A unified approach for the measurement of individual or total volatile organic sulfur compounds in hydrocarbon matrices by dual-plasma chemiluminescence detector and low thermal mass gas chromatography

Journal of Chromatographic Science

Volumn 45, Issue 10, 2007, Pages 671-676

  Gras, Ronda ^a   Luong, Jim ^a   Shearer, Randy ^b  

^a Dow Chemical Canada Inc   (Canada)

^b Rentech Inc   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

EID: 36448989761     PISSN: 00219665     EISSN: None     Source Type: Journal    
DOI: 10.1093/chromsci/45.10.671     Document Type: Article

References (10)

1. R. Bacaud, V. Cebollar, L. Membrado, M. Matt, S. Pessayre, and E. Galvez. Evolution of sulfur compounds and hydrocarbons classes in diesel fuels during hydrodesulfurization - combined use of thinlayer chromatography and GC-sulfur-selective chemiluminescence detection. Ind. Eng. Chem. Res. 41(24): 6005-6014 (2002).
2. R. Filley and S. Eser. Analysis of hydrocarbons and sulfur compounds in two FCC decant oils and their carbonization products. Energy Fuels 11(3): 623-630 (1997).
3. R.L. Shearer, D.L. O'Neal, R. Rios, and M.D. Baker. Analysis of sulfur compounds by gas chromatography with sulfur chemiluminescence detection. J. Chromatogr. Sci 28: 24-28 (1990).
4. J. Luong, R. Gras, and R. Tymko. Innovations in high-pressure liquid injection technique for gas chromatography: pressurized liquid injection system. J. Chromatogr. Sci. 41(10): 550-559 (2003).
5. J. Luong, R. Gras, R. Mustacich, and H. Cortes. Low thermal mass gas chromatography: principle and applications. J. Chromatogr. Sci. 44(5): 253-261(2006).
6. R. Benner and D. Stedman. Universal sulfur detection by chemiluminescence. Anal. Chem. 61: 1268-1271 (1989).
7. R. Shearer. Development of flameless sulfur chemiluminescence detection: applications to gas chromatography. J. High Resolut. Chromatogr. 13: 421-426 (1990).
8. F. Di Sanzo, W. Bray, and B. Chawla. Determination of the sulfur components of gasoline steams by high resolution chromatography. J. High Resolut. Chromatogr. 17: 255-258 (1994).
9. R. Gras, J. Luong, and R. Shearer. Improved speed and sensitivity in the analysis of volatile sulfurs in hydrocarbons by microvolume injection, vacuum outlet GC. Keynote lecture KBL07, 25th ISCC Symposium, May 13-May 17, 2002, Riva del Garda, Italy.
10. R. Nadkarni and A. Kishore. Determination of sulfur in petroleum products and lubricants: a critical review of test performance. Am. Lab. 32: 16-29 (2000).