Isolation and purification of lignans from Magnolia biondii Pamp by isocratic reversed-phase two-dimensional liquid chromatography following microwave-assisted extraction

Journal of Separation Science

Volumn 30, Issue 15, 2007, Pages 2370-2381

  Zhao, Weiquan ^a   Zhou, Tingting ^a   Fan, Guorong ^a   Chai, Yifeng ^a   Wu, Yutian ^a  

^a SECOND MILITARY MEDICAL UNIVERSITY   (China)

Author keywords

Lignan; Magnolia biondii Pamp; Microwave assisted extraction; Preparative chromatography; Two dimensional chromatography

Indexed keywords

LIGNAN; MAGNOLIA BONDII PAMP; MICROWAVE-ASSISTED EXTRACTION;

ETHERS; EXTRACTION; GRADIENT METHODS; LIQUID CHROMATOGRAPHY; PURIFICATION; SOLVENTS;

PLANTS (BOTANY);

DEMETHOXYASCHANTIN; EPIMAGNOLIN A; FARGESIN; LIGNAN; LIGNAN DERIVATIVE; MAGNOLIA BIONDII EXTRACT; MAGNOLIN; PINORESINOL DIMETHYL ETHER; PLANT EXTRACT; UNCLASSIFIED DRUG;

ARTICLE; CARBON NUCLEAR MAGNETIC RESONANCE; CHINESE MEDICINE; CHROMATOGRAPHY; CONTROLLED STUDY; DRUG ISOLATION; DRUG PURIFICATION; DRUG STRUCTURE; ELUTION; EXTRACTION; FLOWER; HERBAL MEDICINE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; MAGNOLIA BIONDII; MAGNOLIACEAE; MASS SPECTROMETRY; MICROWAVE ASSISTED EXTRACTION; NONHUMAN; PRIORITY JOURNAL; PROTON NUCLEAR MAGNETIC RESONANCE; REVERSED PHASE LIQUID CHROMATOGRAPHY; TIME; TWO DIMENSIONAL CHROMATOGRAPHY; ULTRAVIOLET SPECTROSCOPY;

CHEMISTRY, ANALYTICAL; CHROMATOGRAPHY; CHROMATOGRAPHY, HIGH PRESSURE LIQUID; CHROMATOGRAPHY, LIQUID; FLOWERS; LIGNANS; MAGNETIC RESONANCE SPECTROSCOPY; MAGNOLIA; MICROWAVES; MODELS, CHEMICAL; PLANT EXTRACTS; SOLVENTS; TIME FACTORS;

MAGNOLIA BIONDII;

EID: 35648954656     PISSN: 16159306     EISSN: 16159314     Source Type: Journal    
DOI: 10.1002/jssc.200700098     Document Type: Article

References (22)

1. China Pharmacopoeia Committee, Pharmacopoeia of the People's Republic of China, The first Division of 2000 English Edition, China Chemical Industry Press, Beijing, 2000, p. 143.
2. Pan, J. X., Hensens, O., Zink, D., Chang, M. N., Hwang, S. B., Phytochemistry 1987, 26, 1377-1379.
3. Ma, Y. L., Huang, Q. L., Han, G. Q., Phytochemistry 1996, 41, 287-288.
4. Miyazawa, M., Ishikawa, Y., Kasahara, H., Yamanaka, J., Kameoka, H., Phytochemistry 1994, 35, 611-613.
5. Miyazawa, M., Kasahara, H., Kameoka, H., Phytochemistry 1992, 31, 3666-3668.
6. Castellar, M. R., Mondjano, H., Manjón, A, Iborra, J. L., J. Chromatogr. 1993, 648, 187-190.
7. Shin, T. S., Godber, J. S., J. Chromatogr. 1994, 678, 49-58.
8. Lu, T. S., Saito, N., Yokoi, M., Shigihara, A., Honda, T., Phytochemistry 1992, 31, 659- 663.
9. Goiffon, J. P., Brun, M., Bourrier, M. J., J. Chromatogr. 1991, 537, 101-121.
10. Snyder, L. R., Principles of Adsorption Chromatography, Marcel Dekker, New York 1968.
11. Jandera, P., Churacek, J., Gradient Elution in Column Liquid Chromatography, Elsevier, Amsterdam 1985.
12. Snyder, L. R., Stadalius, M. A., in: Horvath, C. (Ed.), High Performance Liquid Chromatography-Advances and Perspectives, Vol. 4, Academic Press, New York 1986, pp. 208-316.
13. Sweeney, A. P., Shalliker, R. A., J. Chromatogr. A 2002, 968, 41-52.
14. Gray, M., Dennis, G. R., Wormell, P, Shalliker, R. A., Slonecker, P., J. Chromatogr. A 2002, 975, 285-297.
15. Wong, V., Shalliker, R. A., J. Chromatogr. A 2004, 1036, 15-24.
16. Miller, L., Bergeron, R., J. Chromatogr. 1993, 648, 381-388.
17. Miller, L., Weyker, C., J. Chromatogr. 1990, 511, 97-107.
18. Brocks, D. R., Pasutto, F. M., Jamali, F., J. Chromatogr. 1992, 581, 83-92.
19. Gray, M.J., Dennis, G. R., Slonecker, P.J., Shalliker, R. A., J. Chromatogr. A 2004, 1028, 247-257.
20. Gray, M.J., Dennis, G. R., Slonecker, P.J., Shalliker, R. A., J. Chromatogr. A 2004, 1041, 101-110.
21. Matsui, T., Tamaya, K., Kawasaki, T., Osajima, Y., J. Chromatogr. B 1999, 729, 89-96.
22. Cortes, H. J. (Ed.), L. D. Rothman, Multidimensional Chromatography, Marcel Dekker, New York 1990, pp. 219-248.