메뉴 건너뛰기




Volumn 190, Issue 2, 2008, Pages 280-291

Cryogenic Q-band (35 GHz) probehead featuring large excitation microwave fields for pulse and continuous wave electron paramagnetic resonance spectroscopy: Performance and applications

Author keywords

DQ EPR; EPR; Hyperfine decoupling; HYSCORE; Loop gap resonator; Q band probehead

Indexed keywords

ANGLE MEASUREMENT; ELECTRON SPIN RESONANCE SPECTROSCOPY; MAGNETIC FIELD EFFECTS; MICROWAVES; PARAMAGNETIC RESONANCE; SENSITIVITY ANALYSIS;

EID: 38149039368     PISSN: 10907807     EISSN: 10960856     Source Type: Journal    
DOI: 10.1016/j.jmr.2007.11.009     Document Type: Article
Times cited : (17)

References (55)
  • 1
    • 0035742337 scopus 로고    scopus 로고
    • A Q-band pulse EPR/ENDOR spectrometer and the implementation of advanced one- and two-dimensional pulse EPR methodology
    • Gromov I., Shane J., Forrer J., Rakhmatoullin R., Rozentzwaig Y., and Schweiger A. A Q-band pulse EPR/ENDOR spectrometer and the implementation of advanced one- and two-dimensional pulse EPR methodology. J. Magn. Reson. 149 2 (2001) 196-203
    • (2001) J. Magn. Reson. , vol.149 , Issue.2 , pp. 196-203
    • Gromov, I.1    Shane, J.2    Forrer, J.3    Rakhmatoullin, R.4    Rozentzwaig, Y.5    Schweiger, A.6
  • 2
    • 38149089442 scopus 로고    scopus 로고
    • P. Höfer, R. Heilig, D.C. Maier, I. Prisecaru, D. Schmalbein, The super Q-FT accessory for pulsed EPR, ENDOR and ELDOR at 34 GHz, Bruker Spin Report 152/153 (2003) 37-43.
  • 3
    • 33747609104 scopus 로고    scopus 로고
    • 26.5-40 GHz Ka-Band Pulsed EPR Spectrometer, Concepts in Magnetic Resonance Part B
    • Astashkin A.V., Enemark J.H., and Raitsimring A. 26.5-40 GHz Ka-Band Pulsed EPR Spectrometer, Concepts in Magnetic Resonance Part B. Mag. Res. Eng. 29B (2006) 125-136
    • (2006) Mag. Res. Eng. , vol.29 B , pp. 125-136
    • Astashkin, A.V.1    Enemark, J.H.2    Raitsimring, A.3
  • 4
    • 0002826498 scopus 로고    scopus 로고
    • Q-band pulsed electron spin-echo spectrometer and its application to ENDOR and ESEEM
    • Davoust C.E., Doan P.E., and Hoffman B.M. Q-band pulsed electron spin-echo spectrometer and its application to ENDOR and ESEEM. J. Magn. Reson. A 119 (1996) 38-44
    • (1996) J. Magn. Reson. A , vol.119 , pp. 38-44
    • Davoust, C.E.1    Doan, P.E.2    Hoffman, B.M.3
  • 8
    • 0001613255 scopus 로고
    • Bridged loop gap resonator a resonant structure for pulsed electron-spin-resonance transparent to high-frequency radiation
    • Pfenninger S., Forrer J., Schweiger A., and Weiland T. Bridged loop gap resonator a resonant structure for pulsed electron-spin-resonance transparent to high-frequency radiation. Rev. Sci. Instrum. 59 (1988) 752-760
    • (1988) Rev. Sci. Instrum. , vol.59 , pp. 752-760
    • Pfenninger, S.1    Forrer, J.2    Schweiger, A.3    Weiland, T.4
  • 9
    • 0000044566 scopus 로고
