Liquid chromatographic fluorescence determination of amino acids in plasma and urine after derivatization with phanquinone

Biomedical Chromatography

Volumn 22, Issue 2, 2008, Pages 207-213

  Gatti, Rita ^a   Gioia, Maria Grazia ^a  

^a UNIVERSITY OF BOLOGNA   (Italy)

Author keywords

Amino acid determination; Biological sample; Liquid chromatography; Phanquinone; Pre chromatographic derivatization

Indexed keywords

BODY FLUIDS; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY;

AMINO ACID DETERMINATION; AMINO-ACIDS; BIOLOGICAL SAMPLES; DERIVATIZATIONS; FLUORESCENCE DETERMINATION; FLUOROGENIC REAGENTS; PHANQUINONE; PHENANTHROLINES; PRE-CHROMATOGRAPHIC DERIVATIZATION; PRE-COLUMN DERIVATISATION;

AMINO ACIDS;

ALANINE; AMINO ACID; ARGININE; ASPARAGINE; ASPARTIC ACID; BUFFER; GLUTAMINE; GLYCINE; HISTIDINE; ISOLEUCINE; LEUCINE; LYSINE; METHIONINE; PHANQUINONE; PHENYLALANINE; PHOSPHATE; SERINE; SULFOSALICYLIC ACID; TAURINE; THREONINE; VALINE;

AMINO ACID ANALYSIS; AMINO ACID BLOOD LEVEL; AMINO ACID URINE LEVEL; ARTICLE; CALIBRATION; CHEMICAL STRUCTURE; DERIVATIZATION; FLUORESCENCE; REVERSED PHASE HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; TEMPERATURE;

EID: 39349102367     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.917     Document Type: Article

References (17)

1. Aoyama C, Santa T, Tsunoda M, Fukushima T, Kitada C and Imai K. A fully automated ammo acid analyzer using NBD-F as a fluorescent derivatization reagent. Biomedical Chromatography 2004; 18: 630-636.
2. Blau K and Halket JM. Handbook of Derivatives for Chromatography. Wiley: New York, 1993.
3. Cynober LA. Plasma amino acid levels with a note on membrane transport: characteristic, regulation, and metabolic significance. Nutrition 2002; 18: 761-766.
4. Eistert B and Fink G. Reactions of α-dicarbonyl compounds and quinones with diazoalkanes. IV. Some experiments with phenanthroline-quinones. Berichte 1962; 95: 2395-2402.
5. European Pharmacopeia, 5th edn, Vol. 1. Council of Europe: France, 2004.
6. Fekkes D. State-of-the-art of high performance liquid chromatographic analysis of amino acids in physiological samples. Journal of Chromatography B 1996; 682: 3-22.
7. Fekkes D, van Dalen A, Edelman M and Voskuilen A. Validation of the determination of amino acids in plasma by high-performance liquid chromatography using automated pre-column derivatization with o-phthaldialdehyde. Journal of Chromatography B 1995; 669: 177-186.
8. Gatti R, Gioia MG and Di Pietra AM. Phanquinone: a useful fluorescent pre-chromatographic derivatization reagent for liquid chromatographic analyses of amino acids dosage forms. Analitica Chimica Acta 2002; 474: 11-20.
9. Gotti R, Gioia MG, Gatti R and Cavrini V. Phanquinone as a suitable derivatization reagent in micellar electrokinetic chromatography and HPLC analysis of amino acids. Journal of Separation Science 2006; 29: 1259-1267.
10. Kubačák P, Mikuš P, Valášková I and Havránek E. Simultaneous determination of essential basic amino acids in pharmaceuticals by capillary isotachophoresis. Archiv der Pharmazie 2006; 339: 96-99.
11. Lunn G and Hellwig LC. Handbook of Derivatization Reactions for HPLC. Wiley: New York, 1998.
12. O'Neil MJ, Smith A and Heckelmann PE. The Merck Index An Encyclopedia of Chemicals, Drugs, and Biologicals, 13th edn. Merck: Whitehouse Station, NJ, 2001.
13. Papadoyannis IN. HPLC in Clinical Chemistry. Marcel Dekker: New York, 1990.
14. Soga T, Kakazu Y, Robert M, Tomita M and Nishioka T. Qualitative and quantitative analysis of amino acids by capillary electrophoresis-electrospray ionization-tandem mass spectrometry. Electrophoresis 2004; 25: 1964-1972.
15. Sweetman SC. Martindale - The Complete Drug Reference, 34th edn. Pharmaceuticals Press: London, 2005.
16. Vogt H and Jeske P. Contribution to the preparation and bactericidal effects of 5- and 6-substituted quaternary 8-hydroxyquinoline derivatives. IV. Synthesis and bacteriological effects of disinfectants. Archiv der Pharmazie 1958; 291: 168-180.
17. Yokoyama Y, Tsuji S and Sato H. Simultaneous determination of creatinine, creatine, and UV-absorbing amino acids using dual-mode gradient low-capacity cation-exchange chromatography. Journal of Chromatography A 2005; 1085: 110-116.