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Volumn 29, Issue 1, 2008, Pages 241-244

Discrete and continuous soft metal complexes of O2S2 and NO2S2 macrocycles with endo- or exo-coordination mode

Author keywords

Coordination polymer; Copper(I) complex; Exo coordination; Mercury(II) complex; O2S2 and NO2S2 macrocycles

Indexed keywords


EID: 38949128722     PISSN: 02532964     EISSN: 12295949     Source Type: Journal    
DOI: 10.5012/bkcs.2008.29.1.241     Document Type: Article
Times cited : (9)

References (24)
  • 14
    • 38949147552 scopus 로고    scopus 로고
    • Parker, D. In Chapter 3, Macrocycle Synthesis: A Practical Approach; Oxford University Press: Oxford, 1996.
    • Parker, D. In Chapter 3, Macrocycle Synthesis: A Practical Approach; Oxford University Press: Oxford, 1996.
  • 18
    • 38949130906 scopus 로고    scopus 로고
    • A crystal was mounted on a Bruker SMART diffractometer equipped with a graphite monochromated Mo Kα (λ, 0.71073 Å) radiation source and a CCD detector. The frame data were processed to give structure factors using the program SAINT. The intensity data were corrected for Lorentz and polarization effects. Empirical absorption corrections were also applied for complexes using the program SADABS. The structure was solved by direct method and refined by full matrix least squares against F2 for all data using SHELXTL software. All non-H atoms were refined with anisotropic displacement parameters. Crystal data for 1: C24H 24Cl2HgO2S2, M, 680.04, Monoclinic, a, 11.0144(4) Å, b, 7.8393(3) Å, c, 28.2461(11) Å, β, 98.608(1)°, V, 2411.44(16) Å3, T, 173(2) K, space group P2 1/n, Z
    • 2 = 0.0727) for 5883 independent reflections [I > 2σ (I)].


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.