SCOPUS 정보 검색 플랫폼

Volumn 54, Issue 5, 2007, Pages 1115-1118

Tribromoisocyanuric acid (TBCA) and oxone®-MX systems as oxidizing agents: Oxidative coupling of thiols to their corresponding disulfides under mild and heterogeneous conditions

(7) Zolfigol, Mohammad Ali a Niknam, Khodabakhsh b Bagherzadeh, Mojtaba c Ghorbani Choghamarani, Arash d Koukabi, Nadiya a Hajjamia, Maryam a Kolvaria, Eskandar a

a BU ALI SINA UNIVERSITY (Iran)

b PERSIAN GULF UNIVERSITY (Iran)

c SHARIF UNIVERSITY OF TECHNOLOGY (Iran)

d ILAM UNIVERSITY (Iran)

Author keywords

Disulfides; Heterogeneous conditions; Oxidation of thiols; Oxidative coupling of thiols; Oxone ; Potassium bromide; Potassium chloride; Sodium chloride; Tribromoisocyanuric acid (TBCA); Wet SiO2

Indexed keywords

EID: 36248942090 PISSN: 00094536 EISSN: None Source Type: Journal
DOI: 10.1002/jccs.200700159 Document Type: Article

Times cited : (28)

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- A general procedure. A suspension of compound 1, Oxone® and wet SiO2, 50% w/w, in CH2Cl2 (10 mL) or TBCA} was stirred at room temperature for a specific time (molar ratio of reagents and needed reactions times indicated in the Table, The progress of the reaction was monitored by TLC. After disappearance of the starting materials 1 on TLC, reaction mixture was filtered off. The residue was washed with CH2Cl2 (2 x 10 mL, Anhydrous Na 2SO4 (1 g) was added to the filtrate and filtered off after 10 min. Dichloromethane was removed and product 2 obtained. Spectral data for 2: 2a-IR (Nujul, 3080, 1575, 1472, 738 cm -1; 1H NMR (90 MHz, acetone-d6, δ (ppm, 7.4-7.2 (m, 10H, 2b-IR (KBr, 3061, 1589, 1486, 1229, 824 cm -1; 1H NMR (CDCl3, δ (ppm, 7.4 (m, 4H, 6.99 m, 4H, 2c
- 6), δ (ppm): 2.7 (t, 2H), 2.9 (t, 2H), 11 (b, 2H). 34. Khazaei, A.; Zolfigol, M. A.; Rostami, A. Synthesis 2004, 2959.

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