Recovery of acetic acid by reactive distillation: Parametric study and nonlinear dynamic effects

Industrial and Engineering Chemistry Research

Volumn 46, Issue 26, 2007, Pages 9196-9204

  Singh, Ajay ^a   Tiwari, Anand ^a   Bansal, Vineet ^a   Gudi, Ravindra D ^a   Mahajani, Sanjay M ^a  

^a INDIAN INSTITUTE OF TECHNOLOGY BOMBAY   (India)

Author keywords

[No Author keywords available]

Indexed keywords

DISTILLATION COLUMNS; MATHEMATICAL MODELS; PARAMETER ESTIMATION; SOLUTIONS;

PARAMETER CONTINUATION METHOD; REACTIVE DISTILLATION; REBOIL RATIO;

ACETIC ACID;

ACETIC ACID; DISTILLATION COLUMNS; MATHEMATICAL MODELS; PARAMETER ESTIMATION; SOLUTIONS;

EID: 38149039397     PISSN: 08885885     EISSN: None     Source Type: Journal    
DOI: 10.1021/ie071070i     Document Type: Conference Paper

References (26)

1. Neumann, R.; Sasoon, Y. Recovery of dilute acetic acid by esterification in a packed chemorectification column. Ind. Eng. Chem. Process Des. Dev. 1984, 23 (4), 654-659.
2. Xu, Z.; Afacan, A.; Chuang, K. T. Removal of Acetic Acid from Water by Catalytic Distillation. Part 1 : Experimental Studies. Can. J. Chem. Eng. 1990, 77, 676-681.
3. Scates, M. O.; Parker, S. E.; Lacy, J. B.; Gibbs, R. K. Recovery of acetic acid from dilute aqueous streams formed during a carbonylation process. U.S. Patent 5,599,976, 1997.
4. Tang, Y. T.; Hung, S. B.; Chen, Y. W.; Huang, H. P.; Lee, M. J.; Yu, C. C. Design of Reactive Distillations for Acetic Acid Esterification with Different Alcohols. AIChE J. 2005, 51, 1683-1699.
5. Hung, W.; Lai, I.; Chen, Y. W.; Hung, S. B.; Huang, H. B.; Lee, M. J.; Yu, C. C. Process Chemistry and Design Alternatives for Converting Dilute Acetic Acid to Esters in Reactive Distillation. Ind. Eng. Chem. Res. 2005, 45, 1722.
6. Singh, A., A.; Tiwari, A. A.; Mahajani, S. M.; Gudi, R. D. Recovery of Acetic acid from Aqueous Solutions by Reactive Distillation. Ind. Eng. Chem. Res. 2006, 45 (6), 2017-2025.
7. Agreda, V. H.; Partiu, L. R.; Heise, W. H. High Purity Methyl Acetate via Reactive Distillation. Chem. Eng. Prog. 1990, 40, 40-46.
8. Kienle, A.; Marquadt, W. Non-linear Dynamics of Reactive Distillation In Reactive Distillation: Status and Future Directions; Sundmacher, K., Kienle, A. Eds.; Wiley-VCH: Weinheim, Germany, 2003.
9. Jacobs, R.; Krishna, R. Multiple Solutions in Reactive Distillation for Methyl tert-Butyl Ether Synthesis. Ind. Eng. Chem. Res. 1993, 32, 1706.
10. Nijhuis, S. A.; Kerkhof, F. P. J. M.; Mak. A. N. S. Multiple steady states during reactive distillation of methyl tert-butyl ether. Ind. Eng. Chem. Res. 1993, 32 (11), 2767-2774.
11. Guttinger, T. E.; Morari, M. Predicting Multiple Steady States in Distillation: Singularity Analysis and Reactive Systems. Comput. Chem. Eng. 1997, 21, S995-S1000.
12. Sneesby. M. G.; Tade, M. O.; Smith, T. N. Steady-state Transitions in the Reactive Distillation of MTBE. Comput. Chem. Eng. 1998, 22, 879-892.
13. Mohl, K. D.; Kienle, A.; Gilles. E. D. Multiple Steady States in a Reactive Distillation Column for the Production of TAME I. Theoretical Analysis. Chem. Eng. Technol. 1998, 21 (2), 133-136.
14. Mohl, K. D.; Kienle, A.; Gilles. E. D.; Rapmund, P.; Sundmacher, K.; Hoffmann, U. Nonlinear Dynamics of Reactive Distillation Processes for the Production of Fuel Ethers. Comput. Chem. Eng. 1997, 21, 989-994.
15. Mohl, K. D.; Kienle, A.; Gilles, E. D.; Rapmund, P.; Sundmacher, K.; Hoffmann, U. Steady-state Multiplicities in Reactive Distillation Columns for the Production of Fuel Ethers MTBE and TAME: Theoretical Analysis and Experimental Verification. Chem. Eng. Sci. 1999, 54 (8), 1029-1043.
16. Baur, R. R.; Higler. A. P.; Taylor. R.; Krishna, R. Comparison of Equilibrium Stage and Nonequilibrium Stage Models for Reactive Distillation. Chem. Eng. J. 1999, 76, 3347.
17. Sundmacher, K.; Hoffmann, U. Multicomponent Mass and Energy Transport on Different Length Scales in a Packed Reactive Distillation Column for Heterogeneously Catalysed Fuel Ether Production. Chem. Eng. Sci. 1999, 49 (24A), 4443-4464.
18. Chen, F.; Huss, R. S.; Malone, M. F.; Doherty, M. F. Multiple Steady States in Reactive Distillation: Kinetic Effects. Comput. Chem. Eng. 2002, 26 (1), 81-93.
19. Katariya, A. M.; Moudgalya, K. M.; Mahajani, S. M. Nonlinear Dynamic Effects in Reactive Distillation for Synthesis of TAME. Ind. Eng. Chem. Res. 2006, 45 (12), 4233-4242.
20. Gehrke, V.; Marquardt, W. A. Singularity Theory Approach to the Study of Reactive Distillation. Comput. Chem. Eng. 2005, 21, S1001-S1006.
21. Kumar, A.; Daoutidies, P. Modelling, Analysis and Control of Ethylene Glycol Reactive Distillation Column. AIChE J. 1999, 45 (1), 51-68.
22. Huss, S. R.; Chen, M. F.; Doherty, M. F.; Malone, M. F. Reactive Distillation for Methyl Acetate Production. Comput. Chem. Eng. 2003, 27 (12), 1855-1866.
23. Doherty. M. F.; Malone, M. F. Conceptual Design of Distillation Systems; McGraw-Hill: New York, 2001.
24. Pöpken, T.; Gotze, L.; Gmehling, J. Reaction Kinetics and Chemical Equilibrium of Homogeneously and Heterogeneously Catalyzed Acetic Acid Esterification with Methanol and Methyl Acetate Hydrolysis. Ind. Eng. Chem. Res. 2000, 39 (7), 2601-2611.
25. Song, W.; Venimadhavan, G.; Manning, J. M.; Malone, M. F.; Doherty, M. F. Measurement of Residue Curve Maps and Heterogeneous Kinetics in Methyl Acetate Synthesis. Ind. Eng. Chem. Res. 1998, 37 (5), 1917-1928.
26. Barbosa, D.; Doherty, M. F. The Simple Distillation of Homogeneous Reactive Mixtures. Chem. Eng. Sci. 1988, 43 (3), 541-550.