L-Glutamic acid precipitation: Agglomeration effects

Crystal Growth and Design

Volumn 8, Issue 1, 2008, Pages 224-237

  Lindenberg, Christian ^a   Schöll, Jochen ^a   Vicum, Lars ^a   Mazzotti, Marco ^a   Brozio, Jörg ^b  

^a ETH ZURICH   (Switzerland)

^b NOVARTIS PHARMA AG   (Switzerland)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 38449098532     PISSN: 15287483     EISSN: None     Source Type: Journal    
DOI: 10.1021/cg070161f     Document Type: Article

References (39)

1. Schöll, J.; Bonalumi, D.; Vicum, L.; Mazzotti, M.; Muller, M. In situ monitoring and modeling of the solvent-mediated polymorphic transformation of L-glutamic acid. Cryst. Growth Des. 2006, 6 (4), 881-891.
2. Schöll, J.; Vicum, L.; Muller, M.; Mazzotti, M. Precipitation of L-glutamic acid: Determination of nucleation kinetics. Chem. Eng. Technol. 2006, 29 (2), 257-264.
3. Schöll, J.; Lindenberg, C.; Vicum, L.; Brozio, J.; Mazzotti, M. Precipitation of L-glutamic acid: determination of growth kinetics. Faraday Discuss. 2007, 136, 238-255.
4. Tavare, N. S.; Shah, M. B.; Garside, J. Crystallization and agglomeration kinetics of nickel ammonium-sulfate in an msmpr crystallizer. Powder Technol. 1985, 44 (1), 13-18.
5. Li, T. S.; Livk, I.; Ilievski, D. The influence of crystalliser configuration on the accuracy and precision of gibbsite crystallisation kinetics estimates. Chem. Eng. Sci. 2001, 56 (7), 2511-2519.
6. Wojcik, J. A.; Jones, A. G. Experimental investigation into dynamics and stability of continuous MSMPR agglomerative precipitation of CaCO3 crystals. Chem. Eng. Res. Des. 1997, 75 (A2), 113-118.
7. Collier, A. P.; Hounslow, M. J. Growth and aggregation rates for calcite and calcium oxalate monohydrate. AIChE J. 1999, 45 (11), 2298-2305.
8. David, R.; Marchai, P.; Klein, J. P.; Villermaux, J. Crystallization and precipitation engineering 0.3. A discrete formulation of the agglomeration rate of crystals in a crystallization process. Chem. Eng. Sci. 1991, 46 (1), 205-213.
9. Mumtaz, H. S.; Hounslow, M. J.; Seaton, N. A.; Paterson, W. R. Orthokinetic aggregation during precipitation: A computational model for calcium oxalate monohydrate. Chem. Eng. Res. Des. 1997, 75 (A2), 152-159.
10. Hounslow, M. J.; Mumtaz, H. S.; Collier, A. P.; Barrick, J. P.; Bramley, A. S. A micro-mechanical model for the rate of aggregation during precipitation from solution. Chem. Eng. Sci. 2001, 56 (7), 2543-2552.
11. Ilievski, D.; Livk, I. An agglomeration efficiency model for gibbsite precipitation in a turbulently stirred vessel. Chem. Eng. Sci. 2006, 61 (6), 2010-2022.
12. Baldyga, J.; Jasinska, M.; Orciuch, W. Barium sulphate agglomeration in a pipe - An experimental study and CFD modeling. Chem. Eng. Technol. 2003, 26 (3), 334-340.
13. Ruf, A.; Worlitschek, J.; Mazzotti, M. Modeling and experimental analysis of PSD measurements through FBRM. Part. Part. Syst. Charact. 2000, 17 (4), 167-179.
14. Worlitschek, J.; Mazzotti, M. Choice of the focal point position using lasentec FBRM. Part. Part. Syst. Charact. 2003, 20(1), 12-17.
15. Braun, B. Aggregation and agglomeration in precipitative crystallization. Ph.D. thesis, Technical University of Munich, Germany, 2003.
16. Hulburt, H. M.; Katz, S. Some problems in particle technology - a statistical mechanical formulation. Chem. Eng. Sci. 1964, 19 (8), 555-574.
17. Mersmann, A., Crystallization Technology Handbook. 2nd ed.; Marcel Dekker Inc.: New York, 2001.
