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Crystal data for C24H86F2Mg 6O24 (942.79 g mol-1, Data were collected for 1 (170 K) and 1a (250 K) using an IPDS diffractometer (STOE) with MoKα radiation (71.073 pm, Structures were solved and refined with SHELX97 (anisotropic for all non-hydrogen atoms, isotropic for acidic hydrogen atoms; the coordinates of hydrogen atoms of the methyl groups were calculated, 1: monoclinic, P21/c (No.14, crystal dimensions 0.5 x 0.5 x 0.25 mm3, a, 1073.5(2, b, 1199.7(2, c, 2022.3(4) pm, β, 97.44 (2)°, V, 2582.5(8) × 106 pm3, Z, 2, wR 2, 0.106 for all 5658 reflections and 293 parameters, R 1, 0.039 for 4157 reflections with I > 2σ(I, 1a: monoclinic, C2/m No.12, crystal dimensions 0.4 x 0.3 x 0.3 m
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