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2O: C, 67.23; H, 7.48; N, 6.82. Found: C, 66.71; H, 7.70; N, 6.79. Calcd for 2·1.5MeOH·0.5EtOH: C, 64.54; H, 7.28; N, 6.47. Found: C, 64.17; H, 7.24; N, 6.50.
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2O: C, 67.23; H, 7.48; N, 6.82. Found: C, 66.71; H, 7.70; N, 6.79. Calcd for 2·1.5MeOH·0.5EtOH: C, 64.54; H, 7.28; N, 6.47. Found: C, 64.17; H, 7.24; N, 6.50.
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31
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35848933762
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Crystal data: [Fe{H(3,5-tBu2)salbh, 3,5- tBu2)salbh}]·EtOH·H2O (1·EtOH·H2O, C46H61N 4O6Fe, M, 821.84, monoclinic, space group P21/c, a, 13.3760(3) Å, b, 31.0562(6) Å, c, 11.8253(2) Å, β, 91.458(1)°, U, 4910.73(17) Å3, Z, 4, T, 293(2) K, Dc, 1.112 Mg m-3, μ, 0.353 mm-1, reflections measured, 10 390, reflections unique, 5522, reflections observed [I > 2σ(I, 3680, R1, 0.0932, wR2, 0.2534; Fe{H(3,5-tBu2)salbh}2]Cl·1. 5MeOH·0.5EtOH 2·1.5MeOH·0.5EtOH, C 46.5H63N4O6ClFe, M, 865.34, triclinic, space group P1, a
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-1, reflections measured = 16 128, reflections unique = 10 997, reflections observed [I > 2σ(I)] = 8532, R1 = 0.0620, wR2 = 0.1602. The hydrogen atoms of the keto form of the ligand (H2a and H2b) were located from the difference Fourier map.
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