-
1
-
-
20544450502
-
-
2nd ed, de Meijere, A, Diederich, F, Eds, Wiley-VCH: Weinheim
-
Metal-Catalyzed Cross-Coupling Reactions, 2nd ed.; de Meijere, A.; Diederich, F., Eds.; Wiley-VCH: Weinheim, 2004.
-
(2004)
Metal-Catalyzed Cross-Coupling Reactions
-
-
-
2
-
-
0003779363
-
-
2nd ed, Beller, M, Bolm, C, Eds, Wiley-VCH: Weinheim
-
Transition Metals for Organic Synthesis, 2nd ed.; Beller, M.; Bolm, C., Eds.; Wiley-VCH: Weinheim, 2004.
-
(2004)
Transition Metals for Organic Synthesis
-
-
-
3
-
-
33744510833
-
-
Dyker, G, Ed, Wiley-VCH: Weinheim
-
Handbook of C-H Transformations; Dyker, G., Ed.; Wiley-VCH: Weinheim, 2005.
-
(2005)
Handbook of C-H Transformations
-
-
-
5
-
-
33846918696
-
-
Alberico, D.; Scott, M. E.; Lautens, M. Chem. Rev. 2007, 107, 174.
-
(2007)
Chem. Rev
, vol.107
, pp. 174
-
-
Alberico, D.1
Scott, M.E.2
Lautens, M.3
-
6
-
-
34248361209
-
-
Campeau, L.-C.; Stuart, D. R.; Fagnou, K. Aldrichimica Acta 2007, 40, 35.
-
(2007)
Aldrichimica Acta
, vol.40
, pp. 35
-
-
Campeau, L.-C.1
Stuart, D.R.2
Fagnou, K.3
-
7
-
-
29144448603
-
-
Ackermann, L. In Topics in Organometallic Chemistry; Chatani, N., Ed.; Springer: Berlin/Heidelberg/New York, 2007, DOI: 10.1007/3418_2007_062.
-
Ackermann, L. In Topics in Organometallic Chemistry; Chatani, N., Ed.; Springer: Berlin/Heidelberg/New York, 2007, DOI: 10.1007/3418_2007_062.
-
-
-
-
9
-
-
33746494445
-
-
Schnurch, M.; Flasik, R.; Khan, A. F.; Spina, M.; Mihovilovic, M. D.; Stanetty, P. Eur. J. Org. Chem. 2006, 3283.
-
(2006)
Eur. J. Org. Chem
, pp. 3283
-
-
Schnurch, M.1
Flasik, R.2
Khan, A.F.3
Spina, M.4
Mihovilovic, M.D.5
Stanetty, P.6
-
11
-
-
0032556390
-
-
For representative examples of [Rh], see: (a) Oi, S.; Fukita, S.; Inoue, Y. Chem. Commun. 1998, 2439.
-
For representative examples of [Rh], see: (a) Oi, S.; Fukita, S.; Inoue, Y. Chem. Commun. 1998, 2439.
-
-
-
-
12
-
-
0347296197
-
-
(b) Bedford, R. B.; Coles, S. J.; Hursthouse, M. B.; Limmert, M. E. Angew. Chem. Int. Ed. 2003, 42, 112.
-
(2003)
Angew. Chem. Int. Ed
, vol.42
, pp. 112
-
-
Bedford, R.B.1
Coles, S.J.2
Hursthouse, M.B.3
Limmert, M.E.4
-
14
-
-
0242352421
-
-
(d) Oi, S.; Watanabe, S.-i.; Fukita, S.; Inoue, Y. Tetrahedron Lett. 2003, 44, 8665.
-
(2003)
Tetrahedron Lett
, vol.44
, pp. 8665
-
-
Oi, S.1
Watanabe, S.-I.2
Fukita, S.3
Inoue, Y.4
-
15
-
-
20444507164
-
-
(e) Ueura, K.; Satoh, T.; Miura, M. Org. Lett. 2005, 7, 2229.
-
(2005)
Org. Lett
, vol.7
, pp. 2229
-
-
Ueura, K.1
Satoh, T.2
Miura, M.3
-
16
-
-
36549016477
-
-
For [Pd]: (f) Miura, M.; Satoh, T. In Topics in Organometallic Chemistry, 14; Tsuji, J., Ed.; Springer: Berlin/Heidelberg/New York, 2005, 55-83.
