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Volumn , Issue 1, 2008, Pages 0037-0040

A new reagent system for efficient silylation of alcohols: Silyl chloride-N-methylimidazole-iodine

Author keywords

Iodine; N methylimidazole; Silyl chlorides; Silylation

Indexed keywords

1 METHYLIMIDAZOLE; ALCOHOL; CHLORIDE; IODINE;

ARTICLE; CHEMICAL REACTION; SILYLATION;

EID: 38549148294 PISSN: 09365214 EISSN: None Source Type: Journal
DOI: 10.1055/s-2007-992379 Document Type: Article

Times cited : (32)

References (16)

1
- 84989409179
- Lalonde, M.; Chan, T. H. Synthesis 1985, 817.
- (1985) Synthesis , pp. 817
- Lalonde, M.¹ Chan, T.H.²

2
- 0011564420
- Akerman, E. Acta Chem. Scand. 1957, 11, 373.
- (1957) Acta Chem. Scand , vol.11 , pp. 373
- Akerman, E.¹

3
- 0029841253
- Nelson, T. D.; Crouch, R. D. Synthesis 1996, 1031.
- (1996) Synthesis , pp. 1031
- Nelson, T.D.¹ Crouch, R.D.²

4
- 0003463148
- 2nd ed, Wiley: New York
- Green, T. W. Protective Groups in Organic Synthesis, 2nd ed.; Wiley: New York, 1991.
- (1991) Protective Groups in Organic Synthesis
- Green, T.W.¹

5
- 29644432244
- Corey, E. J.; Venkateswarlu, A. J. Am. Chem. Soc. 1972, 94, 6190.
- (1972) J. Am. Chem. Soc , vol.94 , pp. 6190
- Corey, E.J.¹ Venkateswarlu, A.²

6
- 85182022279
- Mizhiritski, M. D.; Yuzhelevskii, Y. A. Russ. Chem. Rev. 1987, 56, 355.
- (1987) Russ. Chem. Rev , vol.56 , pp. 355
- Mizhiritski, M.D.¹ Yuzhelevskii, Y.A.²

7
- 0031809210
- Gihani, M. T. E.; Heaney, H. Synthesis 1998, 357.
- (1998) Synthesis , pp. 357
- Gihani, M.T.E.¹ Heaney, H.²

8
- 38549133657
- Nilsson, J.; Stawinski, J. Collect. Symp. Ser. 2002, 5, 87.
- (2002) Collect. Symp. Ser , vol.5 , pp. 87
- Nilsson, J.¹ Stawinski, J.²

9
- 38549160421
- Nilsson, J.; Kraszewski, A.; Stawinski, J. Lett. Org. Chem. 2005, 2, 188.
- (2005) Lett. Org. Chem , vol.2 , pp. 188
- Nilsson, J.¹ Kraszewski, A.² Stawinski, J.³

10
- 0011035422
- Le Goaller, R.; Handel, H.; Labbe, P.; Pierre, J. L. J. Am. Chem. Soc. 1984, 106, 1694.
- (1984) J. Am. Chem. Soc , vol.106 , pp. 1694
- Le Goaller, R.¹ Handel, H.² Labbe, P.³ Pierre, J.L.⁴

11
- 38549090385
- General Procedure for the Preparative Silylation of Alcohols Listed in Table 1: An alcohol (1.0 mmol, N-methylimidazole (3.0 mmol) and iodine (2.0-3.0 mmol) were dissolved in an appropriate, anhyd solvent (3 mL, Table 1, A silyl chloride (TBDMSCl, TBDPSCl or TIPSCl; 1.1 mmol) was added and the reaction mixture was stirred at r.t. until the complete disappearance of the starting material (TLC analysis, The solvent was evaporated, the residue dissolved in EtOAc and washed with coned aq Na2S2O 3. The organic phase was dried over anhyd Na2SO 4 and evaporated. The products were purified by silica gel column chromatography CH2Cl2-MeOH, 100:0 → 95:5, Table 1 entries 1, 3 and 7; pentane-EtOAc, 10:0 → 9:1, Table 1 entries 2, 4-6, 8-10, The synthesized compounds were fully characterized with 1H and 13C NMR and HRMS
- 13C NMR and HRMS.

12
- 0342444538
- Strömberg, R.; Stawinski, J. Nucleosides Nucleotides 1987, 6, 815.
- (1987) Nucleosides Nucleotides , vol.6 , pp. 815
- Strömberg, R.¹ Stawinski, J.²

13
- 0004152586
- Pergamon Press: Oxford
- Greenwood, N. N.; Earnshaw, A. Chemistry of the Elements; Pergamon Press: Oxford, 1984, 978.
- (1984) Chemistry of the Elements , pp. 978
- Greenwood, N.N.¹ Earnshaw, A.²

14
- 38549109851
- Karimi, B.; Golshani, B. J. Org. Chem. 2000, 65, 7118.
- (2000) J. Org. Chem , vol.65 , pp. 7118
- Karimi, B.¹ Golshani, B.²

15
- 0037071207
- Firouzabadi, H.; Iranpoor, N.; Sobhani, S. Tetrahedron Lett. 2002, 43, 3653.
- (2002) Tetrahedron Lett , vol.43 , pp. 3653
- Firouzabadi, H.¹ Iranpoor, N.² Sobhani, S.³

16
- 85077952606
- Saxena, I.; Deka, N.; Sarma, J. C.; Tsuboi, S. Synth. Commun. 2003, 33, 4005.
- (2003) Synth. Commun , vol.33 , pp. 4005
- Saxena, I.¹ Deka, N.² Sarma, J.C.³ Tsuboi, S.⁴

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