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25
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35748959222
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note
-
2-Hexyl-benzo[b]thiophene 4b was prepared from 4a via lithiation using n-BuLi/THF at -78 °C followed by quenching with hexyl bromide. N-n-Hexylbenzo[b]pyrrole 4c was prepared via 1-hexylation of indole under PTC conditions.
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-
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26
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35748939878
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note
-
3): δ 77.72, 122.00, 123.06 (2C), 124.74, 125.09, 125.94, 126.30, 126.72, 129.73, 131.04, 134.35, 137.16, 140.84, 148.11, 170.18.
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-
-
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27
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-
35748945889
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-
note
-
2 atmosphere.
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-
-
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28
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-
35748935409
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-
note
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2: C, 76.90; H, 7.46; N, 2.80, S, 12.83. Found: C, 76.78; H, 7.62; N, 2.63, S, 12.96.
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-
-
-
29
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35748986595
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-
note
-
6: C, 72.34; H, 5.37; S, 22.29. Found: C, 72.50; H, 5.30; S, 22.20.
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-
-
-
30
-
-
35748930120
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-
note
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3: C, 66.99; H, 3.21; S, 25.55. Found: C, 66.86; H, 3.41; S, 25.71.
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-
-
-
31
-
-
35748931351
-
-
note
-
4: C, 67.33; H, 3.14; N, 2.91, S, 26.63. Found: C, 67.23; H, 3.24; N, 3.12, S, 26.39.
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-
-
-
32
-
-
35748951791
-
-
note
-
3: C, 74.82; H, 6.10; N, 2.42, S, 16.65. Found: C, 74.62; H, 6.28; N, 2.22, S, 16.84.
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