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For related work on ruthenium- and enzyme-catalyzed DKR of alcohols see:
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19
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37849008850
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note
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For example, acidic hydrolysis of the acetamide of 1-phenylethylamine requires reaction at 140 °C for 48 h in concentrated hydrochloric acid.
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20
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37849050790
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note
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The racemization with catalyst 1 under the DKR conditions requires a temperature of 90 °C (see Ref. 6).
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22
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37849013640
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note
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It is not clear why the allyl carbonate gives only a moderate enantioselectivity since there was no background reaction in the control reaction. A likely explanation is that the enzyme itself has some effect on the non-catalyzed reaction, increasing the reaction pathway via direct acylation.
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