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Volumn 129, Issue 37, 2007, Pages 11600-11607

trans-RhCI(CO)(PPh3)2-catalyzed monomeric and dimeric cycloisomerization of propargylic 2,3-dienoates. Establishment of α,β-unsaturated δ-lactone rings by cyclometallation

Author keywords

[No Author keywords available]

Indexed keywords

CARBON; CATALYSTS; CHEMICAL BONDS; HYDROGENATION; REACTION KINETICS; REDUCTION;

EID: 35048860971     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja073582u     Document Type: Article
Times cited : (46)

References (57)
  • 16
    • 35048890219 scopus 로고    scopus 로고
    • Crystal data for compound 2a: C 40H32O 4, MW, 576,66 orthorhombic, space group Pbca, final R indices [I > 2σ(I, R1, 0.0506, wR2, 0.1099, R indices (all data, R1, 0.0999, wR2, 0.1265, a, 24.367 (2) Å, b, 8.1958 (7) Å, c, 30.325 (3) Å, α, 90°, β, 90°, γ, 90°, V, 6056.2-(9) Å3, T, 293 (2) K, Z, 8, reflections collected/unique: 33 787/6614 (R(int, 0.1050, Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632768. Crystal data for compound epi-2a: C40H32O 4, MW, 576.66, monoclinic, space group P2(1)/c, final R indices [I > 2σ(I, R1, 0.0854, wR2, 0.1591, R indices (all data, R1, 0.2057, wR2, 0.2011, a, 11.4483 (13) A
    • 3, T = 293 (2) K, Z = 4, reflections collected/unique: 15 200/5383 (R(int) = 0.1430). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632770.
  • 18
    • 35048866014 scopus 로고    scopus 로고
    • Crystal data for compound 2d: C34H36O 4, MW, 508.63, triclinic, space group P1, final R indices [I > 2σ(I, R1, 0.0900, wR2, 0.2104, R indices (all data, R1, 0.2184, wR2, 0.2722, a, 8.6809 (14) Å, b, 15.504 (2) Å, c, 21.838 (3) Å, α, 93.347°, β, 92.725°, γ, 94.441°, V, 2921.4(8) Å3, T, 293 (2) K, Z, 4, reflections collected/unique: 15 521/10707 (R(int, 0.1336, Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647587. Crystal data for compound epi-2d: C 34H36O4, MW, 508.63, orthorhombic, space group Pca2(1, final R indices [I > 2σ(I, R1, 0.0765, wR2, 0.1711, R indices all data, R1, 0.1616, wR2, 0.2112, a, 28.9
    • 3, T = 293 (2) K, Z = 8, reflections collected/unique: 29 213/5646 (R(int) = 0.1745). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647588.
  • 19
    • 35048847163 scopus 로고    scopus 로고
    • Crystal data for compound 3f: C22H20O 2, MW, 316.38, orthorhombic, space group P2(1)2(1)2(1, final R indices [I > 2σ(I, R1, 0.0592, wR2, 0.1473, R indices (all data, R1, 0.0629, wR2, 0.1500, a, 6.0205 (7) Å, b, 16.6705 (18) Å, c, 17.5656 (19) Å, α, 90°, β, 90°, γ, 90°, V, 1763.0(3) Å3, T, 293 (2) K, Z, 4, reflections collected/unique: 10 498/2238 (Rint, 0.1078, Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632769
    • 3, T = 293 (2) K, Z = 4, reflections collected/unique: 10 498/2238 (R(int) = 0.1078). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632769.
  • 23
    • 77955911241 scopus 로고    scopus 로고
    • For Rh(I)-catalyzed cleaving C-O bond of allylic esters, see: Evans, P. A. Modern Rhodium-Catalyzed Organic Reactions; Wiley-VCH: 2005; pp 191-214.
    • For Rh(I)-catalyzed cleaving C-O bond of allylic esters, see: Evans, P. A. Modern Rhodium-Catalyzed Organic Reactions; Wiley-VCH: 2005; pp 191-214.
  • 24
    • 35048888156 scopus 로고    scopus 로고
    • For Pd(0)-catalyzed cleaving C-O bond of propargyl carbonates, see: Tsuji, J. Palladium Reagents and Catalysts; Wiley: Chichester, 2004; pp 543-563.
    • For Pd(0)-catalyzed cleaving C-O bond of propargyl carbonates, see: Tsuji, J. Palladium Reagents and Catalysts; Wiley: Chichester, 2004; pp 543-563.
  • 25
    • 35048842420 scopus 로고    scopus 로고
    • 3, T = 293 (2) K, Z = 4, reflections collected/unique: 10 456/3915 (R(int) = 0.1458). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647589.
    • 3, T = 293 (2) K, Z = 4, reflections collected/unique: 10 456/3915 (R(int) = 0.1458). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647589.
  • 33
    • 0004092363 scopus 로고    scopus 로고
    • Fringuelli, F, Taticchi, A, Eds, John Wiley & Sons
    • (a) Fringuelli, F., Taticchi, A., Eds. The Diels-Alder Reaction; John Wiley & Sons: 2003.
    • (2003) The Diels-Alder Reaction


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.