    • Echo-induced ESR spectroscopy with magnetic field vector jumps: a novel approach to improve the spectral resolution in disordered systems
    • Pfenninger S., Schweiger A., Forrer J., and Ernst R.R. Echo-induced ESR spectroscopy with magnetic field vector jumps: a novel approach to improve the spectral resolution in disordered systems. Chem. Phys. Lett. 154 (1989) 199-204
    • (1989) Chem. Phys. Lett. , vol.154 , pp. 199-204
    • Pfenninger, S.1    Schweiger, A.2    Forrer, J.3    Ernst, R.R.4
  • 10
    • 0011656957 scopus 로고
    • Fourier transform hyperfine spectroscopy
    • Wacker Th., and Schweiger A. Fourier transform hyperfine spectroscopy. Chem. Phys. Lett. 191 (1992) 136-141
    • (1992) Chem. Phys. Lett. , vol.191 , pp. 136-141
    • Wacker, Th.1    Schweiger, A.2
  • 11
    • 19044376526 scopus 로고    scopus 로고
    • Probeheads and instrumentation for pulse EPR and ENDOR spectroscopy with chirped radio frequency pulses and magnetic field steps
    • Forrer J., Pfenninger S., Sierra G., Jeschke G., Schweiger A., Wagner B., and Weiland Th. Probeheads and instrumentation for pulse EPR and ENDOR spectroscopy with chirped radio frequency pulses and magnetic field steps. Appl. Magn. Reson. 10 (1996) 263-279
    • (1996) Appl. Magn. Reson. , vol.10 , pp. 263-279
    • Forrer, J.1    Pfenninger, S.2    Sierra, G.3    Jeschke, G.4    Schweiger, A.5    Wagner, B.6    Weiland, Th.7
  • 12
    • 0032110456 scopus 로고    scopus 로고
    • Two-dimensional nuclear-Zeeman-resolved electron spin echo envelope modulation (NZ-ESEEM) spectroscopy
    • Willer M., Granwehr J., Forrer J., and Schweiger A. Two-dimensional nuclear-Zeeman-resolved electron spin echo envelope modulation (NZ-ESEEM) spectroscopy. J. Magn. Reson. 133 (1998) 46-52
    • (1998) J. Magn. Reson. , vol.133 , pp. 46-52
    • Willer, M.1    Granwehr, J.2    Forrer, J.3    Schweiger, A.4
  • 13
    • 19044378322 scopus 로고
    • Versatile applications of the bridged loop-gap resonator
    • Pfenninger S., Forrer J., Schweiger A., and Weiland Th. Versatile applications of the bridged loop-gap resonator. Phys. Med. 2-4 (1989) 203-212
    • (1989) Phys. Med. , vol.2-4 , pp. 203-212
    • Pfenninger, S.1    Forrer, J.2    Schweiger, A.3    Weiland, Th.4
  • 14
    • 0000322221 scopus 로고
    • Pulsed electron-nuclear double resonance methodology
    • Gemperle C., and Schweiger A. Pulsed electron-nuclear double resonance methodology. Chem. Rev. 91 (1991) 1481-1501
    • (1991) Chem. Rev. , vol.91 , pp. 1481-1501
    • Gemperle, C.1    Schweiger, A.2
  • 15
    • 0001112565 scopus 로고
    • A pulsed ENDOR probehead with the bridged loop-gap resonator-construction and performance
    • Forrer J., Pfenninger S., and Schweiger A. A pulsed ENDOR probehead with the bridged loop-gap resonator-construction and performance. Rev. Sci. Instrum. 61 (1990) 3360-3367
