Determination of optical impurity of pregabalin by HPLC with pre-column chiral derivatization

Journal of Chromatographic Science

Volumn 46, Issue 1, 2008, Pages 42-44

  Chen, Xiaohui ^a   Zhang, Daolin ^b   Deng, Jie ^b   Fu, Xiaotai ^b  

^a CHINA UNIVERSITY OF GEOSCIENCES   (China)

^b Chongqing Pharmaceutical Research Institute Co Ltd   (China)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 38149112749     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/46.1.42     Document Type: Article

References (14)

1. R.H. Dworkin, A.E. Corbin, J.P. Young, Jr, and U. Sharma. Pregabalin for the treatment of postherpetic neuralgia. American Academy of Neurology 60(8): 1274-1283 (2003).
2. Z. Li, Y. Tong-Wei, and Z. Su. Pharmacokinetics of chiral drug. Chinese Journal of Modern Applied Pharmacy 16(2): 4-7 (1999).
3. L. Wei-Zao, L. Wan-Zhang, and Z. Zhi-Rong. Advances in chromatographic separation of chiral drugs. West Chinese Journal of Pharmaceutical Science 15(4): 295-298 (2000).
4. M. Jian-Yin. Chromatographic Separation of Chiral Drugs. Chinese Journal of Pharmaceuticals 33(4): 199-202 (2002).
5. B.L. Windsor and L.L. Radulovic. Measurement of a new anticonvulsant, (S)-3-(aminomethyl)-5-methylhexanoic acid, in plasma and milk by High Performance Liquid Chromatography. J. Chromatogr. B 674(2): 143-148 (1995).
6. T.A.C. Vermeij and P.M. Edelbroek. Simultaneous high-performance liquid chromatographic analyses of pregabalin, gabapentin and vigabatrin in human serum by precolumn derivatization with o-phtaldialdehyde and fluorescence detection. J. Chromatogr. B 810(2): 297-303 (2004).
7. W.H. Pirkle and T.C. Pochasky. Considerations of chiral relevant to the liquid chromatographic separation of enantiomers. Chem. Rev. 89(2): 347-362 (1989).
8. N. Oi and H. Kithara. High-performance liquid chromatographic separation of amino acid enantiomers on urea derivatives of L-valine bonded to silica gel. J. Chromatogr. A 285(1): 198-202 (1984).
9. W. Ying and H. Tai-jun. Enantiospecific Analysis of Fudosteine by RP-HPLC with Chiral Precolumn Derivatization. Progress in Pharmaceutical Sciences 29(1): 422-424 (2005).
10. W. Shao-hui, Y. Hao, and G. Xiu-mei. Determination of Amino Acids in Isatis indigotica Fort by Reversed-Phase High Performance Liquid Chromatography with Pre-column Derivatization. Chinese J. Chromatogr. 23(4): 408-410 (2005).
11. M. Calull, J. Fabregas, R.M. Marcé, and F. Borrull. Determination of free amino acids by precolumn derivatization with phenylisothiocyanate. Application to wine samples. Chromatographia 31(5-6): 272-276 (1991).
12. R.A. Bank, E.J. Jansen, B. Beekman, and J.M. Koppele. Amino acid analysis by reverse-phase high-performance liquid chromatography: improved derivatization and detection conditions with 9-fluorenylmethyl chloroformate. Anal Biochem. 240(1): 167-176 (1996).
13. W. Ji and Z. Xiang-You. Determination of the content of amino acid by pre-column derivatization and RP-HPLC. Journal of Shenyang Pharmaceutical 20(6): 428-429 (2003).
14. Y. Dong-Hui. Determination of 2,3,5,4′-tetrahydroxystilbene 2-O-β-D glucoside in Polygonum mutiflorum Thunb. and Fu Fang Chong Cao capsule by HPLC Journal of Beijing Medical University 32(3): 280-282 (2000).