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Intensity data were collected at room temperature on a Bruker SMART diffractometer with an APEX II CCD detector using omega and psi scans. The structure was solved using SIR92 and refined with SHELXL-97 in the Pl space group within the WINGX software system (PrC15H20O7, FW, 467.23 g/mol, triclinic, P1̄, a, 7.8538(5) Å, b, 11.0219(7) Å, c, 11.6693(8) Å, a, 108.6740(10)°, β, 105.8120(10)°, γ, 104.1080(10)°, Z, μ, 2.875 mm-1, Rint, 8.44, R1, 5.02, wR2, 5.55, Powder X-ray diffraction data were collected on a Scintag XDS 2000 (Cu Kα, 3-60°, 0.05° step, 1.0 s/step, The calculated powder patterns were compared to the single-crystal data and show excellent agreement, confirming phase purity (see the Supporting Information for PXRD pattern and CIF, Further, Crystallographic data for GWMOF-11 has been deposited with the Cambridge Crystallographic Data Centre (CCDC) and may be obtained at
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int = 8.44%, R1 = 5.02%, wR2 = 5.55%). Powder X-ray diffraction data were collected on a Scintag XDS 2000 (Cu Kα, 3-60°, 0.05° step, 1.0 s/step). The calculated powder patterns were compared to the single-crystal data and show excellent agreement, confirming phase purity (see the Supporting Information for PXRD pattern and CIF). Further, Crystallographic data for GWMOF-11 has been deposited with the Cambridge Crystallographic Data Centre (CCDC) and may be obtained at http://www.ccdc.cam.ac.uk/ by citing reference number 659677.
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