    • (1990) Rev. Sci. Instrum. , vol.61 , pp. 3360-3367
    • Forrer, J.1    Pfenninger, S.2    Schweiger, A.3
  • 16
    • 0009580275 scopus 로고
    • Progress in instrumentation for pulsed EPR and ENDOR spectroscopy
    • Forrer J., Pfenninger S., Wagner B., and Weiland Th. Progress in instrumentation for pulsed EPR and ENDOR spectroscopy. Pure Appl. Chem. 64 (1992) 865-872
    • (1992) Pure Appl. Chem. , vol.64 , pp. 865-872
    • Forrer, J.1    Pfenninger, S.2    Wagner, B.3    Weiland, Th.4
  • 17
    • 0347595540 scopus 로고
    • Time-domain chirp electron nuclear double-resonance spectroscopy in one and two dimensions
    • Jeschke G., and Schweiger A. Time-domain chirp electron nuclear double-resonance spectroscopy in one and two dimensions. J. Chem. Phys. 103 (1995) 8329-8337
    • (1995) J. Chem. Phys. , vol.103 , pp. 8329-8337
    • Jeschke, G.1    Schweiger, A.2
  • 19
    • 0007759035 scopus 로고
    • Radio-frequency driven electron-spin-echo envelope modulation spectroscopy
    • Cho H., Pfenninger S., Forrer J., and Schweiger A. Radio-frequency driven electron-spin-echo envelope modulation spectroscopy. Chem. Phys. Lett. 180 (1991) 198-206
    • (1991) Chem. Phys. Lett. , vol.180 , pp. 198-206
    • Cho, H.1    Pfenninger, S.2    Forrer, J.3    Schweiger, A.4
  • 20
    • 84950548801 scopus 로고
    • Puls ESR spektrometer mit loop-gap-resonator bull
    • Forrer J. Puls ESR spektrometer mit loop-gap-resonator bull. ASE/UCS 75 (1984) 1264
    • (1984) ASE/UCS , vol.75 , pp. 1264
    • Forrer, J.1
  • 22
    • 3142672733 scopus 로고
    • The loop-gap resonator. 2. Controlled return flux 3-loop, 2-gap microwave resonators for ENDOR and electron-spin-resonance spectroscopy
    • Wood R., Froncisz W., and Hyde J. The loop-gap resonator. 2. Controlled return flux 3-loop, 2-gap microwave resonators for ENDOR and electron-spin-resonance spectroscopy. J. Magn. Reson. 58 (1984) 243-253
    • (1984) J. Magn. Reson. , vol.58 , pp. 243-253
    • Wood, R.1    Froncisz, W.2    Hyde, J.3
  • 24
    • 38149037089 scopus 로고    scopus 로고
    • R. Biehl, The dielectric ring TE011 cavity, Bruker Report 1 (1986) 45.
  • 25
    • 38149113951 scopus 로고
    • Bridged-loop-gap and dielectric resonators for pulsed ESR and ENDOR spectroscopy with light excitation
    • Elsevier
    • Forrer J., Pfenninger S., Schweiger A., and Weiland Th. Bridged-loop-gap and dielectric resonators for pulsed ESR and ENDOR spectroscopy with light excitation. Magnetic Resonance and Related Phenomena vol. 219 (1989), Elsevier 919-924
    • (1989) Magnetic Resonance and Related Phenomena , vol.219 , pp. 919-924
    • Forrer, J.1    Pfenninger, S.2    Schweiger, A.3    Weiland, Th.4
  • 26
    • 38149135685 scopus 로고    scopus 로고
    • A.D. Blumlein, High frequency electrical conductor or radiator, US Patent No. 2 238 770 (April 15 1941).