-
For [Pd]: (f) Miura, M.; Satoh, T. In Topics in Organometallic Chemistry, Vol. 14; Tsuji, J., Ed.; Springer: Berlin/Heidelberg/New York, 2005, 55-83.
-
-
-
-
17
-
-
0033248563
-
-
(g) Kawamura, Y.; Satoh, T.; Miura, M.; Nomura, M. Chem. Lett. 1999, 961.
-
(1999)
Chem. Lett
, pp. 961
-
-
Kawamura, Y.1
Satoh, T.2
Miura, M.3
Nomura, M.4
-
18
-
-
0034620911
-
-
(h) Kametani, Y.; Satoh, T.; Miura, M.; Nomura, M. Tetrahedron Lett. 2000, 41, 2655.
-
(2000)
Tetrahedron Lett
, vol.41
, pp. 2655
-
-
Kametani, Y.1
Satoh, T.2
Miura, M.3
Nomura, M.4
-
19
-
-
0035833016
-
-
(i) Terao, Y.; Kametani, Y.; Wakui, H.; Satoh, T.; Miura, M.; Nomura, M. Tetrahedron 2001, 57, 5967.
-
(2001)
Tetrahedron
, vol.57
, pp. 5967
-
-
Terao, Y.1
Kametani, Y.2
Wakui, H.3
Satoh, T.4
Miura, M.5
Nomura, M.6
-
20
-
-
31544455027
-
-
(j) Campeau, L.-C.; Parisien, M.; Jean, A.; Fagnou, K. J. Am. Chem. Soc. 2006, 128, 581.
-
(2006)
J. Am. Chem. Soc
, vol.128
, pp. 581
-
-
Campeau, L.-C.1
Parisien, M.2
Jean, A.3
Fagnou, K.4
-
21
-
-
19744365933
-
-
(k) Kalyani, D.; Deprez, N. R.; Desai, L. V.; Sanford, M. S. J. Am. Chem. Soc. 2005, 127, 7330.
-
(2005)
J. Am. Chem. Soc
, vol.127
, pp. 7330
-
-
Kalyani, D.1
Deprez, N.R.2
Desai, L.V.3
Sanford, M.S.4
-
22
-
-
33750438087
-
-
(l) Hull, K. L.; Lanni, E. L.; Sanford, M. S. J. Am. Chem. Soc. 2006, 128, 14047.
-
(2006)
J. Am. Chem. Soc
, vol.128
, pp. 14047
-
-
Hull, K.L.1
Lanni, E.L.2
Sanford, M.S.3
-
24
-
-
25444458063
-
-
(n) Zaitsev, V. G.; Shabashov, D.; Daugulis, O. J. Am. Chem. Soc. 2005, 127, 13154.
-
(2005)
J. Am. Chem. Soc
, vol.127
, pp. 13154
-
-
Zaitsev, V.G.1
Shabashov, D.2
Daugulis, O.3
-
25
-
-
34547883488
-
-
and references cited therein
-
(o) Chiong, H. A.; Pham, Q.-N.; Daugulis, O. J. Am. Chem. Soc. 2007, 129, 9879; and references cited therein.
-
(2007)
J. Am. Chem. Soc
, vol.129
, pp. 9879
-
-
Chiong, H.A.1
Pham, Q.-N.2
Daugulis, O.3
-
26
-
-
17844365805
-
-
Bruneau, C, Dixneuf, P. H, Eds, Springer: Berlin/Heidelberg/New York
-
Kakiuchi, F.; Chatani, N. In Ruthenium Catalysts and Fine Chemistry, Vol. 11; Bruneau, C.; Dixneuf, P. H., Eds.; Springer: Berlin/Heidelberg/New York, 2004, 45-79.
-
(2004)
Ruthenium Catalysts and Fine Chemistry
, vol.11
, pp. 45-79
-
-
Kakiuchi, F.1
Chatani, N.2
-
27
-
-
17844369291
-
-
Murahashi, S.-I, Ed, Wiley-VCH: Weinheim
-
Kakiuchi, F.; Chatani, N. In Ruthenium in Organic Synthesis; Murahashi, S.-I., Ed.; Wiley-VCH: Weinheim, 2004, 219-255.
-
(2004)
Ruthenium in Organic Synthesis
, pp. 219-255
-
-
Kakiuchi, F.1
Chatani, N.2
-
28
-
-
0000592976
-
-
(a) Oi, S.; Fukita, S.; Hirata, N.; Watanuki, N.; Miyano, S.; Inoue, Y. Org Lett. 2001, 3, 2579.
