-
1
-
-
0021818675
-
-
Smith, G. P. Science, 1985, 228, 1315.
-
(1985)
Science
, vol.228
, pp. 1315
-
-
Smith, G.P.1
-
3
-
-
0038064430
-
-
Van der Lely Aart, J.; De Herder Wouter, W.; Krenning Eric, P. Kwekkeboom Dik, J. Endocrine, 2003, 20, 307.
-
(2003)
Endocrine
, vol.20
, pp. 307
-
-
Van der Lely Aart, J.1
De Herder Wouter, W.2
Krenning Eric, P.3
Kwekkeboom Dik, J.4
-
7
-
-
0000318227
-
-
Yu, H. M.; Chen, S. T.; Wang, K. T. J. Org. Chem., 1992, 57, 4781.
-
(1992)
J. Org. Chem
, vol.57
, pp. 4781
-
-
Yu, H.M.1
Chen, S.T.2
Wang, K.T.3
-
9
-
-
35648999991
-
-
De Leon-Rodriguez, L. M.; Kovacs, Z.; Sherry, A. D. Lett. Org. Chem., 2005, 2, 160.
-
(2005)
Lett. Org. Chem
, vol.2
, pp. 160
-
-
De Leon-Rodriguez, L.M.1
Kovacs, Z.2
Sherry, A.D.3
-
10
-
-
0003463148
-
-
Third ed, John Wiley & Sons, Inc
-
Greene, T. W.; Wuts, P. G. M. Protective Groups in Organic Chemistry, Third ed., John Wiley & Sons, Inc., 1999.
-
(1999)
Protective Groups in Organic Chemistry
-
-
Greene, T.W.1
Wuts, P.G.M.2
-
11
-
-
0034117685
-
-
Bhorade, R.; Weissleder, R.; Nakakoshi, T.; Moore, A.; Tung, C.-H. Bioconjugate Chem., 2000, 11, 301.
-
(2000)
Bioconjugate Chem
, vol.11
, pp. 301
-
-
Bhorade, R.1
Weissleder, R.2
Nakakoshi, T.3
Moore, A.4
Tung, C.-H.5
-
12
-
-
35649021238
-
-
Nα-(9-Fluorenylmethoxycarbonyl)-p-nitro-L-phenylalanine (2) p-nitro-L-phenylalanine (1.0g, 4.73 mmol) was dissolved in a mixture of Dioxane (5 mL) and 10% Na2CO3 solution (10 mL, The solution temperature was lowered at 0 °C and 9-Fluorenylmethyl chloroformate (1.68 g, 1.05 equiv, in Dioxane (5 mL) was slowly added. Reaction flask was flushed with Nitrogen, sealed and reaction was allowed to stand overnight. Solution was concentrated under reduced pressure, DI water was added (10mL) and pH adjusted to 2.0 by addition of HCl conc. giving the formation of solids. Solids were filtered out and then taken into Ethyl Acetate (200 mL) upon heating and washed with DI water (2x 200 mL, Organic phase was dried with Na2SO4, filtered, solvent evaporated and solids dried under vacuum yielding 1.58 g (85, of a light yellow solid. m.p.=255°C 1H NMR (200 MHz, DMSO-d6) 8.0(d, 2H, J= 8.4 Hz, arom, 7.8d, 2H,J, 8.4 Hz
-
6: C, 72.07; H, 6.05; N, 4.94. Found: C, 71.95; H, 6.12; N, 500.
-
-
-
-
13
-
-
37049089078
-
-
Bycroft, B. W.; Chan, W. C.; Chharbra, S. R.; Hone, N. D. J. Chem. Soc. Chem. Commun., 1993, 778.
-
(1993)
J. Chem. Soc. Chem. Commun
, pp. 778
-
-
Bycroft, B.W.1
Chan, W.C.2
Chharbra, S.R.3
Hone, N.D.4
-
14
-
-
35649008355
-
-
Microwave assisted reactions were carried out in a Microwave Accelerated Reaction System, Mars X, Version 047928, CEM corporation. Reaction conditions are: Swelling, 1 pulse of 120 sec at 15W; Coupling, 4 pulses of 15 sec at 100 W; Capping, 3 pulses of 30 see at 75 W; Deprotection, 3 pulses of 30 see at 75W. Cooling was applied after each pulse to keep reaction temperature below 60°C.
-
Microwave assisted reactions were carried out in a Microwave Accelerated Reaction System, Mars X, Version 047928, CEM corporation. Reaction conditions are: Swelling, 1 pulse of 120 sec at 15W; Coupling, 4 pulses of 15 sec at 100 W; Capping, 3 pulses of 30 see at 75 W; Deprotection, 3 pulses of 30 see at 75W. Cooling was applied after each pulse to keep reaction temperature below 60°C.
-
-
-
-
17
-
-
0025602549
-
-
Abrams, M. J.; Juweid, M.; TenKate, C. I.; Schwartz, D. A.; Hauser, M. M.; Gaul, F. E.; Fuccello, A. J.; Rubin, R. H.; Strauss, H. W.; Fischman, A. J. J. Nucl. Med., 1990, 31, 2022.
-
(1990)
J. Nucl. Med
, vol.31
, pp. 2022
-
-
Abrams, M.J.1
Juweid, M.2
TenKate, C.I.3
Schwartz, D.A.4
Hauser, M.M.5
Gaul, F.E.6
Fuccello, A.J.7
Rubin, R.H.8
Strauss, H.W.9
Fischman, A.J.10
-
19
-
-
1642322987
-
-
De Leon-Rodriguez, L. M.; Kovacs, Z.; Dieckmann, G. R.; Sherry, A. D. Chem. - Eur. J., 2004, 10, 1149.
-
(2004)
Chem. - Eur. J
, vol.10
, pp. 1149
-
-
De Leon-Rodriguez, L.M.1
Kovacs, Z.2
Dieckmann, G.R.3
Sherry, A.D.4
-
20
-
-
0032813187
-
-
Maruyama, K.; Nagasawa, H.; Suzuki, A. Peptides, 1999, 20, 881.
-
(1999)
Peptides
, vol.20
, pp. 881
-
-
Maruyama, K.1
Nagasawa, H.2
Suzuki, A.3
|