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36249005849
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note
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1H NMR (400 MHz): 4.23(s, 5H, cp-H), 4.44(s, 2H, cp-H), 4.61(s, 2H, cp-H), 7.51-7.58(m, 3H, Ar-H), 7.84(s, 1H, CH{double bond, long}N), 7.86-8.00(m, 4H, Ar-H), 9.31(s, 1H, CSN-H), 10.12(s, 1H, Ar-NH).
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22
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36249025135
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note
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2 (all data) = 0.1129. The crystal structure was determined on a Rigaku RAXIS-IV imaging plate area detector with graphite monochromated Mo Kα radiation (λ = 0.71073 Å) at temperature 291(2) K. Reflections (I > 2σ) of 3231 were corrected for Lorentz-polarization effects. All calculations were performed using the Shelxl-97 crystallographic software package [7].
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23
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36249027443
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G.M. Sheldrick, Shelxl-97: Program for Crystal Structure Refinement, University of Göttingen, Göttingen, Germany, 1997.
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33645237898
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Huang, C.H.8
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