-
(2001)
Org Lett
, vol.3
, pp. 2579
-
-
Oi, S.1
Fukita, S.2
Hirata, N.3
Watanuki, N.4
Miyano, S.5
Inoue, Y.6
-
29
-
-
0013373107
-
-
(b) Oi, S.; Ogino, Y.; Fukita, S.; Inoue, Y. Org. Lett. 2002, 4, 1783.
-
(2002)
Org. Lett
, vol.4
, pp. 1783
-
-
Oi, S.1
Ogino, Y.2
Fukita, S.3
Inoue, Y.4
-
30
-
-
0037442914
-
-
(c) Kakiuchi, F.; Kan, S.; Igi, K.; Chatani, N.; Murai, S. J. Am. Chem. Soc. 2003, 125, 1698.
-
(2003)
J. Am. Chem. Soc
, vol.125
, pp. 1698
-
-
Kakiuchi, F.1
Kan, S.2
Igi, K.3
Chatani, N.4
Murai, S.5
-
31
-
-
24944442184
-
-
(d) Oi, S.; Sakai, K.; Inoue, Y. Org. Lett. 2005, 7, 4009.
-
(2005)
Org. Lett
, vol.7
, pp. 4009
-
-
Oi, S.1
Sakai, K.2
Inoue, Y.3
-
32
-
-
17444374923
-
-
(e) Oi, S.; Aizawa, E.; Ogino, Y.; Inoue, Y. J. Org. Chem. 2005, 70, 3113.
-
(2005)
J. Org. Chem
, vol.70
, pp. 3113
-
-
Oi, S.1
Aizawa, E.2
Ogino, Y.3
Inoue, Y.4
-
33
-
-
34249011440
-
-
and references cited therein
-
(f) Ueno, S.; Chatani, N.; Kakiuchi, F. J. Am. Chem. Soc. 2007, 129, 6098; and references cited therein.
-
(2007)
J. Am. Chem. Soc
, vol.129
, pp. 6098
-
-
Ueno, S.1
Chatani, N.2
Kakiuchi, F.3
-
34
-
-
33744543074
-
-
For a review on the use of secondary phosphine oxides in catalysis, see
-
For a review on the use of secondary phosphine oxides in catalysis, see: Ackermann, L. Synthesis 2006, 1557.
-
(2006)
Synthesis
, pp. 1557
-
-
Ackermann, L.1
-
36
-
-
33746307336
-
-
Ackermann, L.; Althammer, A.; Born, R. Angew. Chem. Int. Ed. 2006, 45, 2619.
-
(2006)
Angew. Chem. Int. Ed
, vol.45
, pp. 2619
-
-
Ackermann, L.1
Althammer, A.2
Born, R.3
-
37
-
-
34548319237
-
-
Ackermann, L.; Born, R.; Álvarez Bercedo, P. Angew. Chem. Int. Ed. 2007, 46, 6364.
-
(2007)
Angew. Chem. Int. Ed
, vol.46
, pp. 6364
-
-
Ackermann, L.1
Born, R.2
Álvarez Bercedo, P.3
-
38
-
-
36549060887
-
-
Representative Procedure, Synthesis of 3d (Table 1, Entry 3) A suspension of 5 (12.6 mg, 0.05 mmol, 5.0 mol, K2CO 3 (415 mg, 3.00 mmol, 2-phenylpyridine (160 mg, 1.03 mmol, and 4-bromoacetophenone (438 mg, 2.20 mmol) in anhyd NMP (2.0 mL) was stirred for 22 h at 120°C under N2. After the reaction mixture was cooled to ambient temperature, Et2O (50 mL) and H2O (40 mL) were added. The separated aqueous phase was extracted with Et2O (3 x 50 mL, The combined organic layers were washed with H2O (50 mL) and brine (50 mL, dried over Na2SO4, and concentrated in vacuo. The remaining residue was purified by column chromatography on silica gel (n-pentane-Et2O, 3:1 → 2:1 → 1:1 → 1:2 → 1:3) to yield 3d (361 mg, 90, mp 200.5-201.5°C) as a yellow solid. 1H NMR (300 MHz, CDCl3, δ, 8.30 d, J
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2: 391.1572; found: 391.1550.
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