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Crystal data for (NMe4)4/3Na 8/3[(Sn(OH)2)2L2]·40H 2O: Mr, 1834.08, cubic, F432, a, 38.502(2) Å, V, 57076(4) Å3, Z, 24, θmax, 27.48°, MoKα radiation, λ, 0.71073 Å, T, 130 K, μ-(MoKα, 0.629 mm -1, 89867 reflections measured, 5500 unique which were used in all calculations, 202 parameters, The structure was solved by direct methods (SHELX97[6, wR2, 0.2317 (all data) and R1, 0.0736 (I > 2σ(I, Flack parameter, 0.00(9, b) Crystal data for (NMe4)4/3Na8/3[(WO2) 2L2]·12MeOH·4H2O: M r, 1804.782, cubic Pa3, a, 37.3271 (3) Å, V, 52008.3(7) Å3, Z
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2O) contain the supplementary crystallographic data for this paper. These data can be obtained free of charge from The Cambridge Crystallographic Data Centre via www.ccdc.cam.ac.uk/data_request/cif.
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36549053085
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SHELX97 Programs for Crystal Structure Analysis. (Release 97-2). G. M. Sheldrick, Institut für Anorganische Chemie der Universität, Tammanstrasse 4, 3400 Göttingen, Germany, 1998.
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SHELX97 Programs for Crystal Structure Analysis. (Release 97-2). G. M. Sheldrick, Institut für Anorganische Chemie der Universität, Tammanstrasse 4, 3400 Göttingen, Germany, 1998.
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