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3943067215
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note
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3): δ = 20.5, 55.2, 61.5, 64.4, 68.0, 68.6, 70.2, 72.7, 73.2, 73.4, 75.0, 75.7, 77.6, 79.8, 80.7, 81.8, 97.9, 127.6, 127.9, 128.1, 128.4, 137.8, 137.9, 138.5, 155.2, 169.5, 169.9, 170.5.
-
-
-
-
20
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3943082884
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note
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4 and the solvent was evaporated. The crude product was dissolved in dry MeOH (4 mL) and 70 μL of a 1 M solution of NaOMe (0.07 mmol) were added, furnishing 60 mg of 4d (92%) as a white solid after flash chromatography.
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23
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0000323139
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0242380218
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32
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3943052847
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note
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3OD): δ = 63.0, 66.4, 69.0, 72.0, 72.5, 76.1, 82.6, 156.8.
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