PbS nanoparticles: Synthesis and size determination by x-ray diffraction

Inorganic Materials

Volumn 40, Issue 1, 2004, Pages 3-10

  Belova, N S ^a   Rempel', A A ^a  

^a INSTITUTE OF SOLID STATE CHEMISTRY   (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

LEAD; SULFUR;

ANALYTIC METHOD; AQUEOUS SOLUTION; ARTICLE; ATOMIC PARTICLE; CRYSTAL; MATHEMATICAL ANALYSIS; NANOPARTICLE; PARTICLE SIZE; PRECIPITATION; X RAY DIFFRACTION;

EID: 3543022126     PISSN: 00201685     EISSN: None     Source Type: Journal    
DOI: 10.1023/B:INMA.0000012170.32403.1c     Document Type: Article

References (38)

1. Gusev, A.I. and Rempel', A.A., Nanokristallicheskie materialy (Nanocrystalline Materials), Moscow: Fizmatlit, 2000.
2. Khairutdinov, R.F., Chemistry of Semiconductor Nanoparticles, Usp. Khim., 1998, vol. 67, no. 2, pp. 125-139.
3. Alivisatos, A.P., Semiconductor Clusters, Nanocrystals, and Quantum Dots, Science (Washington, D. C., 1883-), 1996, vol. 271, no. 5251, pp. 933-937.
4. Tolbert, S.H. and Alivisatos, A.P., Size Dependence of a First Order Solid-Solid Transition: The Wurtzite to Rock Salt Transformation in CdSe Nanocrystals, Science (Washington, D. C., 1883-), 1994, vol. 265, no. 5170, pp. 373-376.
5. Goldstein, A.N., Echer, C.M., and Alivisatos, A.P., Melting in Semiconductor Nanocrystals, Science (Washington, D. C., 1883-), 1992, vol. 256, no. 5062, pp. 1425-1427.
6. Klein, D.L., Roth, R., Lim, A.K.L., et al., A Single-Electron Transistor Made from a Cadmium Selenide Nanocrystal, Nature (London), 1997, vol. 389, no. 6652, pp. 699-701.
7. Kouwenhoven, L.P. and McEuen, P.L., Single Electron Transport through a Quantum Dot, Nanotechnology, Timp, G., Ed., Berlin: Springer, 1999, pp. 471-536.
8. Wise, F.W., Lead Salt Quantum Dots: The Limit of Strong Quantum Confinement, Acc. Chem. Res., 2000, vol. 33, no. 11, pp. 773-780.
9. Kang, I. and Wise, F.W., Electronic Structure and Optical Properties of PbS and PbSe Quantum Dots, J. Am. Opt. Soc., 1997, vol. 14, no. 7, pp. 1632-1646.
10. Kitaev, G.A., Bol'shchikova, T.P., Fofanov, G.M., et al., Thermodynamic Assessment of Conditions for Metal Sulfide Precipitation from Aqueous Solutions by Thiourea, in Kinetika i mekhanizm obrazovaniya tverdoi fazy (Kinetics and Mechanisms of the Formation of Solid Phases), Sverdlovsk: Ural. Politekhnicheskii Inst., 1968, pp. 113-126.
11. Prigogine, I. and Defay, R., Thermodynamique chimique conformément aux méthodes de Gibbs et De Donder, Paris: Dunod, 1951. Translated under the title Khimicheskaya termodinamika, Novosibirsk: Nauka, 1966.
12. Prigogine, I. and Defay, R., Thermodynamique chimique conformément aux méthodes de Gibbs et De Donder, Paris: Dunod, 1951. Translated under the title Khimicheskaya termodinamika, Novosibirsk: Nauka, 1966.
13. Butler, J.N., Ionic Equilibrium: A Mathematical Approach, Reading: Addison-Wesley, 1964. Translated under the title Ionnye ravnovesiya, Leningrad: Khimiya, 1973.
14. Butler, J.N., Ionic Equilibrium: A Mathematical Approach, Reading: Addison-Wesley, 1964. Translated under the title Ionnye ravnovesiya, Leningrad: Khimiya, 1973.
15. Noda, Y., Ohba, S., Sato, S., and Saito, Y., Charge Distribution and Atomic Thermal Vibration in Lead Chalcogenide Crystals, Acta Crystallogr., Sect. B: Struct. Sci., 1983, vol. 39, no. 3, pp. 312-317.
