calderazzo, F.; Ferri, I.; Pampaloni, G.; Troyanov, S. J. Organomet. Chem. 1996, 518, 189.
31. Bino, A.; Cotton, F. A. J. Am. Chem. Soc. 1980, 102, 608.
32. Efimenko, I. A.; Balakaeva, T. A.; Kurbakova, A. P.; Kanishcheva, A. S.; Chuvaev, A. V.; Stepanovich, V. M.; Mikhailov, Yu. N. Zh. Neorg. Khim. 1992, 37, 1312.
33. Cotton, F. A.; Ucko, D. A. Inorg. Chim. Acta 1972, 6, 161.
34. Yellowlees, L.; Elliot, M.; Parsons, S.; Messenger, D. Cambridge Crystallographic Data Centre, Private Communication, CCDC 278284.
35. (a) Vicente, J.; Arcas, A.; Fernández-Hernández, J. M.; Sironi, A., Masciocchi, N. Chem. Commun., 2005, 1267.
36. (b) Vicente, J.; Arcas, A.; Fernández-Hernández, J. M.; Bautista, D. Organometallics, 2006, 25, 4404.
37. Hollmann, P.; Preetz, W.; Hillebrecht, H.; Thiele, G. Z. Anorg. Allg. Chem. 1992, 611, 28.
38. Cavigliasso, G.; Lovell, T.; Stranger, R. Dalton Trans. 2006, 2017, and references therein.
39. Aurivillius, B.; Stålhandske, C. Acta Chem. Scand. A 1978, 32, 715.
40. Cook, P. M.; Dahl, L. F.; Dickerhoof, D. W J. Am. Chem. Soc. 1972, 94, 5511.
41. Köhn, R. D.; Kampe, P.; Kociok-Köhn, G. Eur. J. Inorg. Chem. 2005, 3217.
42. (a) Eicher, J.; Müller, U.; Dehnicke, K. Z. Anorg. Allg. Chem. 1985, 521, 37.
43. (b) Brusilovets, A. I.; Rusanov, E. B.; Chernega, A. N. Zh. Obshch. Khim. 1995, 65, 1819.
44. (c) Krut'ko, D. P.; Borzov, M. V.; Veksler, E. N.; Churakov, A. V.; Howard, J. A. K. Polyhedron 1998, 17, 3889.
45. (d) Coles, S. J.; Hursthouse, M. B.; Kelly, D. G.; Walker, N. M. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 1999, 55, 1789.
46. (e) Sarsfield, M. J.; Said, M.; Thornton-Pett, M.; Gerrard, L. A.; Bochmann, M. J. Chem. Soc., Dalton Trans. 2001, 822.
47. (f) Hart, R.; Levason, W.; Patel, B.; Reid, G. J. Chem. Soc., Dalton Trans. 2002, 3153.
48. (g) Centore, R.; Tuzi, A.; Liguori, D. Acta Crystallogr., Sect. C: Cryst. Struct. Commun. 2003, 59, m241.
49. (a) Calderazzo, F.; Pallavicini, P.; Pampaloni, G.; Zanazzi, P. F. J. Chem. Soc., Dalton Trans. 1990, 2743.
50. (b) Neumüller, B.; Dehnicke, K. Z. Anorg. Allg. Chem. 2004, 630, 2576.
51. Hey, E.; Weller, F.; Dehnicke, K. Z. Anorg. Allg. Chem. 1984, 508, 86.
52. Kolesnichenko, V.; Swenson, D. C.; Messerle, L. Chem. Commun. 1998, 2137.
53. Krebs, B.; Henkel, G.; Dartmann, M.; Preetz, W.; Bruns, M. Z. Naturforsch., B :Chem. Sci. 1984, 39, 843.
54. McGrady, J. E.; Stranger, R.; Lovell, T. Inorg. Chem. 1998, 17, 3802, and references therein.