Separation of propylene/propane mixtures by titanosilicate ETS-10 membranes prepared in one-step seeded hydrothermal synthesis

Journal of Membrane Science

Volumn 311, Issue 1-2, 2008, Pages 326-335

  Tiscornia, Inés ^a   Irusta, Silvia ^a   Téllez, Carlos ^a   Coronas, Joaquín ^a   Santamaría, Jesús ^a  

^a UNIVERSITY OF ZARAGOZA   (Spain)

Author keywords

ETS 10; Microporous titanosilicate; Propylene separation; Titanosilicate membranes; XPS analysis

Indexed keywords

ADSORPTION; HEAT TREATMENT; HYDROTHERMAL SYNTHESIS; SCANNING ELECTRON MICROSCOPY; SEPARATION; SILICATES; X RAY DIFFRACTION; X RAY PHOTOELECTRON SPECTROSCOPY;

MICROPOROUS TITANOSILICATE; PROPYLENE SEPARATION; TITANOSILICATE MEMBRANES;

PROPYLENE;

FLUORIDE; POLYMER; PROPANE; PROPYLENE; SILICATE; TITANIUM DERIVATIVE;

ADSORPTION; HEAT TREATMENT; HYDROTHERMAL SYNTHESIS; PROPYLENE; SCANNING ELECTRON MICROSCOPY; SEPARATION; SILICATES; X RAY DIFFRACTION; X RAY PHOTOELECTRON SPECTROSCOPY;

ARTICLE; MEMBRANE COMPONENT; MEMBRANE PERMEABILITY; MEMBRANE STABILIZATION; MEMBRANE STRUCTURE; PETROCHEMICAL INDUSTRY; PH MEASUREMENT; PRIORITY JOURNAL; SCANNING ELECTRON MICROSCOPY; SEPARATION TECHNIQUE; SYNTHESIS; TEMPERATURE SENSITIVITY; X RAY DIFFRACTION;

EID: 39149113098     PISSN: 03767388     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.memsci.2007.12.028     Document Type: Article

References (40)

