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Volumn 340, Issue 3, 1988, Pages

Photochemical synthesis and structural characterization of (η5-C5Me5)3Mo3(CO)4(μ2-H)(μ3-O): an unprecedented 46-electron trimolybdenum cluster containing a localized monoprotonated MoMo double bond

(4) Gibson, Charles P a David Rae, A a Tomchick, Diana R a Dahl, Lawrence F a

a UNIVERSITY OF WISCONSIN MADISON (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 3843112216 PISSN: 0022328X EISSN: None Source Type: Journal
DOI: 10.1016/0022-328X(88)80033-0 Document Type: Article

Times cited : (13)

References (36)

1
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- (a) C.P. Gibson, J.A. Mahood, J.-S. Huang, and L.F. Dahl, Abstr. Papers, 187th Nat. Meet. Am. Chem. Soc., St. Louis, MO: American Chemical Society, Washington DC, 1984, INOR 202

2
- 84918157463
- (b) J.A. Mahood, C.P. Gibson, and L.F. Dahl, Abstr. Papers, 190th Nat. Meet. Am. Chem. Soc., Chicago, IL; American Chemical Society, Washington DC, 1985, INOR 77

3
- 84918157462
- (c) C.P. Gibson, B.R. Adams, and L.F. Dahl, Abstr. Papers, 190th Nat. Meet. Am. Chem. Soc., Chicago, IL; American Chemical Society, Washington DC, 1985, INOR 73.

4
- 0001556390
- (1986) Organometallics , vol.5 , pp. 1676
- Gibson¹ Huang² Dahl³

5
- 84918157461
- (a) C.P. Gibson, J.A. Mahood, J.-S. Huang, and L.F. Dahl, Abstr. Papers, 187th Nat. Meet. Am. Chem. Soc., St. Louis, MO: American Chemical Society, Washington DC, 1984, INOR 202

6
- 84918157460
- (b) J.A. Mahood, C.P. Gibson, and L.F. Dahl, Abstr. Papers, 190th Nat. Meet. Am. Chem. Soc., Chicago, IL; American Chemical Society, Washington DC, 1985, INOR 77

7
- 84918157459
- (c) C.P. Gibson, B.R. Adams, and L.F. Dahl, Abstr. Papers, 190th Nat. Meet. Am. Chem. Soc., Chicago, IL; American Chemical Society, Washington DC, 1985, INOR 73.

8
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- C.P. Gibson and L.F. Dahl, Organometallics, in press.

9
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11
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12
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- King¹ Eqbal² King³

13
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- (1983) J. Organomet. Chem. , vol.342 , pp. 57
- Huang¹ Dahl²

14
- 84918157457
- 2O (which also is the likely source of the bridging hydrogen atom) have been implicated as sources of triply bridging oxygen atoms in other oxo-capped triangular molybdenum-based mixed-metal clusters [1,2,10].

15
- 84872140994
- University of Wisconsin-Madison
- (1986) Ph.D. Thesis
- Mahood¹

16
- 84918157456
- 3 molecule and a centrosymmetrically disordered THF molecule) was determined from an interpretation of a Patterson map followed by successive Fourier and [[Truncated]]

17
- 84917823052
- University of New South Wales, Kensington, adapted for a Harris/7 computer by A.D. Rae, University of Wisconsin-Madison, 1983.
- (1976) RAELS, A Comprehensive Least-Squares Program
- Rae¹

18
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- Rigid-body motion in crystals – the application of constraints on the TLS model
- (1975) Acta Crystallographica Section A: Crystal Physics, Diffraction, Theoretical and General Crystallography , vol.31 , pp. 570
- Rae¹

19
- 84918157455
- Evidence for the existence of these π-acceptor semibridging carbonyl ligands is given by: (1) abnormally small Mo(2)C(2)O(2) and Mo(2)C(4)O(4) bond angles of 157.6(5) and 158.6(6)°, respectively; (2) the sharply acute Mo(1)Mo(2)C(2) and Mo(3)Mo(2)C(4) bond angles of 58.9(2) and 59.6(2)°, respectively; and (3) the relatively short carbonyl carbon distance to the second metal atom of 2.535(7) Å for the C(2) … Mo(1) interaction and 2.559(7) Å for the C(4) … Mo(3) interaction. These values are entirely consistent with the structural data recently tabulated by Crabtree and Lavin [15] in their detailed analysis of the bent semibridging carbonyl ligand.

20
- 33845374774
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- Crabtree¹ Lavin²

21
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- L.F. Dahl, Stereochemical Analysis of Various Transition Metal Hydride Clusters and Resulting Bonding Implications, in Annals of the New York Academy of Science on Catalytic Transition Metal Hydrides, Jan. 1984, pp. 1–26, and refs. cited therein.

22
- 84918157453
- 5 ligands that are bound to the mirror-related and unique Mo atoms, respectively; the latter high-field resonance is readily attributed to a molybdenum-bound hydride ligand [18,19].

23
- 84918157452
- 3 displayed a high-field doublet for the hydrido atom at [[Truncated]]

24
- 33947479598
- 2) (Synthesis)
- (1963) Inorg. Chem. , vol.2 , pp. 1031
- Hayter¹

25
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- (X-Ray photographic study)
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26
- 0010811366
- Neutron diffraction studies of the metal-hydrogen-metal bond. I. Symmetric, bent, three-center, two-electron molybdenum-hydrogen-molybdenum bond in .mu.-hydrido-.mu.-dimethylphosphido-bis(.eta.5-cyclopentadienyldicarbonylmolybdenum)
- (Neutron diffraction study)
- (1974) Journal of the American Chemical Society , vol.96 , pp. 6610
- Petersen¹ Dahl² Williams³

27
- 26744439179
- (X-ray diffractometry study)
- (1978) Inorg. Chem. , vol.17 , pp. 1308
- Petersen¹ Willilams²

28
- 0000866838
- −, Synthesis and X-ray diffractometry study)
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- Petersen¹ Stewart²

29
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- Indirect location of hydride ligands in metal cluster complexes
- (1980) Journal of the Chemical Society, Dalton Transactions , pp. 2509
- Orpen¹

30
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- C.P. Gibson and L.F. Dahl, Organometallics, in press.

31
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- (1976) Inorg. Chem. , vol.15 , pp. 1843
- Churchill¹ DeBoer² Rotella³

32
- 0000853619
- Crystallographic studies of transition metal hydride complexes
- and refs. cited therein.
- (1981) Struct. Bonding , vol.4 , pp. 1
- Teller¹ Bau²

33
- 84918157450
- 3-O) core (which has a MoMo distance of 2.916(1) Å and two ReMo distances of 2.913(1) and 3.010(1) Å) is attributed to a [[Truncated]]

34
- 84918157449
- 2Re molecule and a centrosymmetrically ordered one-half hexane molecule were located from a Patterson map (which gave initial metal coordinates) and subsequent Fourier and difference maps. Least-squares refinement (RAELS [12]) with 238 variables converged [[Truncated]]

35
- 0003625966
- G. Wilkinson, F.G.A. Stone, E.W. Abel, Pergamon Press, New York
- (1982) Comprehensive Organometallic Chemistry , pp. 1425-1520
- Bruce¹

36
- 0040731271
- (1976) J. Organomet. Chem. , vol.113 , pp. C61
- Bertolucci¹ Freni² Romiti³ Ciani⁴ Sironi⁵ Albano⁶

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