Isotropic filtering using polyhedral phase cycles: Application to singlet state NMR

Journal of Magnetic Resonance

Volumn 191, Issue 1, 2008, Pages 148-155

  Pileio, Giuseppe ^a   Levitt, Malcolm H ^a  

^a UNIVERSITY OF SOUTHAMPTON   (United Kingdom)

Author keywords

Isotropic filtering; Long lived spin states; Phase cycling; Singlet states; Spherical tensor operators

Indexed keywords

FILTRATION; RADIO FREQUENCY IDENTIFICATION (RFID); SOLUTIONS; TENSORS;

ISOTROPIC FILTERING; LONG-LIVED SPIN STATES; PHASE CYCLING; SINGLET STATES; SPHERICAL TENSOR OPERATORS;

NUCLEAR MAGNETIC RESONANCE;

ALGORITHM; ANISOTROPY; ARTICLE; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY; SENSITIVITY AND SPECIFICITY; SIGNAL PROCESSING;

ALGORITHMS; ANISOTROPY; MAGNETIC RESONANCE SPECTROSCOPY; REPRODUCIBILITY OF RESULTS; SENSITIVITY AND SPECIFICITY; SIGNAL PROCESSING, COMPUTER-ASSISTED;

EID: 39149124771     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2007.11.021     Document Type: Article

References (28)

1. Ernst R.R., Bodenhausen G., and Wokaun A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions (1987), Clarendon Press, Oxford
2. Keeler J. Understanding NMR Spectroscopy (2005), Wiley, Chichester
3. Levitt M.H., Madhu P.K., and Hughes C.E. Cogwheel Phase Cycling. J. Magn. Reson. 155 (2002) 300-306
4. Jerschow A., and Kumar R. Calculation of coherence pathway selection and cogwheel cycles. J. Magn. Reson. 160 (2003) 59-64
5. Ivchenko N., Hughes C.E., and Levitt M.H. Application of cogwheel phase cycling to sideband manipulation experiments in solid-state NMR. J. Magn. Reson. 164 (2003) 286-293
6. Zuckerstätter G., and Müller N. Coherence pathway selection by cogwheel phase cycling in liquid-state NMR. Concepts Magn. Reson. 30A (2007) 81-99
7. Ivchenko N., Hughes C.E., and Levitt M.H. Multiplex phase cycling. J. Magn. Reson. 160 (2003) 52-58
8. Suter D., and Pearson J.G. Experimental classification of multi-spin coherence under the full rotation group. Chem. Phys. Lett. 144 (1988) 328
9. van Beek J.D., Carravetta M., Antonioli G.C., and Levitt M.H. Spherical tensor analysis of nuclear magnetic resonance signals. J. Chem. Phys. 122 (2005) 24510
10. Bowden G.J., and Hutchison W.D. Tensor operator formalism for multiple-quantum NMR. 1. Spin-1 nuclei. J. Magn. Reson. 67 (1986) 403-414
11. Sanctuary B.C., and Halstead T.K. Multipole NMR Adv. Magn. Opt. Reson. 15 (1990) 80
12. 1 limit: singlet nuclear spin states in low magnetic fields. Phys. Rev. Lett. 92 (2004) 153003
13. Carravetta M., and Levitt M.H. Theory of long-lived nuclear spin states in solution nuclear magnetic resonance. I. Singlet states in low magnetic field. J. Chem. Phys. 122 (2005) 214505
14. Carravetta M., and Levitt M.H. Long-lived nuclear spin states in high-field solution NMR. J. Am. Chem. Soc. 126 (2004) 6228-6229
15. Pileio G., Concistrè M., Carravetta M., and Levitt M.H. Long-lived nuclear spin states in the solution NMR of four-spin systems. J. Magn. Reson. 182 (2006) 353-357
16. Cavadini S., Dittmer J., Antonijevic S., and Bodenhausen G. Slow diffusion by singlet state NMR. J. Am. Chem. Soc. 127 (2005) 15744-15748
17. Gopalakrishnan K., and Bodenhausen G. Lifetimes of singlet-states under coherent off-resonance irradiation in NMR spectroscopy. J. Magn. Reson. 182 (2006) 254-259
18. Sarkar R., Vasos P.R., and Bodenhausen G. Singlet-state exchange NMR spectroscopy for the study of very slow dynamic processes. J. Am. Chem. Soc. 129 (2007) 328-334
19. 13C hyperpolarization in small molecules with parahydrogen-induced polarization. J. Chem. Phys. 124 (2006) 201109
20. Pileio G., and Levitt M.H. J-stabilization of singlet states in the solution NMR of multiple-spin system. J. Magn. Reson. 187 (2007) 141-145
21. Vinogradov E., and Grant A.K. Long lived states in solution NMR: selection rules for intramolecular dipolar relaxation in low magnetic fields. J. Magn. Reson. 188 (2007) 176-182
22. Carravetta M., Danquigny A., Mamone S., Cuda F., Johannessen O.G., Heinmaa I., Panesar K., Stern R., Grossel M.C., Horsewill A.J., Samoson A., Murata M., Murata Y., Komatsu K., and Levitt M.H. Solid-state NMR of endohedral hydrogen-fullerene complexes. Phys. Chem. Chem. Phys. 9 (2007) 4879
23. Edén M., and Levitt M.H. Computation of orientational averages in solid state NMR by Gaussian spherical quadrature. J. Magn. Reson. 132 (1998) 220-239
24. Stevensson B., and Edén M. Efficient orientational averaging by the extension of Lebedev grids via regularized octahedral symmetry expansion. J. Magn. Reson. 181 (2006) 162-176
25. Jeener J. Superoperators in magnetic resonance. Adv. Magn. Reson. 10 (1982) 1-51
26. Coxeter H.S.M. Regular Polytopes (1963), Macmillan, New York
27. Samoson A., Lippmaa E., and Pines A. High-resolution solid-state NMR averaging of second-order effects by means of a double rotor. Mol. Phys. 65 (1988) 1013-1018
28. Chmelka B.F., and Pines A. Some developments in nuclear magnetic resonance of solids. Science 246 (1989) 71-77