Chemical synthesis of graphite bis(perfluoropinacolato)borate and graphite bis(hexafluorohydroxyisobutyrato)borate intercalation compounds

Carbon

Volumn 45, Issue 13, 2007, Pages 2672-2677

  Katinonkul, Watcharee ^a   Lerner, Michael M ^a  

^a OREGON STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

GRAPHITE; HYDROFLUORIC ACID; NEGATIVE IONS; OXIDATION; SYNTHESIS (CHEMICAL); THERMOGRAVIMETRIC ANALYSIS; X RAY POWDER DIFFRACTION;

ANHYDROUS HYDROFLUORIC ACIDS; CHEMICAL OXIDATION; FLAKY GRAPHITES; GRAPHITE CHELATE BORATE INTERCALATION COMPOUNDS;

INTERCALATION;

EID: 35349023230     PISSN: 00086223     EISSN: None     Source Type: Journal    
DOI: 10.1016/j.carbon.2007.07.020     Document Type: Article

References (34)

1. Billaud D., Pron A., Vogel F., and Herold A. Intercalation of pyrographite by nitryl and nitrosyl salts. Mater Res Bull 15 11 (1980) 1627-1634
2. Billaud D., Pron A., and Vogel F. Electrical resistivity and X-ray spacings of graphite tetrafluoroborate, hexafluorophosphate and hexafluoroantimonate compounds synthesized from nitronium salts. Synth Met 2 (1980) 177-184
3. Forsman W., and Mertwoy H. Intercalation of graphite by nitrosonium ion attack. Carbon 20 3 (1982) 255-256
4. Chenite A., and Billaud D. Novel graphite-hexafluoroarsenate intercalation compounds. Carbon 20 2 (1982) 120-121
5. Billaud D., and Chenite A. Electrochemical intercalation of fluorides into pyrographite. J Power Sources 13 (1984) 1-7
6. 3 H. Mater Sci Eng 31 (1977) 87-89
7. Ruisinger B., and Boehm H. Intercalation of perfluorobutanesulfonic acid in graphite. Carbon 31 7 (1993) 1131-1137
8. Boehm H., Helle W., and Ruisinger B. Graphite salts with perfluoroalkanesulfonic acids and alkanesulfonic acids. Synth Met 23 (1988) 395-400
9. Ruisinger B., and Boehm H. Two different intercalate structures in the intercalation compounds of graphite with perfluorobutanesulfonic acid. Angew Chem Int Ed Engl 26 (1987) 253-255
10. Zhang Z., and Lerner M.M. Preparation, characterization, and exfoliation of graphite perfluorooctanesulfonate. Chem Mater 8 1 (1996) 257-263
11. 6 in hydrofluoric acid or mixed acid solution. Chem Mater 11 4 (1999) 1100-1109
12. -. Carbon 42 14 (2004) 2981-2987
13. Bourelle E., Douglade J., and Metrot A. Electrochemical exfoliation of graphite in trifluoroacetic media. Mol Cryst Liq Cryst Sci Technol Sect A 244 (1994) 227-232
14. Zhang X., Sukpirom N., and Lerner M.M. Graphite intercalation of bis(trifluoromethane-sulfonyl)imide and other anions with perfluoroalkanesulfonyl substituents. Mater Res Bull 34 3 (1999) 363-372
15. Zhang X., and Lerner M.M. Graphite intercalation with perfluoroalkylsulfonates, and perfluoroalkylsulfonyl imides and methide. Mol Cryst Liq Cryst Sci Technol Sect A 340 (2000) 37-42
16. Davies J., and Eric D. Spectroscopic studies on organic molecules intercalated into clays. J Inclusion Phenom Mol Recognit Chem 24 (1996) 133-147
17. Kloprogge J.T. Synthesis of smectites and porous pillared clay catalysts: review. J Porous Mater 5 1 (1998) 5-41
18. Ding Z., Kloprogge J.T., Frost R.L., Lu G.Q., and Zhu H.Y. Porous clays and pillared clays-based catalysts.Part 2: A review of the catalytic and molecular sieve applications. J Porous Mater 8 4 (2001) 273-293
19. Vaia R.A., Vasudevan S., Krawiec W., Scanlon L.G., and Giannelis E.P. New polymer electrolyte nanocomposites Melt intercalation of poly(ethylene oxide) in mica-type silicates. Adv Mater (Weinheim, Ger.) 7 (1995) 154-156
20. Kim D.W., Blumstein A., Kumar J., and Tripathy S.K. Layered aluminosilicate/chromophore nanocomposites and their electrostatic layer-by-layer assembly. Chem Mater 13 2 (2001) 243-246
21. Lee T.W., Park O.O., Kim J.J., Hong J.M., and Kim Y.C. Efficient photoluminescence and electroluminescence from environmentally stable polymer/clay nanocomposites. Chem Mater 13 6 (2001) 2217-2222
22. Carrado K.A. Synthetic organo- and polymer-clays: preparation, characterization, and materials applications. Appl Clay Sci 17 (2000) 1-23
23. Alexandre M., and Dubois P. Polymer-layered silicate nanocomposites: preparation, properties and uses of a new class of materials. Mater Sci Eng R R28 1-2 (2000) 1-63
24. Yan W., and Lerner M.M. Preparation of a graphite bis(perfluoropinacolato)borate intercalation compound. J Electrochem Soc 150 9 (2003) D169-D173
25. - intercalation compound. J Electrochem Soc 151 2 (2004) J15-J20
26. Katinonkul W., and Lerner M.M. The first synthesis of a graphite bis(oxalato)borate intercalation compound. J Phys Chem Sol 68 3 (2007) 394-399
27. Combination fluoride electrodes instruction manual (2002), VWR International, Inc., Westchester, PA, USA
28. Allen M., Janzen A.F., and Willis C.J. Fully fluorinated alkoxides. IV. Derivatives of perfluoropinacol. Can J Chem 46 (1968) 3671-3677
29. Greenberg A.E., Clesceri L.S., and Eaton A.D. Standard methods for the examination of water and waste water. 18th ed. (1992), APHA & AWWA & WEF, Washington, DC p. 4-61-2
30. Nakajima T. Synthesis, structure, and physicochemical properties of fluorine-graphite intercalation compounds. In: Nakajima T. (Ed). Fluorine-carbon and fluoride-carbon materials-chemistry, physics and applications (1995), Marcel Dekker, New York 1-31
31. Besenhard J., and Fritz H. The electrochemistry of black carbons. Angew Chem Int Ed Engl 22 (1983) 950-975
32. - dans le graphite par methode electrochimique. Caracterisation des produits obtenus. Carbon 19 (1981) 193-198
33. Besenhard J., Wudy E., Moehwald H., Nickl J., Biberacher W., and Foag W. Anodic oxidation of graphite in sulfuric acid. Dilatometry, in situ X-ray diffraction, and impedance spectroscopy. Synth Met 7 (1983) 185-192
34. Katinonkul W., and Lerner M.M. Effect of reaction time on the composition of graphite bis(trifluoromethanesulfonyl)imide. Carbon 45 3 (2007) 499-504