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Volumn 44, Issue 5, 2007, Pages 1009-1011

A facile three-components, one-pot synthesis of pyrimido[4,5-d]pyrimidine- 2,5-dione derivatives under microwave-assisted conditions

(4) Dabiri, Minoo a Arvin Nezhad, Hamid a Khavasi, Hamid R a Bazgir, Ayoob a

a SHAHID BEHESHTI UNIVERSITY (Iran)

Author keywords

[No Author keywords available]

Indexed keywords

6 AMINO 3 METHYL 2 (METHYLTHIO)PYRIMIDIN 4(3H) ONE; ALDEHYDE; PYRIMIDINE DERIVATIVE; PYRIMIDO[4,5 D]PYRIMIDINE 2,5 DIONE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHEMICAL STRUCTURE; MELTING POINT; MICROWAVE IRRADIATION; ONE POT SYNTHESIS; POLYMERIZATION; PROTON NUCLEAR MAGNETIC RESONANCE; REACTION ANALYSIS; STRUCTURE ANALYSIS; X RAY ANALYSIS; X RAY DIFFRACTION;

EID: 36649002099 PISSN: 0022152X EISSN: None Source Type: Journal
DOI: 10.1002/jhet.5570440505 Document Type: Article

Times cited : (45)

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- Crystal data analyses: Stoe IPDS-II two-circle diffractometer, MoKα radiation (λ, 0.71073, T =293(2) K; Graphite monochromator; numerical absorption correction. Structure solution by direct methods using SHELXS and refinement by full-matrix least-squares on F2 using SHELXL of the X-STEP32 suite of programs [16] all non-hydrogen atoms were refined anisotropically. Crystal data for 4a: C14H14N 4O2S (DMSO, M, 380.50 gmol-1; crystal dimensions 0.20 x 0.10 x 0.05 mm3; Triclinic, space group P1, Z=2; a, 8.661(4, b, 10.132(4, c, 11.185(4) Å, α, 77.11(3)°, β, 67.16(3)°, γ, 86.52(3)°; V, 881.3(6) Å3; Z, 2; F000, 400, pealc, 1.434 g cm-3; 2.02°< θ<29.30°; section of the reciprocal lattice: -11 ≤ h ≤ 10, 13 ≤ k ≤ 13, 13 ≤ 1 ≤ 14; of 8552 measured reflections, 7279 were independent
- -3).

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