PGSTE-WATERGATE: An STE-based PGSE NMR sequence with excellent solvent suppression

Journal of Magnetic Resonance

Volumn 191, Issue 1, 2008, Pages 159-163

  Zheng, Gang ^a   Stait Gardner, Timothy ^a   Anil Kumar, P G ^a   Torres, Allan M ^a   Price, William S ^a  

^a UNIVERSITY OF WESTERN SYDNEY   (Australia)

Author keywords

Diffusion; PGSE; PGSTE; Solvent suppression; WATERGATE

Indexed keywords

COMBINATORIAL MATHEMATICS; DIFFUSION; DRUG PRODUCTS; NUCLEAR MAGNETIC RESONANCE; SUGAR (SUCROSE);

PULSED GRADIENTS; SOLVENT SUPPRESSION;

ORGANIC SOLVENTS;

SOLVENT; WATER;

ALGORITHM; ARTICLE; ARTIFACT; CHEMISTRY; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SIGNAL PROCESSING;

ALGORITHMS; ARTIFACTS; MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SIGNAL PROCESSING, COMPUTER-ASSISTED; SOLVENTS; WATER;

EID: 39149136509     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2007.12.001     Document Type: Article

References (21)

1. Stilbs P. Fourier transform pulsed-gradient spin-echo studies of molecular diffusion. Prog. Nucl. Magn. Reson. Spectrosc. 19 (1987) 1-45
2. Johnson Jr. C.S. Diffusion ordered nuclear magnetic resonance spectroscopy: principles and applications. Prog. Nucl. Magn. Reson. Spectrosc. 34 (1999) 203-256
3. Price W.S. Gradient NMR. Annu. Rep. NMR Spectrosc. (1996), Academic Press, New York 51-142
4. Price W.S. Water signal suppression in NMR spectroscopy. In: Webb G.A. (Ed). Annu. Rep. NMR Spectrosc. vol. 38 (1999), Academic Press, London 289-354
5. Warren W.S., Hammes S.L., and Bates J.L. Dynamics of radiation damping in nuclear magnetic resonance. J. Chem. Phys. 91 (1989) 5895-5904
6. Lin Y.Y., Lisitza N., Ahn S., and Warren W.S. Resurrection of crushed magnetization and chaotic dynamics in solution NMR spectroscopy. Science 290 (2000) 118-122
7. Piotto M., Saudek V., and Sklenář V. Gradient-tailored excitation for single-quantum NMR spectroscopy of aqueous solutions. J. Biomol. NMR 2 (1992) 661-665
8. V. Saudek, M. Piotto, V. Sklenár, Bruker Report, 1994, p. 6.
9. 15N HSQC experiments optimized to retain full sensitivity. J. Magn. Reson. Ser. A 102 (1993) 241-245
10. 1H NMR spectroscopy of biological fluids. Anal. Chem. 68 (1996) 3370-3376
11. Hwang T.L., and Shaka A.J. Water suppression that works. Excitation sculpting using arbitrary wave-forms and pulsed-field gradients. J. Magn. Reson. Ser. A 112 (1995) 275-279
12. Price W.S., Elwinger F., Vigouroux C., and Stilbs P. PGSE-WATERGATE, a new tool for NMR diffusion-based studies of ligand-macromolecule binding. Magn. Reson. Chem. 40 (2002) 391
13. Farrar T.C. Density matrices in NMR spectroscopy: part I. Concepts Magn. Reson. A 2 (1990) 1-12
14. Levitt M.H. Spin Dynamics: Basics of Nuclear Magnetic Resonance (2001), John Wiley & Sons, Chichester, New York
15. Pelta M.D., Morris G.A., Stchedroff M.J., and Hammond S.J. A one-shot sequence for high-resolution diffusion-ordered spectroscopy. Magn. Reson. Chem. 40 (2002) 147-152
16. Sun P.Z., Seland J.G., and Cory D. Background gradient suppression in pulsed gradient stimulated echo measurements. J. Magn. Reson. 161 (2003) 168-173
17. Galvosas P., Stallmach F., and Kärger J. Background gradient suppression in stimulated echo NMR diffusion studies using magic pulsed field gradient ratios. J. Magn. Reson. 166 (2004) 164-173
18. Liu M.L., Mao X.A., Ye C.H., Huang H., Nicholson J.K., and Lindon J.C. Improved WATERGATE pulse sequences for solvent suppression in NMR spectroscopy. J. Magn. Reson. 132 (1998) 125-129
19. Kingsley P.B. Product operators, coherence pathways, and phase cycling. Part III: phase cycling. Concepts Magn. Reson. 7 (1995) 167-192
20. Mills R. Self-diffusion in normal and heavy water in the range 1-45 deg. J. Phys. Chem. 77 (1973) 685-688
21. Price W.S., Tsuchiya F., and Arata Y. Lysozyme aggregation and solution properties studied using PGSE NMR diffusion measurements. J. Am. Chem. Soc. 121 (1999) 11503-11512