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27
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85069409169
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-
note
-
Satisfactory C, H and N microanalytical data were obtained for the formulae 1, 2 and 4.
-
-
-
-
28
-
-
85069413744
-
-
note
-
The yellow crystals had been found to lose solvent rapidly, and they were kept in the mother liquor until a suitable crystal was selected for crystallography.
-
-
-
-
29
-
-
85069399046
-
-
note
-
2) = 0.0560 (0.1646) for 2819 observed (I > 2σ(I)) reflections.
-
-
-
-
31
-
-
85069407623
-
-
note
-
Its identity was confirmed by a unit cell determination and comparison with the authentic material.
-
-
-
-
33
-
-
85069406447
-
-
and references therein
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36
-
-
85069417863
-
-
note
-
This remains up to date the only procedure for the isolation of pure 1; on the contrary the yellow crystals of 2 · 2MeCN are always isolated in a mixture with orange crystals of 1.
-
-
-
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38
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25344454818
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