  • 28
    • 34249036549 scopus 로고    scopus 로고
    • Uniform radio frequency fields in loop-gap resonators for EPR spectroscopy
    • Mett R.R., Sidabras J.W., and Hyde J.S. Uniform radio frequency fields in loop-gap resonators for EPR spectroscopy. Appl. Magn. Reson. 31 (2007) 573-589
    • (2007) Appl. Magn. Reson. , vol.31 , pp. 573-589
    • Mett, R.R.1    Sidabras, J.W.2    Hyde, J.S.3
  • 29
    • 0037205190 scopus 로고    scopus 로고
    • Polarization-transfer electron-Zeeman resolved EPR
    • Eichel R., and Schweiger A. Polarization-transfer electron-Zeeman resolved EPR. Chem. Phys. Lett. 358 (2002) 271-277
    • (2002) Chem. Phys. Lett. , vol.358 , pp. 271-277
    • Eichel, R.1    Schweiger, A.2
  • 30
    • 0035935964 scopus 로고    scopus 로고
    • Right-angle wiggling electron paramagnetic resonance spectroscopy
    • Eichel R., and Schweiger A. Right-angle wiggling electron paramagnetic resonance spectroscopy. J. Chem. Phys. 115 (2001) 9126-9135
    • (2001) J. Chem. Phys. , vol.115 , pp. 9126-9135
    • Eichel, R.1    Schweiger, A.2
  • 31
    • 0035743683 scopus 로고    scopus 로고
    • Longitudinally detected EPR-improved instrumentation and new pulse schemes
    • Granwehr J., Forrer J., and Schweiger A. Longitudinally detected EPR-improved instrumentation and new pulse schemes. J. Magn. Reson. 151 (2001) 78-84
    • (2001) J. Magn. Reson. , vol.151 , pp. 78-84
    • Granwehr, J.1    Forrer, J.2    Schweiger, A.3
  • 32
    • 33745714237 scopus 로고    scopus 로고
    • Design of Q-band loop-gap resonators at frequencies of 34-36 GHz for single electron spin spectroscopy in semiconductor nanostructures
    • Art. No. 064702.
    • Simovic B., Studerus P., Gustavsson S., Leturcq R., Ensslin K., Schuhmann R., Forrer J., and Schweiger A. Design of Q-band loop-gap resonators at frequencies of 34-36 GHz for single electron spin spectroscopy in semiconductor nanostructures. Rev. Sci. Instrum. 77 (2006) Art. No. 064702.
    • (2006) Rev. Sci. Instrum. , vol.77
    • Simovic, B.1    Studerus, P.2    Gustavsson, S.3    Leturcq, R.4    Ensslin, K.5    Schuhmann, R.6    Forrer, J.7    Schweiger, A.8
  • 33
    • 0001312847 scopus 로고
    • Coherent and incoherent echo spectroscopy with extended-time excitation
    • Schweiger A., Braunschweiler L., Fauth J.M., and Ernst R.R. Coherent and incoherent echo spectroscopy with extended-time excitation. Phys. Rev. Lett. 54 (1985) 1241-1244
    • (1985) Phys. Rev. Lett. , vol.54 , pp. 1241-1244
    • Schweiger, A.1    Braunschweiler, L.2    Fauth, J.M.3    Ernst, R.R.4
  • 34
    • 0002214132 scopus 로고
    • Elimination of unwanted echoes and reduction of dead time in 3-pulse electron spin-echo spectroscopy
    • Fauth J.M., Schweiger A., Braunschweiler L., Forrer J., and Ernst R.R. Elimination of unwanted echoes and reduction of dead time in 3-pulse electron spin-echo spectroscopy. J. Magn. Reson. 66 (1986) 74-85
    • (1986) J. Magn. Reson. , vol.66 , pp. 74-85
    • Fauth, J.M.1    Schweiger, A.2    Braunschweiler, L.3    Forrer, J.4    Ernst, R.R.5
  • 35
    • 38149135684 scopus 로고    scopus 로고
    • L. Braunschweiler, Elektronenspinecho-Spektroskopie mit Langzeit-Anregung, Diss. ETH No. 7887.
  • 36
    • 33745700182 scopus 로고    scopus 로고
    • Probehead operating at 35 GHz for continuous wave and pulse electron paramagnetic resonance applications
    • Art. No. 064704.
    • Gromov I., Forrer J., and Schweiger A. Probehead operating at 35 GHz for continuous wave and pulse electron paramagnetic resonance applications. Rev. Sci. Instrum. 77 (2006) Art. No. 064704.
    • (2006) Rev. Sci. Instrum. , vol.77
    • Gromov, I.1    Forrer, J.2    Schweiger, A.3
  • 37
    • 38149004749 scopus 로고    scopus 로고
    • Angst und Pfister, CH-8600, Dübendorf, Switzerland.
