Quantitation of trace betamethasone or dexamethasone in dexamethasone or betamethasone active pharmaceutical ingredients by reversed-phase high-performance liquid chromatography

Journal of Chromatographic Science

Volumn 46, Issue 1, 2008, Pages 15-22

  Kang, Ping Xiao ^a   Xiong, Yuan ^a   Rustum, Abu M ^a  

^a MERCK RESEARCH LABORATORIES   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 38149085331     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/46.1.15     Document Type: Article

References (25)

1. Goodman & Gilman's The Pharmacological Basis of Therapy, 11th ed. L. Brunton, J. Lazo, and K. Parker, Eds. McGraw-Hill, New York, 2005, pp. 1593-1612.
2. Principles of Medical Pharmacology, H. Kalant, 7th ed. D.M. Grant, J. and Mitchell, Eds. Saunders-Elsevier Canada, Toronto, 2007, pp. 647-657
3. Lippincott's Illustrated Reviews, Pharmacology. R.D. Howland and M.J. Mycek, Eds. Lippincott Williams & Wilkins, Baltimore, MD, 2006, pp. 307-314.
4. A.H. Jobe and R. F. Soll. Choice and dose of corticosteroid for antenatal treatments. Am. J. Obstet. Gynecol. 190: 878-881 (2004).
5. A.H. Jobe. Postnatal corticosteroids for preterm infants - do what we say, not what we do. N. Engl. J. Med. 350: 1351-1351 (2004).
6. A. Whitelaw and M. Thoresen. Antenatal steroids and the developing brain. Arch. Dis. Child. Fetal Neonatal Ed. 83: F154-F157 (2000).
7. A. dos S. Pereira, L.S.O.B. Oliveira, G. D. Mendes, J.J. Gabbai, and G. De Nucci. Quantification of betamethasone in human plasma by liquid chromatography-tandem mass spectrometry using atmospheric pressure photoionization in negative mode. J. Chromatogr. B 828: 27-32 (2005).
8. K.E. Arthur, J-C. Wolff, and D.J. Carrier. Analysis of betamethasone, dexamethasone and related compounds by liquid chromatography-electrospray mass spectrometry. Rapid Commun. Mass Spectrom. 18: 678-684 (2004).
9. K. De Wasch, H.F. De Brabander, M. Van de Wiele, J. Vercammen, D. Courtheyn, and S. Impens. Differentiation between dexamethasone and betamethasone in a mixture using multiple mass spectrometry. J. Chromatogr. A 926: 79-86 (2001).
10. S.-M. Wu, S.-H. Chen, and H.-L. Wu. Determination of betamethasone and dexamethasone by derivatization and liquid chromatography. Anal. Chim. Acta. 268: 255-260 (1992).
11. N.W. Tymes. The determination of corticoids and related steroid analogs by high-performance liquid chromatography. J. Chromatog. Sci. 15: 151-155 (1977).
12. J.C. Caron and B. Shroot. Determination of partition coefficients of glucocorticosteroids by high-performance liquid chromatography. J. Pharm. Sci. 73: 1703-1706 (1984).
13. L.R. Snyder, J.J. Kirkland and J.L. Glajch. Practical HPLC Method Development, 2nd ed. John Wiley & Sons, New York, NY, 1997, pp. 21-58.
14. E.F. Hewitt, P. Lukulay, and S. Galushko. Implementation of a rapid and automated high performance liquid chromatography method development strategy for pharmaceutical drug candidates. J. Chromatogr. A 1107: 79-87 (2006).
15. I. Molnar. Computerized design of separation strategies by reversed-phase liquid chromatography: development of DryLab software. J. Chromatogr. A 965: 175-194 (2002).
16. J. García-Lavandeiraa, J.A. Martínez-Pontevedraa, M. Loresa, and R. Cela. Computer-assisted transfer of programmed elutions in reversed-phase high-performance liquid chromatography. J. Chromatogr. A 1128: 17-26 (2006).
17. L.R. Snyder and J.W. Dolan, Reversed-phase separation of a chiral isomers by varying temperature and either gradient time or solvent strength. J. Chromatogr. A 892: 107-121 (2000).
18. A. Santos-Montes, A.I. Gasco-Lopez, and R. Izquierdo-Hornillos. Optimization of the high-performance liquid chromatographic separation of a mixture of natural and synthetic corticosteroids. J. Chromatogr. B 620: 15-23 (1993).
19. M.R. Euerby, A.P. McKeown, and P. Petersson. Chromatographic classification and comparison of commercially available perfluorinated stationary phases for reversed-phase liquid chromatography using principal component analysis. J. Sep. Sci. 23: 295-306 (2003).
20. T. Cserhati and E. Forgacs. Effect of β-cyclodextrin derivatives on the retention of steroidal drugs. J. Chromatogr. B 681: 205-211 (1996).
21. P.K. Zarzycki, K.M. Kulhanek, and R. Smith. Chromatographic behaviour of selected steroids and their inclusion complexes with β-cyclodextrin on octadecylsilica stationary phases with different carbon loads. J Chromatogr. A 955: 71-78 (2002).
22. P.K. Zarzycki and R. Smith. Separation of steroids using temperature-dependent inclusion chromatography. J Chromatogr. A 912: 45-52 (2001).
23. K.G. Flood, E.R. Reynolds, and N.H. Snow. Characterization of inclusion complexes of betamethasone-related steroids with cyclodextrins using high-performance liquid chromatography. J. Chromatogr. A 903: 49-65 (2000).
24. J.C. Reeepmeyer. Separation of R- and S-thalidomide by reversed-phase HPLC with β-cyclodextrin in the mobile phase. Chirality. 8: 11-17 (1996).
25. P.K. Zarzycki, E. Wlodarczyk, D-W. Lou, and K. Jinno. Evaluation of methanol-water and acetonitrile-water binary mixtures as eluents for temperature-dependent inclusion chromatography. Anal. Sci. 22: 453-456 (2006).