A rapid benchtop NMR method for determination of droplet size distributions in food emulsions

European Journal of Lipid Science and Technology

Volumn 109, Issue 11, 2007, Pages 1095-1103

  Van Duynhoven, John P M ^a   Maillet, Benjamin ^a   Schell, Jimmy ^a   Tronquet, Mathieu ^a   Goudappel, Gert Jan W ^a   Trezza, Elena ^a   Bulbarello, Andrea ^a   Van Dusschoten, Dagmar ^b,c  

^a UNILEVER RESEARCH VLAARDINGEN   (Netherlands)

^b DSM RESEARCH   (Netherlands)

^c FORSCHUNGSZENTRUM JÜLICH   (Germany)

Author keywords

Benchtop; Droplet size distributions; Food emulsions; NMR

Indexed keywords

EID: 36349013169     PISSN: 14387697     EISSN: 14389312     Source Type: Journal    
DOI: 10.1002/ejlt.200700019     Document Type: Article

References (20)

1. D. W. De Bruijne, A. Bot: Fat-fabricated Foods Aspen Publishers, Gaithersburg (USA) 1999.
2. G. Dobson: Spectroscopy and spectrometry of lipids. Part 1. Lipid analysis by vibrational spectroscopy. Eur J Lipid Sci Technol. 2001, 103, 815-826.
3. H. Todt, W. Burk, G. Guthausen, A. Guthausen, A. Kamlowski, D. Schmalbein: Quality control with time-domain NMR. Eur J Lipid Sci Technol. 2001, 103, 835-840.
4. J. C. Vandenenden, D. Waddington, H. Vanaalst, C. G. Vankralingen, K. J. Packer: Rapid-determination of water droplet size distributions by PFG-NMR. J Colloid Interface Sci. 1990, 140, 105-113.
5. P. T. Callaghan: Principles of Nuclear Magnetic Resonance Microscopy. Clarendon Press, Oxford (UK) 1993.
6. B. Balinov, O. Soderman, T. Warnheim: Determination of water droplet size in margarines and low-calorie spreads by nuclear-magnetic-resonance self-diffusion. J Am Oil Chem Soc. 1994, 71, 513-518.
7. C. T. Verrips, J. Zaalberg: The intrinsive microbial stability of water-in-oil emulsions. 1. Theory. Exp Eur J Appl Microbiol Biotechnol. 1980, 10, 73-79.
8. G. J. W. Goudappel, J. P. M. van Duynhoven, M. M. W. Mooren: Measurement of oil droplet size distributions in food oil/water emulsions by time domain pulsed field gradient NMR. J Colloid Interface Sci. 2001, 239, 535-542.
9. A. Bot, E. Floter, J. G. Lammers, E. Pelan: Controlling the texture of spreads. In: Semi-solid Foods. Ed. BM. McKenna, CRC Press, Boca Raton (USA) 2003, pp. 350-372.
10. J. S. Murday, R. M. Cotts: Self-diffusion coefficient of liquid lithium. J Chem Phys. 1968, 48, 4938-4945.
11. K. J. Packer, C. J. Rees: Pulsed NMR studies of restricted diffusion. J Colloid Interface Sci. 1972, 40, 216-218.
12. J. P. M. van Duynhoven, G. J. W. Goudappel, G. van Dalen, P. C. van Bruggen, J. C. G. Blonk, A. P. A. M. Eijkelenboom: Scope of droplet size measurements in food emulsions by pulsed field gradient NMR at low field. Magn Reson Chem. 2002, 40, S51-S59.
13. P. Jokela, P. D. I. Fletcher, R. Aveyard, J. R. Lu: The use of computerized microscopic image-analysis to determine emulsion droplet size distributions. J Colloid Interface Sci. 1990, 134, 417-426.
14. G. van Dalen: Determination of the water droplet size distribution of fat spreads using confocal scanning laser microscopy. J Microsc. 2002, 208, 116-133.
15. H. G. Barth: Modern Methods of Particle Size Analysis. John Wiley, New York (USA) 1984.
16. T. Allen: Particle Size Measurement. Chapman and Hall, London (UK) 1975.
17. P. S. Denkova, S. Tcholakova, N. D. Denkov, K. D. Danov, B. Campbell, C. Shawl, D. Kim: Evaluation of the precision of drop-size determination in oil/water emulsions by low-resolution NMR spectroscopy. Langmuir. 2004, 20, 11402-11413.
18. S. Kiokas, A. A. Reszka, A. Bot: The use of static light scattering and PFG-NMR to measure droplet sizes in heat-treated acidified protein-stabilised O/W gels. Int Dairy J. 2004, 14, 287-295.
19. K. G. Hollingsworth, A. J. Sederman, C. Buckley, L. F. Gladden, M. L. Johns: Fast emulsion droplet sizing using NMR self-diffusion measurements. J Colloid Interface Sci. 2004, 274, 244-250.
20. C. Buckley, K. G. Hollingsworth, A. J. Sederman, D. J. Holland, M. L. Johns, L. F. Gladden: Applications of fast diffusion measurement using Difftrain. J Magn Reson. 2003, 161, 112-117.