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Methanesulfonyl azide was prepared to Danheiser’s modification of Boyer’s method [see ref. 10(6)] in a greater than 90% yield and was used for diazo transfer reactions without further purification; (6) see
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Methanesulfonyl azide was prepared to Danheiser’s modification of Boyer’s method [see ref. 10(6)] in a greater than 90% yield and was used for diazo transfer reactions without further purification; (6) see J. H. Boyer, C. H. Mack, W. Goebel and L. R. Morgan, Jr., J. Org. Chem., 1959,23, 1051.
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0000851925
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The carbonate complex Na4Rh2(C03)4-2.5H20 was prepared from rhodium(n) acetate in > 90% yield according to literature procedure
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The carbonate complex Na4Rh2(C03)4-2.5H20 was prepared from rhodium(n) acetate in > 90% yield according to literature procedure, in C. R. Wilson and H. Taube, Inorg. Chem., 1975.14, 405.
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references cited therein
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R. E. Lowenthal, A. Abiko and S. Masamune, Tetrahedron Lett., 1990, 31, 6005 and references cited therein.
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For intramolecular examples of this process, see
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For intramolecular examples of this process, see J. S. Clark and S. A. Krowiak, Tetrahedron Lett., 1993, 34, 4385.
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