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Volumn 7, Issue 12, 2007, Pages 2390-2393

Synthesis and characterization of a praseodymium-adipate framework templated with 1,2-bis(4-pyridyl)ethane: Host-guest interactions and structural survey

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EID: 37549013265     PISSN: 15287483     EISSN: None     Source Type: Journal    
DOI: 10.1021/cg700741v     Document Type: Article
Times cited : (39)

References (33)
  • 10
    • 0034777214 scopus 로고    scopus 로고
    • Ferey, G. Chem. Mater. 2001, 13, 3084-3098.
    • (2001) Chem. Mater , vol.13 , pp. 3084-3098
    • Ferey, G.1
  • 25
    • 84868419673 scopus 로고    scopus 로고
    • Intensity data were collected at room temperature on a Bruker SMART diffractometer with an APEX II CCD detector using omega and psi scans. The structure was solved using SIR92 and refined with SHELXL-97 in the Pl space group within the WINGX software system (PrC15H20O7, FW, 467.23 g/mol, triclinic, P1̄, a, 7.8538(5) Å, b, 11.0219(7) Å, c, 11.6693(8) Å, a, 108.6740(10)°, β, 105.8120(10)°, γ, 104.1080(10)°, Z, μ, 2.875 mm-1, Rint, 8.44, R1, 5.02, wR2, 5.55, Powder X-ray diffraction data were collected on a Scintag XDS 2000 (Cu Kα, 3-60°, 0.05° step, 1.0 s/step, The calculated powder patterns were compared to the single-crystal data and show excellent agreement, confirming phase purity (see the Supporting Information for PXRD pattern and CIF, Further, Crystallographic data for GWMOF-11 has been deposited with the Cambridge Crystallographic Data Centre (CCDC) and may be obtained at
    • int = 8.44%, R1 = 5.02%, wR2 = 5.55%). Powder X-ray diffraction data were collected on a Scintag XDS 2000 (Cu Kα, 3-60°, 0.05° step, 1.0 s/step). The calculated powder patterns were compared to the single-crystal data and show excellent agreement, confirming phase purity (see the Supporting Information for PXRD pattern and CIF). Further, Crystallographic data for GWMOF-11 has been deposited with the Cambridge Crystallographic Data Centre (CCDC) and may be obtained at http://www.ccdc.cam.ac.uk/ by citing reference number 659677.
  • 27
    • 0004150157 scopus 로고    scopus 로고
    • Institut für Anorganische Chemie der Universität Göttingen: Göttingen, Germany
    • Sheldrick, G. M. SHELX97; Institut für Anorganische Chemie der Universität Göttingen: Göttingen, Germany, 1998.
    • (1998) SHELX97
    • Sheldrick, G.M.1
  • 31
    • 37549039594 scopus 로고    scopus 로고
    • JADE, edition 6.1; Materials Data Inc.: Livermore, CA, 2002.
    • JADE, edition 6.1; Materials Data Inc.: Livermore, CA, 2002.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.