Large-quantity single crystal synthesis of TPA-ZSM-5 using KOH as a mineralizer

Zeitschrift fur Kristallographie

Volumn 222, Issue 10, 2007, Pages 551-554

  Kamiya, Natsumi ^a   Torii, Yuki ^a   Sasaki, Masahiro ^a   Nishi, Koji ^a   Yokomori, Yoshinobu ^a  

^a NATIONAL DEFENSE ACADEMY   (Japan)

Author keywords

Analcime; Lermer's method; Single crystal structure analysis; Synthesis; X ray diffraction; Zeolite W; ZSM 5

Indexed keywords

EID: 35648980455     PISSN: 00442968     EISSN: None     Source Type: Journal    
DOI: 10.1524/zkri.2007.222.10.551     Document Type: Article

References (27)

1. Nishi, K.; Hidaka, A.; Yokomori, Y.: Structure of toluene 6.4-ZSM-5 and the toluene disproportionation reaction on ZSM-5. Acta Crystallogr. B61 (2005) 160-163.
2. van Koningsveld, H.; Jansen, J. C.: Single crystal structure analysis of zeolite H-ZSM-5 loaded with naphthalene. Micropor. Mater. 6 (1996) 159-167.
3. van Koningsveld, H.; Jansen, J. C.; Man, A. J. M.: Single-crystal structure analysis and energy minimizations of a MFI-type zeolite at low p-dichlorobenzene sorbate loading. Acta Crystallogr. B52 (1996) 131-139.
4. van Koningsveld, H.; Jansen, J. C.; van Bekkum, H.: The Location of p-Dichlorobenzene in a Single Crystal of Zeolite H-ZSM-5 at High Sorbate Loading. Acta Crystallogr. B52 (1996) 140-144.
5. Reck, G.; Kornatowski, J.; Hill, W.; Caro, J.: Structure of Dipole Chains in an MFI Type Molecular Sieve. J. Phys. Chem. 100 (1996) 1698-1704.
6. van Koningsveld, H.; Koegler, J. H.: Preparation and structure of crystal of zeolite H-ZSM-5 loaded with p-nitroaniline. Micropor. Mater. 9 (1997) 71-81.
7. 2O. Zeolites 3 (1983) 57-62.
8. Kornatowski, J.: Growth of large crystals of ZSM-5 zeolite. Zeolites 8 (1988) 77-78.
9. Daqing, Z.; Shilun, Q.; Wenqin, P.: Synthesis of Large Single Crystals of Pentasil-type Silica Zeolites from Non-alkaline Medium. J. Chem. Soc., Chem. Comm. (1990) 1313-1314.
10. Mueller, U.; Unger, K. K.: Preliminary studies on the synthesis of alkaline-free large crystals of ZSM-5. Zeolites 8 (1988) 154-156.
11. Shimizu, S.; Hamada, H.: Synthesis of Giant Zeolite Crystals by a Bulk-Material Dissolution Technique. Angew. Chem. Int. Ed. 38 (1999) 2725-2727.
12. Lermer, H.; Draeger, M.; Steffen, J.; Unger, K. K.: Synthesis and structure refinement of ZSM-5 single crystals. Zeolites 5 (1985) 131-134.
13. van Koningsveld, H.; van Bekkum, H.; Jansen, J. C.: On the Location and Disorder of the Tetrapropylammonium (TPA) Ion in Zeolite ZSM-5 with Improved Framework Accuracy. Acta Crystallogr. B43 (1987) 127-132.
14. Chen; S. Z.; Huddersman, K.; Keir, D.; Rees, L. V. C.: Synthesis of large uniform crystals of ZSM-5. Zeolites 8 (1988) 106-109.
15. Geus, E. R.; van Bekkum, H.: Calcination of large MFI-type single crystals, Part 2: Crack formation and thermomechanical properties in view of the preparation of zeolite membranes. Zeolites 15 (1995) 333-341.
16. Althoff, R.; Schulz-Dobrick, B.; Schüth, F.; Unger, K.: Controlling the spatial distribution of aluminum in ZSM-5 crystals. Micropor. Mater. 1 (1993) 207-218.
17. Yokomori, Y.; Idaka, S.: The structure of TPA-ZSM-5 with Si/Al = 23. Micropor. Mesopor. Mater. 28 (1999) 405-413.
18. Thoma, S. G.; Nenoff, T. M.: A novel synthesis of zeolite W using organometallic precursors. Micropor. Mesopor. Mater. 34 (2000) 301-306.
19. Yokomori, Y.; Idaka, S.: The crystal structure of analcime. Micropor. Mesopor. Mater. 21 (1998) 365-370.
20. Mazzi, F.; Galli, E.; Gottardi, G.: The crystal structure of tetragonal leucite. Am. Mineral. 61 (1976) 108-115.
21. 12, a Pollucite Analogue. Acta Crystallogr. C47 (1991) 237-241.
22. Shannon, R. D.; Prewitt, C. T.: Effective ionic radii in oxides and fluorides. Acta Crystallogr. B25 (1969) 925-946.
23. Barrer, R. M.; White, E. A. D.: The hydrothermal chemistry of silicates. Part II. Synthetic crystalline sodium aluminosilicates. J. Chem. Soc. (1952) 1561-1571.
24. 2O system. Econ. Geol. 52 (1957) 169-179.
25. 2O. J. Chem. Soc. (1961) 983-999.
26. Breck, D. W.: Zeolite Molecular Sieves. John Wiley, New York (1974).
27. Koegler, J. H.; van Bekkum, H.; Jansen, J. C.: Growth model of oriented crystals of zeolite Si-ZSM-5. Zeolites 19 (1997) 262-269.