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26
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39749116552
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-
2): δ 216.9 [s, J(SnP) = 149 Hz, trans isomer].
-
2): δ 216.9 [s, J(SnP) = 149 Hz, trans isomer].
-
-
-
-
27
-
-
39749103208
-
-
12): δ 136.8 [s, J(SnP) = 563 Hz].
-
12): δ 136.8 [s, J(SnP) = 563 Hz].
-
-
-
-
28
-
-
39749201978
-
-
2): δ 19.3 [s, J(SnP) = 674 Hz].
-
2): δ 19.3 [s, J(SnP) = 674 Hz].
-
-
-
-
29
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39749178704
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-
X-ray data for 4·2C7H8: orange crystals, triclinic (P1, a, 12.1377(1) Å, b, 13.0674(1) Å, c, 13.2949(1) Å, α, 111.897(1)°, β, 102.987(1)°, γ, 104.300(1)°, V, 1774.30(4) Å3, T, 100 K, Z, 1, R, 0.0248 [observed data with I > 2σI, GOF, 1.333
-
3, T = 100 K, Z = 1, R = 0.0248 [observed data with I > 2σ(I)], GOF = 1.333.
-
-
-
-
30
-
-
39749121137
-
-
3, T = 120 K, Z = 4, R = 0.0499 [observed data with I > 2σ(I)], GOF = 1.02.
-
3, T = 120 K, Z = 4, R = 0.0499 [observed data with I > 2σ(I)], GOF = 1.02.
-
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31
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33644900751
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0000056821
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