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Inorganic Chemistry

Volumn 47, Issue 3, 2008, Pages 772-774

Multiferroic homochiral metal-organic framework

(6) Ye, Qiong a Fu, Da Wei a Tian, Hang a Xiong, Ren Gen a Chan, Philip Wai Hong b Huang, Songping D c

a SOUTHEAST UNIVERSITY (China)

b Nanyang Technological University (Singapore)

c KENT STATE UNIVERSITY (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 39749097881 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic701828w Document Type: Article

Times cited : (105)

References (29)

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- Synthesis of 1: The hydrothermal reaction of (L)-ethyl lactate (1.0 mL) in the presence of Tb(ClO4)3· 6H2O (1 mmol) with 1.5 mL of water in a sealed Pyrex tube at 110°C for 2-4 days gave colorless block compound 1 in 50% yield based on Tb(ClO4)3·6H2O after cooling down. IR (cm-1, 3480 (s, br, 2980 (vw, 2937 (vw, 1603 (vs, 1470 (m, 1434 (m, 1359 (m, 1315 (w, 1241 (w, 1105 (vs, 933 (w, 870 (w, 781 (w, 628 (w, 570 (w, 452 (w, Anal. Calcd for C6H14ClO 12Tb: C, 15.24; H, 2.96. Found: C, 15.30; H, 3.01. TGA suggests that MOF 1 can be stable before ca. 200°C (see the Supporting Information, Synthesis of 2: The hydrothermal reaction of (L)-ethyl lactate (1.0 mL) in the presence of Tb(ClO4) 3·6H2O (1 mmol) with 1.5 mL of deuterated oxide (D2O) in a sea
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- -1, S = 1.055; Flack parameter = 0.01-(4).

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