Estimation of uncertainty in the analysis of carbonyl compounds by HPLC-UV using DNPH derivatization

Journal of Liquid Chromatography and Related Technologies

Volumn 31, Issue 3, 2008, Pages 361-381

  Delgado, Bárbara ^a   Ayala, Juan H ^a   González, Venerando ^a   Afonso, Ana M ^a  

^a UNIVERSIDAD DE LA LAGUNA   (Spain)

Author keywords

Carbonyl compounds; Gas chromatography; High performance liquid chromatography; Uncertainty

Indexed keywords

CARBONYLATION; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; STATISTICAL METHODS; ULTRAVIOLET DETECTORS; UNCERTAINTY ANALYSIS;

CALIBRATION CURVES; CARBONYL COMPOUNDS;

ORGANIC COMPOUNDS;

CARBONYL DERIVATIVE; HYDRAZONE DERIVATIVE;

ACCURACY; ANALYTIC METHOD; ARTICLE; CONCENTRATION RESPONSE; DERIVATIZATION; GAS CHROMATOGRAPHY; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MASS SPECTROMETRY; METHODOLOGY; STATISTICAL ANALYSIS; ULTRAVIOLET RADIATION; UNCERTAINTY; VALIDATION PROCESS;

EID: 37549063428     PISSN: 10826076     EISSN: 1520572X     Source Type: Journal    
DOI: 10.1080/10826070701780664     Document Type: Article

References (24)

1. Bakeas, E.B.; Argyris, D.I.; Siskos, P.A. Carbonyl compounds in the urban environment of Athens, Greece. Chemosphere 2003, 52 (5), 805-813.
2. Grosjean, D. Atmospheric chemistry of toxic contaminants. 2. Saturated aliphatics - acetaldehyde, dioxane, ethylene-glycol ethers, propylene-oxide. J. Waste Mgmt. Assoc. 1990, 40 (11), 1522-1531.
3. Deandrade, J.B.; Pinheiro, H.L.C.; Andrade, M.V. The formaldehyde and acetaldehyde content of atmospheric aerosol. J. Braz. Chem. Soc. 1995, 6 (3), 287-290.
4. Nondek, L.; Rodier, D.R.; Birks, J.W. Measurement of sub-ppbv concentrations of aldehydes in a forest atmosphere using a new HPLC technique. Environ. Sci. Technol. 1992, 26 (6), 1174-1178.
5. Hedberg, E.; Kristensson, A.; Ohlsson, M.; Johansson, C.; Johansson, P.-A.; Swietlicki, E.; Vesely, V.; Wideqvist, U.; Westerholm, R. Chemical and physical characterization of emissions from birch wood combustion in a wood stove. Atmos. Environ. 2002, 36 (30), 4823-4837.
6. Lehmpuhl, D.W.; Birks, J.W. New gas chromatographic electron-capture detection method for the determination of atmospheric aldehydes and ketones based on cartridge sampling and derivatization with 2,4,6- trichlorophenylhydrazine. J. Chromatogr. A 1996, 740 (1), 71-81.
7. Tanner, R.L.; Meng, Z. Seasonal-variations in ambient atmospheric levels of formaldehyde and acetaldehyde. Environ. Sci. Technol. 1984, 18 (9), 723-726.
8. Keuken, M.P.; Schoonebeek, C. Simultaneous determination of c1-c2 aldehydes and organic-acids in aqueous atmospheric samples by high-performance liquid-chromatography. Int. J. Environ. Anal. Chem. 1989, 35 (4), 227-239.
9. Kiss, G.; Varga, B.; Puchony, Z.V.; Gelencsér, A.; Krivácsy, Z.; Hlavay, J. Sample preparation of atmospheric aerosol for the determination of carbonyl compounds. Talanta 1999, 48 (4), 755-762.
10. Dong, J.-Z.; Moldoveanu, S.C. Gas chromatography-mass spectrometry of carbonyl compounds in cigarette mainstream smoke after derivatization with 2,4-dinitrophenylhydrazine. J. Chromatogr. A 2004, 1027 (1-2), 25-35.
11. Schauer, J.J.; Kleeman, M.J.; Cass, G.R.; Simoneit, B.R.T. Measurement of emissions from air pollution sources. 3. C-1-C-29 organic compounds from fireplace combustion of wood. Environ. Sci. Technol. 2001, 35 (9), 1716-1728.
12. Koziel, J.; Jia, M.; Khaled, A.; Noah, J.; Pawliszyn, J. Field air analysis with SPME device. Anal. Chim. Acta 1999, 400, 153-162.
13. Strassnig, S.; Wenzl, T.; Lankmayr, E.P. Microwave-assisted derivatization of volatile carbonyl compounds with O-(2,3,4,5,6- pentafluorobenzyl)hydroxylamine. J. Chromatogr. A 2000, 891 (2), 267-273.
14. Michels, J.J. Improved measurement of formaldehyde in water-soluble polymers by high-performance liquid chromatography coupled with post-column reaction detection. J. Chromatogr. A 2001, 914 (1-2), 123-129.
15. Kempter, C.; Pötter, W.; Binding, N.; Kläning, H.; Witting, U.; Karst, U. Tailormade derivatizing agents for carbonyl compounds using liquid chromatography. Anal. Chim. Acta 2000, 410 (1-2), 47-64.
16. Kempter, C.; Karst, U. Determination of carbonyl compounds in waters using triazine-based hydrazine reagents and liquid chromatography. Analyst 2000, 125, 433-438.
17. Zurek, G.; Karst, U. 2,4-dinitro-3,5,6-trideuterophenylhydrazones for the quantitation of aldehydes and ketones in air samples by liquid chromatography-mass spectrometry. J. Chromatogr. A 2000, 869 (1-2), 251-259.
18. Jachmann, N.; Karst, U. Synthesis and application of 4-(N,N- dimethylaminosulfonyl)-7-N-methylhydrazino-2,1,3-benzoxadiazole (MDBDH) as a new derivatizing agent for aldehydes. Fresenius J. Anal. Chem. 2001, 369 (1), 47-53.
19. Velikonja, S.; Jarc, I.; Zupancic-Kralj, L.; Marsel, J. Comparison of gaschromatographic and spectrophotometric techniques for the determination of formaldehyde in water. J. Chromatogr. A 1995, 704 (2), 449-454.
20. Uralets, V.P.; Rijks, J.A.; Leclercq, P.A. Syn-anti isomerization of 2,4-dinitrophenylhydrazones of volatile carbonyl-compounds in capillary gas chromatographic-mass spectrometric analyses. J. Chromatogr. 1980, 194 (2), 135-144.
21. Miller, J.; Miller, J. Statistics and Chemometrics for Analytical Chemistry, 4th Edn.; Pearson Education Limited, Publisher: Prentice Hall, 2000.
22. ISO. Guide to the Expression of Uncertainty in Measurement; International Standards Organisation: Geneva, 1993.
23. EURACHEM Guide. Quantifying Uncertainty in Analytical Measurement, 2nd Edn.; 2000.
24. Analytical Methods Committee, The Royal Society of Chemistry. Uncertainty of measurement: implications of its use in analytical science. Analyst 1995, 120, 2303-2308.