A robust conglomerate structure type in salts of cationic organopalladium complexes and non-coordinating anions

CrystEngComm

Volumn 10, Issue 1, 2008, Pages 39-47

  Kalf, Irmgard ^a   Wang, Ruimin ^a   Englert, Ulli ^a  

^a RWTH AACHEN UNIVERSITY   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 37149016369     PISSN: 14668033     EISSN: 14668033     Source Type: Journal    
DOI: 10.1039/b712641g     Document Type: Article

References (34)

1. M. Pallavicini C. Bolchi L. Fumagalli O. Piccolo E. Valoti Tetrahedron: Asym. 2007 18 906
2. J. Jacques M. Leclercq M. J. Brienne Tetrahedron 1981 37 1727
3. C. J. Price Chem. Eng. Prog. 1997 93 34
4. J. Jacques, A. Collet and S. H. Wilen, Enantiomers, Racemates, and Resolutions, Krieger Publishing Company, Malabar, Florida, 1994
5. A. Collet M. J. Brienne J. Jacques Chem. Rev. 1980 80 215
6. E. Ballesteros M. Gallego M. Valcarcel Anal. Chem. 1996 68 322
7. W. M. L. Wood, in Chirality in Industry II. ed., A. N. Collins,,, G. N. Sheldrake, and, J. Crosby,, John Wiley & Sons, Chichester, 1997, pp. 119
8. M. K. Saha R. Ramanujam I. Bernal F. R. Fronczek Cryst. Growth Des. 2002 2 205
9. I. Kalf R. Wang U. Englert J. Organomet. Chem. 2006 691 2277
10. A. Ladenburg Liebigs Ann. Chem. 1908 364 227
11. J. Vicente I. Saura-Llamas M. G. Palin Organometallics 1997 16 826
12. Y. Fuchita K. Yoshinaga Y. Ikeda J. Kinoshita-Kawashima J. Chem. Soc., Dalton Trans. 1997 2495
13. A. C. T. North D. C. Phillips F. S. Mathews Acta Crystallogr., Sect. A 1968 24 351
14. G. M. Sheldrick, "SADABS, Program for Empirical Absorption Correction of Area Detector Data," University of Göttingen, 1996
15. G. M. Sheldrick, "SHELXS97, Program for Crystal Structure Solution," University of Göttingen, 1997
16. G. M. Sheldrick, "SHELXL97, Program for Crystal Structure Refinement," University of Göttingen, 1997
17. H. D. Flack Acta Crystallogr., Sect. A 1983 39 876
18. U. Englert A. Häring C. Hu I. Kalf Z. Anorg. Allg. Chem. 2002 628 1173
19. B. Calmuschi U. Englert Acta Crystallogr., Sect. C 2003 58 m545
20. Y. LePage J. Appl. Crystallogr. 1987 20 264
21. Y. LePage J. Appl. Crystallogr. 1988 21 983
22. A. L. Spek J. Appl. Crystallogr. 2003 36 7
23. D. E. Williams, "PCK83, a crystal molecular packing analysis program," Quantum Chemistry Programs Exchange, 1983
24. U. Englert, in Advances in Molecular Structure Research, Vol. 6, ed., M. Hargittai, and, I. Hargittai,, JAI Press Inc., Greenwich, CT, 2000, pp. 49
25. A. C. Cope E. C. Friedrich J. Am. Chem. Soc. 1968 90 909
26. F. Allen Acta Crystallogr., Sect. B 2002 B58 380
27. Error-free entries without disorder for which 3D coordinates were available, CSD Version 5.28, including update of January 2007
28. W. E. Rhine J. H. Davis G. Stucky J. Am. Chem. Soc. 1975 97 2079
29. W. E. Rhine J. H. Davis G. Stucky J. Organomet. Chem. 1977 134 139
30. M. F. Lappert A. Singh L. M. Englehardt A. H. White J. Organomet. Chem. 1984 262 271
31. M. H. Wang U. Englert U. Koelle J. Organomet. Chem. 1993 453 127
32. G. Gilli, in Fundamentals of Crystallography, ed., G. Giacovazzo,, Oxford University Press, Oxford, 2002, pp. 585
33. M. C. Etter J. C. MacDonald J. Bernstein Acta Crystallogr., Sect. B 1990 46 256
34. I. Kalf and U. Englert, unpublished results. Microanalytical data and preliminary X-ray results suggest solvate formation for several of these complexes. No conglomerates and no dominant structure type were encountered: exchange of the counteranion and/or substitution on the arene ring resulted in different packing patterns even for closely related compounds. These largely unrelated structures will be reported elsewhere as structure communications