  • 38
    • 38149044855 scopus 로고    scopus 로고
    • Collini-Flühmann AG 8600, Dübendorf, Switzerland.
  • 39
    • 0001645454 scopus 로고    scopus 로고
    • S-band (2-4 GHz) pulse electron paramagnetic resonance spectrometer: construction, probe head design, and performance
    • Willer M., Forrer J., Keller J., Van Doorslaer S., Schweiger A., Schuhmann R., and Weiland T. S-band (2-4 GHz) pulse electron paramagnetic resonance spectrometer: construction, probe head design, and performance. Rev. Sci. Instrum. 71 (2000) 2807-2817
    • (2000) Rev. Sci. Instrum. , vol.71 , pp. 2807-2817
    • Willer, M.1    Forrer, J.2    Keller, J.3    Van Doorslaer, S.4    Schweiger, A.5    Schuhmann, R.6    Weiland, T.7
  • 40
    • 38149132331 scopus 로고    scopus 로고
    • P. Höfer, P. Carl, X-band pulse-EPR resonator performance, Bruker Report 157/158 (2006) 52-56.
  • 41
    • 38149127053 scopus 로고    scopus 로고
    • J. Forrer, J. Keller, S. Stoll, G. Jeschke, A. Schweiger, Influence of microwave coupling elements on the electromagnetic field distribution and loaded Q-values of pulse EPR mw resonators, in: M.E. Smith, J.H. Strange (Eds.), Magnetic Resonance and Related Phenomena-Extended book of Abstracts of the 28th Congress Ampere, University of Kent at Canterbury, 1996, pp. 35-36.
  • 42
    • 38149105699 scopus 로고    scopus 로고
    • CST Microwave Studio: CST GmbH, Darmstadt, Germany, www.cst.com.
  • 43
    • 0031206837 scopus 로고    scopus 로고
    • Theory of double quantum two-dimensional electron spin resonance with application to distance measurements
    • Saxena S., and Freed J.H. Theory of double quantum two-dimensional electron spin resonance with application to distance measurements. J. Chem. Phys. 107 (1997) 1317-1340
    • (1997) J. Chem. Phys. , vol.107 , pp. 1317-1340
    • Saxena, S.1    Freed, J.H.2
  • 44
    • 0001590048 scopus 로고    scopus 로고
    • Multiple-quantum ESR and distance measurements
    • Borbat P.P., and Freed J.H. Multiple-quantum ESR and distance measurements. Chem. Phys. Lett. 313 (1999) 145-154
    • (1999) Chem. Phys. Lett. , vol.313 , pp. 145-154
    • Borbat, P.P.1    Freed, J.H.2
  • 45
    • 0009924593 scopus 로고    scopus 로고
    • Double-quantum ESR and distance measurements
    • Berliner L.J., et al. (Ed), Kluwer Academic/Plenum Publishers, New York
    • Borbat P.P., and Freed J.H. Double-quantum ESR and distance measurements. In: Berliner L.J., et al. (Ed). Biological Magnetic Resonance vol. 19 (2000), Kluwer Academic/Plenum Publishers, New York 383-459
    • (2000) Biological Magnetic Resonance , vol.19 , pp. 383-459
    • Borbat, P.P.1    Freed, J.H.2
  • 46
    • 0002495363 scopus 로고    scopus 로고
    • Distance measurements by CW and pulsed EPR
    • Berliner L.J., Eaton S.S., and Eaton G.R. (Eds), Kluwer Academic/Plenum Publishers, New York
    • Eaton S.S., and Eaton G.R. Distance measurements by CW and pulsed EPR. In: Berliner L.J., Eaton S.S., and Eaton G.R. (Eds). Biological Magnetic Resonance vol. 19 (2000), Kluwer Academic/Plenum Publishers, New York 1-27
    • (2000) Biological Magnetic Resonance , vol.19 , pp. 1-27
    • Eaton, S.S.1    Eaton, G.R.2
  • 47
    • 0000242143 scopus 로고
