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38049106751
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Although the polymerization temperature was elevated to 50 °C after the complete consumption of 7CC, TOX did not polymerize again.This result is attributable to the decrease in polymerizability of TOX originating from the decrease in polarity of the solvent mixture after the consumption of 7CC or deactivation of the propagating species
-
Although the polymerization temperature was elevated to 50 °C after the complete consumption of 7CC, TOX did not polymerize again.This result is attributable to the decrease in polymerizability of TOX originating from the decrease in polarity of the solvent mixture after the consumption of 7CC or deactivation of the propagating species.
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28
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0031078421
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38049099722
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1H NMR spectroscopic analysis.
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1H NMR spectroscopic analysis.
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32
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38049099724
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The end groups of the poly(TOX) (entry 1) was capped by the treatment with acetic anhydride according to ref. 2.
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The end groups of the poly(TOX) (entry 1) was capped by the treatment with acetic anhydride according to ref. 2.
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33
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11144315344
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36
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38049164711
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Other copolymers are viscous oils, and their XRD measurements showed no reflection peak
-
Other copolymers are viscous oils, and their XRD measurements showed no reflection peak.
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