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Volumn 47, Issue 1, 2008, Pages 190-192

Mg6F2(OMe)10(MeOH)14 - An alkoxide fluoride of an alkaline earth metal

Author keywords

Alkoxides; Fluorides; Magnesium; Sol gel processes; Structure elucidation

Indexed keywords

ALKALINE EARTH METALS; FLUORIDE MINERALS; HYDROGEN BONDS; SOL-GEL PROCESS;

EID: 37549020315     PISSN: 14337851     EISSN: None     Source Type: Journal    
DOI: 10.1002/anie.200703516     Document Type: Article
Times cited : (17)

References (13)
  • 2
    • 0141857251 scopus 로고    scopus 로고
    • Angew. Chem. Int. Ed. 2003, 42, 4251-4254.
    • (2003) Chem. Int. Ed , vol.42 , pp. 4251-4254
    • Angew1
  • 7
    • 37549012278 scopus 로고    scopus 로고
    • Crystal data for C24H86F2Mg 6O24 (942.79 g mol-1, Data were collected for 1 (170 K) and 1a (250 K) using an IPDS diffractometer (STOE) with MoKα radiation (71.073 pm, Structures were solved and refined with SHELX97 (anisotropic for all non-hydrogen atoms, isotropic for acidic hydrogen atoms; the coordinates of hydrogen atoms of the methyl groups were calculated, 1: monoclinic, P21/c (No.14, crystal dimensions 0.5 x 0.5 x 0.25 mm3, a, 1073.5(2, b, 1199.7(2, c, 2022.3(4) pm, β, 97.44 (2)°, V, 2582.5(8) × 106 pm3, Z, 2, wR 2, 0.106 for all 5658 reflections and 293 parameters, R 1, 0.039 for 4157 reflections with I > 2σ(I, 1a: monoclinic, C2/m No.12, crystal dimensions 0.4 x 0.3 x 0.3 m
    • 3. CCDC-656257 (1) and CCDC-656258 (1a) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/ data_request/cif.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.