Solid-state photodimerization of 1,2-bis(5′-pyrimidyl)ethene

Synthetic Communications

Volumn 37, Issue 21, 2007, Pages 3835-3839

  Bosch, Eric ^a   Matheny, Julie M ^a   Rath, Nigam ^b  

^a MISSOURI STATE UNIVERSITY   (United States)

^b UNIVERSITY OF MISSOURI ST LOUIS   (United States)

Author keywords

2+2 cycloaddition; Crystal structure; Photolysis; Solid state

Indexed keywords

1,2 BIS(5' PYRIMIDYL)ETHENE; ALKENE DERIVATIVE; CALIXARENE; CYCLOBUTANE DERIVATIVE; DICHLOROMETHANE; ETHYLENE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL STRUCTURE; CRYSTALLIZATION; DIMERIZATION; LIGHT; SOLID STATE; X RAY ANALYSIS;

EID: 35348957796     PISSN: 00397911     EISSN: 15322432     Source Type: Journal    
DOI: 10.1080/00397910701568785     Document Type: Article

References (7)

1. For a review, see Schmidt, G. M. J. Photodimerization in the solid state. Pure Appl. Chem. 1971, 27, 647-678.
2. Feldman, K. S.; Campbell, R. F. Efficient stereo- and regiocontrolled alkene photodimerization through hydrogen bond enforced preorganization in the solid state. J. Org. Chem. 1995, 60, 1924-1925.
3. For a brief review, see MacGillivray, L. R.; Papaefstathiou, G. S.; Friscic, T.; Varshney, D. B.; Hamilton, T. D. Template-controlled synthesis in the solid state. Topics Curr. Chem. 2005, 248, 201-221.
4. Yoshizawa, M.; Takeyama, Y.; Okana, T.; Fujita, M. Cavity-directed synthesis within a self-assembled coordination cage: Highly selective [2 + 2] cross-photodimerization of olefins. J. Am. Chem. Soc. 2003, 125, 3243-3247.
5. (a) Barnes, C. L.; Bosch, E. The quest for chain-link hydrogen-bonded capsules: Self-assembly of C-methyl calix[4]resorcinarene with 5,5′-bipyrimidine. Cryst. Growth Design 2005, 5, 1049-1053;
6. (b) Georgiev, I.; Barnes, C. L.; Draganjac, M.; Bosch, E. The quest for chain-link hydrogen-bonded capsules: Self-assembly of C-methyl calix[4]resorcinarene with 1,2-bis(5′-pyrimidyl)ethyne. Cryst. Growth Design 2004, 4, 235-239.
7. Matheny, J. M.; Bosch, E.; Barnes, C. L. Self-assembly of C-methyl calix[4]resorcinarene with 1,2-bis(5′-pyrimidyl)ethene. Cryst. Growth Design 2007, 7, 984-988.