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Volumn 37, Issue 1, 2008, Pages 16-17

Solvatochromic luminescence based on the excimer formation of bipyridine platinum(II) complexes with linear alkyl chains

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EID: 38949150077 PISSN: 03667022 EISSN: None Source Type: Journal
DOI: 10.1246/cl.2008.16 Document Type: Article

Times cited : (17)

References (17)

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8
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- 3): γ 0.87 (t, 2H), 1.25-1.32 (broad, 16H), 1.68 (t, 2H), 2.7 (t, 2H), 7.12 (t, 2H), 8.22 (s, 1H), 8.56 (d, 1H). ESI-MS m/z: 465 (M + 1). Mp 68-70 °C.
- 3): γ 0.87 (t, 2H), 1.25-1.32 (broad, 16H), 1.68 (t, 2H), 2.7 (t, 2H), 7.12 (t, 2H), 8.22 (s, 1H), 8.56 (d, 1H). ESI-MS m/z: 465 (M + 1). Mp 68-70 °C.

9
- 38949176924
- For [Pt(CN)2(dC9bpy)L 1HNMR (in CDCl3, γ 0.88 (t, 3H, 1.28-1.38 (br, 12H, 1.75 (m, 2H, 2.86 (t, 2H, 7.39 (d, 1H, 7.96 (s, 1H, 9.12 (d, 1H, 13CNMR (in CDCl3, γ 14.1, 22.6, 29.2, 29.3, 29.4, 29.6, 29.8, 31.8, 36.0, 106.8, 123.5, 127.6, 151.1, 155.6, 158.2. IR (KBr, cm-1, 2135, 2146 (VCN, Mp 181 °C. For [Pt(CN)2(dC11bpy, 1HNMR (in CDCl3, γ 0.88 (t, 3H, 1.27-1.38 (br, 16H, 1.75 (t, 2H, 2.86 (t, 2H, 7.38 (d, 1H, 7.96 (s, 1H, 9.08 (d, 1H, 13CNMR (in CDCl3, γ 14.1, 22.6, 29.2, 29.3, 29.3, 29.4, 29.5, 29.5, 29.8, 31.8, 36.0, 106.9, 123.5, 127.6, 151.3, 155.6, 158.1. IR (KBr, cm-1, 2135, 2146 VCN, Mp 185 °C
- CN). Mp 185 °C.

10
- 38949175631
- Crystal data for [Pt(CN)2(dC9bpyJ]-CH 3CN, Formula: C32-H47N5Pt 1, M, 696.85, triclinic, a, 9.829(3, b, 10.325(4, c= 16.264(6) Å, α, 84.824(9)°, β, 83.338(9)°, γ, 78.820(9)°, U, 1604.6(10) Å3, T, 173 K, space group, P1, Z, 2, D caicd, 1.442 gcm-3. For [Pt(CN)2(dC 11bpy)]•CH3CN, Formula: C36H 55N5Pt1, Mr, 752.95, triclinic, a, 9.7952(2, b= 10.3271(5, c, 18.3967(5) Å, α, 80.567(7)°, β, 82.046(7)°, γ, 79.745(7)°, U, 1795.0(1) Å3, T =173 K, space group, P1, Z, 2, Dcalcd, 1.393 g cm-3. Full crystallographic details have been deposited with Cambridge Crystallograph
- -3. Full crystallographic details have been deposited with Cambridge Crystallographic Data Centre as supplementary publication nos. CCDC-658486 and 658485, respectively.

11
- 38949183869
- Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journal/chem-lett/index.html.
- Supporting Information is available electronically on the CSJ-Journal Web site, http://www.csj.jp/journal/chem-lett/index.html.

12
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- and cited therein
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- Ma, B.¹ Djurovich, P.I.² Thompson, M.E.³

17
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