16. Rietveld, H.M., A Profile Refinement Method for Nuclear and Magnetic Structures, J. Appl. Crystallogr., 1969, vol. 2, no. 2, pp. 65-71.
17. Klug, H.P. and Alexander, L.E., X-ray Diffraction Procedures, New York: Wiley, 1974, 2nd ed.
18. Warren, B.E., X-ray Diffraction, New York: Dover, 1990.
19. 5, Phys. Rev. B: Condens. Matter, 2001, vol. 63, pp. 1-7.
20. x Solid Solutions, Neorg. Mater., 2003, vol. 39, no. 1, pp. 49-53 [Inorg. Mater. (Engl. Transl.), vol. 39, no. 1, pp. 43-46].
21. x Solid Solutions, Neorg. Mater., 2003, vol. 39, no. 1, pp. 49-53 [Inorg. Mater. (Engl. Transl.), vol. 39, no. 1, pp. 43-46].
22. Hall, W.H., X-ray Line Broadening in Metals, Proc. Phys. Soc., Sect. A (London), 1949, vol. 62, part 11, no. 359, pp. 741-743.
23. Hall, W.H. and Williamson, G.K., The Diffraction Pattern of Cold Worked Metals: I. The Nature of Extinction, Proc. Phys. Soc., Sect. B (London), 1951, vol. 64, part 11, no. 383, pp. 937-946.
24. Williamson, G.K. and Hall, W.H., X-ray Line Broadening from Filed Aluminium and Wolfram, Acta. Metall., 1953, vol. 1, no. 1, pp. 22-31.
25. James, R.W., The Optical Principles of the Diffraction of X-rays, Woodbridge: Ox Bow, 1982.
26. Nelson, J.B. and Riley, D.P., An Experimental Investigation of Extrapolation Methods in the Derivation of Accurate Unit-Cell Dimensions of Crystals, Proc. Phys. Soc. (London), 1945, vol. 57, part 3, no. 321, pp. 160-177.
27. Azároff, L. V. and Buerger, M., The Powder Method in X-ray Crystallography, New York: McGraw-Hill, 1958. Translated under the title Metod poroshka v rentgenografii, Moscow: Inostrannaya Literatura, 1961.
28. Azároff, L. V. and Buerger, M., The Powder Method in X-ray Crystallography, New York: McGraw-Hill, 1958. Translated under the title Metod poroshka v rentgenografii, Moscow: Inostrannaya Literatura, 1961.
29. 2 and Deviations from Stoichiometry in Lead Chalcogenides, Zh. Fiz. Khim., 1974, vol. 68, no. 5, pp. 1187-1189.
30. Kroger, F.A., The Chemistry of Imperfect Crystals, Amsterdam: North Holland, 1964. Translated under the title Khimiya nesovershennykh kristallov, Moscow: Mir, 1969.
31. Kroger, F.A., The Chemistry of Imperfect Crystals, Amsterdam: North Holland, 1964. Translated under the title Khimiya nesovershennykh kristallov, Moscow: Mir, 1969.
32. 5, Neorg. Mater., 2001, vol. 37, no. 6, pp. 716-727 [Inorg. Mater. (Engl. Transl.), vol. 37. no. 7, pp. 603-612].
33. 5, Neorg. Mater., 2001, vol. 37, no. 6, pp. 716-727 [Inorg. Mater. (Engl. Transl.), vol. 37. no. 7, pp. 603-612].
34. Delmon, B., Introduction à la cinétique hétérogène, Paris: Technip, 1969. Translated under the title Kinetika geterogennykh reaktsii, Moscow: Mir, 1972.
35. Delmon, B., Introduction à la cinétique hétérogène, Paris: Technip, 1969. Translated under the title Kinetika geterogennykh reaktsii, Moscow: Mir, 1972.
36. Uritskaya, A.A., Kitaev, G.A., and Belova, N.S., Kinetics of Cadmium Sulfide Precipitation from Aqueous Thiourea Solutions, Zh. Prikl. Khim. (S.-Peterburg), 2002, vol. 75, no. 5, pp. 864-865.
37. Kitaev, G. A. and Khvorenkova, A.Zh., Kinetics of Lead Selenide Formation in Aqueous Solutions of Sodium Selenosulfate, Zh. Prikl. Khim. (S.-Peterburg), 1999, vol. 72, no. 9, pp. 1440-1443.
38. Pintilie, I., Pentia, E., Pintilie, L., et al., Growth and Characterization of PbS Deposited on Ferroelectric Ceramics, J. Appl. Phys., 1995, vol. 78, no. 3, pp. 1713-1718.