18. Saffman, P. G.; Turner, J. S. On the collision of drops in turbulent clouds. J. Fluid Mech. 1956, 1 (1), 16-30.
19. Shamlou, P. A., Processing of solid-liquid suspensions; Butterworth-Heinemann: Oxford, UK, 1993.
20. Kuboi, R.; Komasawa, I.; Otake, T. Collision and coalescence of dispersed drops in turbulent liquid flows. J. Chem. Eng. Jpn. 1972, 5 (4), 423-424.
21. Chesters, A. K. The modeling of coalescence processes in fluid liquid dispersions - a review of current understanding. Chem. Eng. Res. Des. 1991, 69 (4), 259-270.
22. Liew, T. L.; Barrick, J. P.; Hounslow, M. J. A micro-mechanical model for the rate of aggregation during precipitation from solution. Chem. Eng. Technol. 2003, 26 (3), 282-285.
23. Rielly, C. D.; Marquis, A. J. A particle's eye view of crystallizer fluid mechanics. Chem. Eng. Sci. 2001, 56 (7), 2475-2493.
24. Yu, S. Micromixing and parallel reactions. Ph.D. thesis, ETH Zurich, Switzerland, 1993.
25. Laufhütte, D.; Mersmann, A. Local energy-dissipation in turbulent stirring of fluids and its significance for the desing of stirring equipment. Chem. Eng. Tech. 1985, 57 (12), 1104-1105.
26. Kumar, S.; Ramkrishna, D. On the solution of population balance equations by discretization - III. Nucleation, growth and aggregation of particles. Chem. Eng. Sci. 1997, 52 (24), 4659-4679.
27. Schöll, J. Nucleation, growth, and solid phase transformation during precipitation processes. Ph.D. thesis, ETH Zurich, Switzerland, 2006.
28. Scholl, J.; Lindenberg, C.; Vicum, L.; Brozio, J.; Mazzotti, M. Antisolvent precipitation of PDI 747: kinetics of particle formation and growth. Cryst. Growth Des. 2007, 7 (9), 1653-1661.
29. Kashchiev, D.; Verdoes, D.; Vanrosmalen, G. M. Induction time and metastability limit in new phase formation. J. Cryst. Growth 1991, 110 (3), 373-380.
30. Marchisio, D. L.; Soos, M.; Sefcik, J.; Morbidelli, M.; Barresi, A. A.; Baldi, G. Effect of fluid dynamics on particle size distribution in particulate processes. Chem. Eng. Technol. 2006, 29 (2), 191-199.
31. Vicum, L.; Ottiger, S.; Mazzotti, M.; Makowski, L.; Baldyga, J. Multiscale modeling of a reactive mixing process in a semibatch stirred tank. Chem. Eng. Sci. 2004, 59 (8-9), 1767-1781.
32. Kraume, M., Mischen und Rühren, 1st ed.; Wiley-VCH: Weinheim, 2003.
33. Beck, J. V.; Arnold, K. J., Parameter Estimation in Engineering and Science 1st ed.; John Wiley & Sons: New York, 1977.
34. Baldyga, J.; Bourne, J. R., Turbulent Mixing and Chemical Reactions, 1st ed.; John Wiley & Sons Ltd: Chichester, 1999.
35. Marchisio, D. L.; Soos, M.; Sefcik, J.; Morbidelli, M. Role of turbulent shear rate distribution in aggregation and breakage processes. AIChE J. 2006, 52 (1), 158-173.
36. Mumtaz, H. S.; Hounslow, M. J. Aggregation during precipitation from solution: an experimental investigation using Poiseuille flow. Chem. Eng. Sci. 2000, 55 (23), 5671-5681.
37. Ilievski, D. Development and application of a constant supersaturation, semi-batch crystalliser for investigating gibbsite agglomeration. J. Cryst. Growth 2001, 233 (4), 846-862.
38. Ilievski, D.; White, E. T. Agglomeration during Precipitation -Agglomeration Mechanism Identification for Al(Oh)(3) Crystals in Stirred Caustic Alumínate Solutions. Chem. Eng. Sci. 1994, 49 (19), 3227-3239.
39. Bramley, A. S.; Hounslow, M. J.; Ryall, R. L. Aggregation during precipitation from solution: A method for extracting rates from experimental data. J. Colloid Interface Sci. 1996, 183 (1), 155-165.