    • Hyperfine sublevel correlation (HYSCORE) spectroscopy: a 2D ESR investigation of the squaric acid radical
    • Höfer P., Grupp A., Nebenführ H., and Mehring M. Hyperfine sublevel correlation (HYSCORE) spectroscopy: a 2D ESR investigation of the squaric acid radical. Chem. Phys. Lett. 132 (1986) 279-282
    • (1986) Chem. Phys. Lett. , vol.132 , pp. 279-282
    • Höfer, P.1    Grupp, A.2    Nebenführ, H.3    Mehring, M.4
  • 48
    • 0000402279 scopus 로고    scopus 로고
    • Generation and transfer of coherence in electron-nuclear spin systems by non-ideal microwave pulses
    • Jeschke G., and Schweiger A. Generation and transfer of coherence in electron-nuclear spin systems by non-ideal microwave pulses. Mol. Phys. 88 (1996) 355-383
    • (1996) Mol. Phys. , vol.88 , pp. 355-383
    • Jeschke, G.1    Schweiger, A.2
  • 49
    • 0001671730 scopus 로고    scopus 로고
    • Sensitivity enhancement by matched microwave pulses in one- and two-dimensional electron spin echo envelope modulation spectroscopy
    • Jeschke G., Rakhmatullin R., and Schweiger A. Sensitivity enhancement by matched microwave pulses in one- and two-dimensional electron spin echo envelope modulation spectroscopy. J. Magn. Res. 131 (1998) 261-271
    • (1998) J. Magn. Res. , vol.131 , pp. 261-271
    • Jeschke, G.1    Rakhmatullin, R.2    Schweiger, A.3
  • 50
    • 0030726657 scopus 로고    scopus 로고
    • Crystal structure of methyl coenzyme M reductase: the key enzyme of biological methane formation
    • Ermler U., Grabarse W., Shima S., Goubeaud M., and Thauer R.K. Crystal structure of methyl coenzyme M reductase: the key enzyme of biological methane formation. Science 278 (1997) 1457-1462
    • (1997) Science , vol.278 , pp. 1457-1462
    • Ermler, U.1    Grabarse, W.2    Shima, S.3    Goubeaud, M.4    Thauer, R.K.5
  • 52
    • 1842732521 scopus 로고    scopus 로고
    • Hyperfine decoupling in electron paramagnetic resonance as a powerful tool for unraveling complicated ESEEM spectra of S = 1/2, I ≥ 1/2 systems
    • Mitrikas G., and Schweiger A. Hyperfine decoupling in electron paramagnetic resonance as a powerful tool for unraveling complicated ESEEM spectra of S = 1/2, I ≥ 1/2 systems. J. Magn. Reson. 168 (2004) 88-96
    • (2004) J. Magn. Reson. , vol.168 , pp. 88-96
    • Mitrikas, G.1    Schweiger, A.2
  • 53
    • 0001681194 scopus 로고    scopus 로고
    • New hyperfine-decoupling schemes in electron paramagnetic resonance spectroscopy
    • Van Doorslaer S., and Schweiger A. New hyperfine-decoupling schemes in electron paramagnetic resonance spectroscopy. Chem. Phys. Lett. 308 (1999) 187-194
    • (1999) Chem. Phys. Lett. , vol.308 , pp. 187-194
    • Van Doorslaer, S.1    Schweiger, A.2
  • 54
    • 0011009349 scopus 로고
    • Electron nuclear double resonance study of bis(acetylacetonato)oxovanadium(IV) and some of its adducts in frozen solution
    • Kirste B., and van Willigen H. Electron nuclear double resonance study of bis(acetylacetonato)oxovanadium(IV) and some of its adducts in frozen solution. J. Chem. Phys. 86 (1982) 2743-2749
    • (1982) J. Chem. Phys. , vol.86 , pp. 2743-2749
    • Kirste, B.1    van Willigen, H.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.