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38949206233
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Selocted data for 3: FABMS: m/z 402 [M+H, 1H NMR (CDCl3, δ 7.83 (dd, 1H, H-8, 7.63 (br s, 1H, H-5, 7.50 (dd, 1H, J6.7, 8.0 Hz, 6.8d, 2.0 Hz, H-6, 7.18 (t IH, J7.8, 7.9 H7, H-7, 6.83 (dd, 1H, J, 9.0 Hz, 4.5 Hz, H-2, 5.32 (br s, 1H, H-13, 4.40-4.00 (m, 6H, 3xCH2CH3, 3.32 (dd, 1H, CH2-1a, 3.08 (dd, 1H, H-1b, 1.34 (t, 3H, J= 7.0 Hz, CH2CH3, 1.18 (2xt, 6H, J= 7.1 Hz, CH2CH3, 13C NMR (CDC13, δ 192.9 (C-9, 169.0, 162.3, 154.0 (C=0, 144.4 (C-2, 140.5 (C-11, 134.7 (C-3, 132.6 (C-6, 127.3 (C-8, 125.5 (C-7, 125.2 (C-10, 124.6 (C-5, 65.3, 63.5 (2xCH2CH3, 62.7 (C-12, 62.0 (CH2CH3, 60.5 (C-13, 39.1 (C-1, 14.4, 14.1, 13.9 3xCH2CH3
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3).
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11
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0001021516
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Lindner, J.9
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13
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38949112771
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Crystal lrrpct GbR bohn (Germany); for Software Review see: W. T. Pennington, J. Appl. Cryst., 1999, 32, 1028.
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Crystal lrrpct GbR bohn (Germany); for Software Review see: W. T. Pennington, J. Appl. Cryst., 1999, 32, 1028.
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