1. Rocha J., and Lin Z. Microporous mixed octahedral-pentahedral-tetrahedral framework silicates. Rev. Mineral Geochem. 57 (2005) 173-201
2. 2 composite membranes and their pervaporation performance. J. Membr. Sci. 174 (2000) 31-42
3. Guan G., Kusakabe K., and Morooka S. Synthesis and permeation properties of ion-exchanged ETS-4 tubular membranes. Micropor. Mesopor. Mater. 50 (2001) 109-120
4. Shattuck K.G., Yilmaz B., Warzywoda J., and Sacco A. Hydrothermal synthesis of oriented ETS-4 films on porous α-alumina substrates. Micropor. Mesopor. Mater. 88 (2006) 56-62
5. Yilmaz B., Shattuck K.G., Warzywoda J., and Sacco A. Oriented growth of ETS-4 films using the method of secondary growth. Chem. Mater. 18 (2006) 1107-1112
6. Sebastián V., Lin Z., Rocha J., Téllez C., Santamaría J., and Coronas J. Synthesis, characterization, and separation properties of Sn- and Ti-silicate umbite membranes. Chem. Mater. 18 (2006) 2472-2479
7. Jeong H.K., Krohn J., Sujaoti K., and Tsapatsis M. Oriented molecular sieve membranes by heteroepitaxial growth. J. Am. Chem. Soc. 124 (2002) 12966-12968
8. Lin Z., Rocha J., Navajas A., Téllez C., Coronas J., and Santamaría J. Synthesis and characterisation of titanosilicate ETS-10 membranes. Micropor. Mesopor. Mater. 67 (2004) 79-86
9. Kita H., Li X., Takei K., Zhang X., Okamoto K., and Itabashi K. Synthesis of highly acid-resistant zeolite membranes and their permeation properties. In: Akin F., and Lin Y. (Eds). Proceedings of the 8th International Conference on Inorganic Membranes. Cincinnati, USA (2004) 250-253
10. Tiscornia I., Lin Z., Rocha J., Téllez C., Coronas J., and Santamaría J. Preparation of titanosilicate ETS-10 and vanadosilicate AM-6 membranes. Stud. Surf. Sci. Catal. 158 (2005) 423-430
11. Ji Z., Warzywoda J., and Sacco A. Titanosilicate ETS-10 thin film preparation on fused silica optical fibers. Micropor. Mesopor. Mater. 101 (2007) 279-287
12. Lin Z., Rainho J.P., Domingues J., Carlos L.D., and Rocha J. Photoluminescent films of microporous titanosilicate ETS-10 doped with europium(III). Micropor. Mesopor. Mater. 79 (2005) 13-19
13. 8 separation using polymeric membranes. J. Membr. Sci. 211 (2003) 299-309
14. Stoitsas K.A., Gotzias A., Kikkinides E.S., Steriotis Th.A., Kanellopoulos N.K., Stoukides M., and Zaspalis V.T. Porous ceramic membranes for propane-propylene separation via the π-complexation mechanism: unsupported systems. Micropor. Mesopor. Mater. 78 (2005) 235-243
15. Nair B.N., Keizer K., Elferink W.J., Gilde M.J., Verweij H., and Burggraaf A.J. Synthesis, characterisation and gas permeation studies on microporous silica and alumina-silica membranes for separation of propane and propylene. J. Membr. Sci. 116 (1996) 161-169
16. Nikolakis V., Xomeritakis G., Abibi A., Dickson M., Tsapatsis M., and Vlachos D.G. Growth of a faujasite-type zeolite membrane and its application in the separation of saturated/unsaturated hydrocarbon mixtures. J. Membr. Sci. 184 (2001) 209-219
17. Giannakopoulos I.G., and Nikolakis V. Separation of propylene/propane mixtures using faujasite-type zeolite membranes. Ind. Eng. Chem. Res. 44 (2005) 226-230
18. Fuertes A.B., and Menendez I. Separation of hydrocarbon gas mixtures using phenolic resin-based carbon membranes. Sep. Purif. Technol. 28 (2002) 29-41
19. Yamamoto M., Kusakabe K., Hayashi J., and Morooka S. Carbon molecular sieve membrane formed by oxidative carbonization of a copolyimide film coated on a porous support tube. J. Membr. Sci. 133 (1997) 195-205
20. Yoshino M., Nakamura S., Kita H., Okamoto K.I., Tanihara N., and Kusuki Y. Olefin/paraffin separation performance of carbonized membranes derived from an asymmetric hollow fiber membrane of 6FDA/BPDA-DDBT copolyimide. J. Membr. Sci. 215 (2003) 169-183
21. Al-Baghli N.A., and Loughlin K.F. Binary and ternary adsorption of methane, ethane, and ethylene on titanosilicate ETS-10 zeolite. J. Chem. Eng. Data 51 (2006) 248-254
22. Tiscornia I., Prádanos P., Irusta S., Téllez C., Coronas J., and Santamaría J. Preparation and characterization of titanosilicate Ag-ETS-10 for propylene and propane adsorption. J. Phys. Chem. C 111 (2007) 4702-4709
23. 2: a comprehensive study. Micropor Mesopor. Mater. 23 (1998) 253-263
24. Lv L., Su F., and Zhao X.S. A reinforced study on the synthesis of microporous titanosilicate ETS-10. Micropor. Mesopor. Mater. 76 (2004) 113-122
25. Bernal M.P., Coronas J., Menéndez M., and Santamaría J. Characterization of zeolite membranes by temperature programmed permeation and step desorption. J. Membr. Sci. 195 (2002) 125-138
26. Anderson M.W., Terasaki O., Ohsuna T., Malley P.J.O., Philippou A., MacKay S.P., Ferreira A., Rocha J., and Lidin S. Microporous titanosilicate ETS-10: a structural survey. Philos. Mag. B 71 (1995) 813-841
27. Noack M., Kölsch P., Schäfer R., Toussaint P., Sieber I., and Caro J. Preparation of MFI membranes of enlarged area with high reproducibility. Micropor. Mesopor. Mater. 49 (2001) 25-37
28. 3 supports. Sep. Purif. Technol. 32 (2003) 397-401
29. Kong C., Lu J., Yang J., and Wang J. Preparation of silicalite-1 membranes on stainless steel supports by a two-stage varying-temperature in situ synthesis. J. Membr. Sci. 285 (2006) 258-264
30. Navajas A., Mallada R., Téllez C., Coronas J., Menéndez M., and Santamaría J. Study on the reproducibility of mordenite tubular membranes for the dehydration of ethanol. J. Membr. Sci. 299 (2007) 166-173
31. Sridhar S., and Khan A.A. Simulation studies for the separation of propylene and propane by ethylcellulose membrane. J. Membr. Sci. 159 (1999) 209-219
32. Shimazu A., Miyazaki T., Maeda M., and Ikeda K. Relationships between the chemical structures and the solubility, diffusivity, and permselectivity of propylene and propane in 6FDA-based polymides. J. Polym. Sci. B: Polym. Phys. 38 (2000) 2525-2536
33. 2. Micropor. Mesopor. Mater. 81 (2005) 1-10
34. Ech-chamikh E., Essafti A., Ijdiyaou Y., and Azizan M. XPS study of amorphous carbon nitride (a-C:N) thin films deposited by reactive RF sputtering. Sol. Energy Mater. Sol. C 90 (2006) 1420-1423
35. Swaraj S., Oran U., Lippitz A., Friedrich J., and Unger W. Study of influence of external plasma parameters on plasma polymerised films prepared from organic molecules (acrylic acid, allyl alcohol, allyl amine) using XPS and NEXAFS. Surf. Coat. Technol. 200 (2005) 494-497
36. Zecchina A., Xamena F.X.L.I., Paze C., Palomino G.T., Bordiga S., and Arean C.O. Alkyne polymerization on the titanosilicate molecular sieve ETS-10. Phys. Chem. Chem. Phys. 3 (2001) 1228-1231
37. Krisnandi Y., and Howe R. Effects of ion-exchange on the photoreactivity of ETS-10. Appl. Catal. A 307 (2006) 62-69
38. Lv L., Lee F., Zhou J., and Zhao X. XPS study on microporous titanosilicate ETS-10 upon acid treatment. Micropor. Mesopor. Mater. 96 (2006) 270-275
39. Hasegawa Y., and Ayame A. Investigation of oxidation states of titanium in titanium silicalite-1 by X-ray photoelectron spectroscopy. Catal. Today 71 (2001) 177-187
40. In: Wagner C., Riggs W., Davis L., Moulder J., and Muilenberg G. (Eds). Handbook of X-ray Photoelectron Spectroscopy (1979), Perkin-Elmer Corporation