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For other chiral supramolecular assemblies, see: a
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dim values for 5 and 8 will be published in an upcoming paper.
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dim values for 5 and 8 will be published in an upcoming paper.
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Analytical Data Compound 3:11 1H NMR (300 MHz, DMSO-d6, δ, 10.22 (s, 1 H, 8.31 (d, 2 H, J, 8.01 Hz, 7.55 (m, 5 H, 3.34 (s, 3 H) ppm. 13C NMR (75 MHz, DMSO-d6, δ, 171.8, 171.2, 168.4, 164.9, 137.0, 132.8, 129.3, 128.8, 26.4 ppm. Compound 4: mp 188-191°C. 1H NMR (300 MHz, DMSO-d6, δ, 8.35 (d, 2 H, J, 7.74 Hz, 7.94 (s, 1 H, 7.48 (m, 5 H, 1.33 (s, 9 H) ppm. 13C NMR (75 MHz, DMSO-d6, δ, 176.5, 173.1, 168.3, 164.5, 136.1, 132.6, 128.9, 40.9, 27.8 ppm. Compound 5: 1H NMR (300 MHz, DMSO-d6, δ, 8.63 (s, 1 H, 8.58 (s, 1 H, 8.46 (d, 2 H, J, 6.18 Hz, 7.53 (m, 3 H, 5.96 (m, 1 H, 5.11 (m, 2 H, 3.19 (t, 2 H, J, 7.28 Hz, 2.55 (q, 2 H, J, 7.16 Hz, 1.38 (s, 9 H) ppm. 13C NMR 75 MHz, DMSO-d6
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