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Volumn 46, Issue 21, 2007, Pages 8487-8489

Novel coordination polymers based on the tetrathioterephthalate dianion as the bridging ligand

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EID: 35648967070     PISSN: 00201669     EISSN: None     Source Type: Journal    
DOI: 10.1021/ic701414v     Document Type: Article
Times cited : (35)

References (28)
  • 11
    • 33747792376 scopus 로고    scopus 로고
    • (a) Xu, Z. Coord. Chem. Rev. 2006, 250, 2745-2757.
    • (2006) Coord. Chem. Rev , vol.250 , pp. 2745-2757
    • Xu, Z.1
  • 17
    • 35649022332 scopus 로고    scopus 로고
    • 3.
    • 3.
  • 18
    • 0141520591 scopus 로고    scopus 로고
    • We have identified C-H⋯S hydrogen bonds using common criteria. These are the sum of the van der Waals radii for H and S (H, 1.20 Å; S, 1.80 Å) and the angles C-H⋯S (θ) and H-S⋯C (φ, See: (a) Cosp, A, Larrosa, I, Anglada, J. M, Bofill, J. M, Romea, P, Urpi, F. Org. Lett. 2003, 5, 2809
    • We have identified C-H⋯S hydrogen bonds using common criteria. These are the sum of the van der Waals radii for H and S (H, 1.20 Å; S, 1.80 Å) and the angles C-H⋯S (θ) and H-S⋯C (φ). See: (a) Cosp, A.; Larrosa, I.; Anglada, J. M.; Bofill, J. M.; Romea, P.; Urpi, F. Org. Lett. 2003, 5, 2809.
  • 23
    • 33646260300 scopus 로고    scopus 로고
    • Chalcogenocarboxylic Acid Derivatives
    • Springer: Berlin
    • Kano, N.; Kawashima, T. Chalcogenocarboxylic Acid Derivatives. Topics in Current Chemistry; Springer: Berlin, 2005; Vol. 251, pp 141-180.
    • (2005) Topics in Current Chemistry , vol.251 , pp. 141-180
    • Kano, N.1    Kawashima, T.2
  • 24
    • 35649013926 scopus 로고    scopus 로고
    • No Bragg peaks were observed in the PXRD pattern of the solid obtained after heating 1 at 180°C under an Ar flow.
    • No Bragg peaks were observed in the PXRD pattern of the solid obtained after heating 1 at 180°C under an Ar flow.
  • 26
    • 35648942875 scopus 로고    scopus 로고
    • 2 is treated with something other than DMF coordinating molecules, such as pyridine and small alkylamines, new crystalline materials are formed. The corresponding PXRD patterns are provided in the Supporting Information
    • analysis
    • When 2 is treated with something other than DMF coordinating molecules, such as pyridine and small alkylamines, new crystalline materials are formed. The corresponding PXRD patterns are provided in the Supporting Information. However, the atomic structures of these solids are currently unknown because the quality of the crystals does not allow single-crystal X-ray analysis.
    • However, the atomic structures of these solids are currently unknown because the quality of the crystals does not allow single-crystal X-ray
    • When1
  • 27
    • 35649002145 scopus 로고    scopus 로고
    • A possible porosity in 2 was investigated by recording the nitrogen adsorption isotherm at 77 K. The results show that there is no permanent porosity, accessible at least by this probe molecule (see Figure S4 in the Supporting Information).
    • A possible porosity in 2 was investigated by recording the nitrogen adsorption isotherm at 77 K. The results show that there is no permanent porosity, accessible at least by this probe molecule (see Figure S4 in the Supporting Information).


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