HPLC-MS analysis of alkyl ethoxylates as alkyl ethoxysulfates: A new and reliable approach

Rivista Italiana delle Sostanze Grasse

Volumn 83, Issue 1, 2006, Pages 18-22

  Pratesi, C R ^a   Faccetti, L ^a   Andriollo, N ^a   Cassani, G ^a  

^a Research and Technology   (Italy)

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EID: 35148900152     PISSN: 00356808     EISSN: None     Source Type: Journal    
DOI: None     Document Type: Article

References (15)

1. P. JANDERA, M. HOLCAPEK, G. THEODORIDIS, Investigation of chromatographic behaviour of ethoxylated alcohol surfactants In normal-phase and reversed phase using high-performance liquid chromatographymass spectrometry. J. Chromatogr. A 813, 299 (1988)
2. S. K. HUANG, M. H. ROOD, The analysis of alkyl-capped alcohol ethoxylates by Atmospheric Pressure Chemical Ionization Mass Spectrometry. Rapid Commun. Mass Spectrom, 73, 1152 (1999)
3. X. C. WANG, Y. JIN, Analysis of carbon number distribution in alcohol ethoxylates by HPLC Electrospray Ionization Mass Spectrometry. Sepu 78, 332 (2000)
4. R. SPILKER, B. MENZEBACH, K. KUBE, Analysis of surfactants In formulations by Mass Spectrometry. Riv. Ital. Sostanze Grasse 78, 241 (2001)
5. H. BACHUS, H.-J. STAN, High-Performance Liquid Chromatography-UV analysis of aliphatic alcohol ethoxylates and their corresponding sulfates by esterification with 2-Furoyl-Chloride. Tenside Surfact. Deterg. 40, 10 (2003)
6. A. MARCOMINI, G. POIANA, C. CARTER, L. CAVALLI, G. CASSANI, M. LAZZARIN, Aerobic biodegradation of monobranched aliphatic alcohol polyethoxylates. Environ. Toxicol. Chem. 19, 555 (2000)
7. P. R. GEISSLER, Quantitative analysis of ethoxylated alcohols by Supercritical Fluid Chromatography. Anal. Chem. 66, 685 (1989)
8. H. T. KALINOSKI, A. JENSEN, Characterization of nonionic surfactants using Supercritical Fluid Chromatography and Carbon-13 Nuclear Magnetic Resonance Spectroscopy. J. Am. Oil Chem. Soc. 66, 1171 (1989)
9. A. E. JOHNSON, P R. GEISSLER, L. D. TALLEY, Determination of relative ethoxylation rate constants from Supercritical Fluid Chromatographic analysis of ethoxylated alcohols. Anal. Chem. 67, 123 (1990)
10. A. H. SILVER, H. T. KALINOSKI, Comparison of High-Temperature Gas Chromatography and Carbon Dioxide Supercritical Fluid Chromatography for the analysis of alcohol ethoxylates. J. Am. Oil Chem. Soc. 69, 599 (1992)
11. 1H NMR Coupling for the analysis of fatty alcohol ethoxylates. Polymer Bull. (Berlin) 8, 673 (1997)
12. C. E. HAMMOND, D. K. KUBIK, Determination of ethylene oxide content In n-alcohol ethoxylates by proton nuclear magnetic resonance spectroscopy. J. Am. Oil Chem. Soc. 77, 113 (1994)
13. nd ed. 1997, http://www.iupac.org/goldbook/P04908.pdf
14. T. Okada, Efficient evaluation of poly(oxyethylene) complex formation with alkali-metal cations. Macromolecules 23, 4216 (1990)
15. C. CRESCENZI, A. DI CORCIA, R. SAMPRI, A. MARCOMINI, Determination of nonionic ethoxylate surfactants in environmental waters by liquid chromatography/electrospray mass spectrometry. Anal. Chem. 67, 1797 (1995)