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0037176294
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(a) Brummond, K. M.; Chen, H.; Sill, P. C.; You, L. J. Am. Chem. Soc. 2002, 124, 15186.
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12
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0037125488
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0038175367
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16
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35048890219
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-
Crystal data for compound 2a: C 40H32O 4, MW, 576,66 orthorhombic, space group Pbca, final R indices [I > 2σ(I, R1, 0.0506, wR2, 0.1099, R indices (all data, R1, 0.0999, wR2, 0.1265, a, 24.367 (2) Å, b, 8.1958 (7) Å, c, 30.325 (3) Å, α, 90°, β, 90°, γ, 90°, V, 6056.2-(9) Å3, T, 293 (2) K, Z, 8, reflections collected/unique: 33 787/6614 (R(int, 0.1050, Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632768. Crystal data for compound epi-2a: C40H32O 4, MW, 576.66, monoclinic, space group P2(1)/c, final R indices [I > 2σ(I, R1, 0.0854, wR2, 0.1591, R indices (all data, R1, 0.2057, wR2, 0.2011, a, 11.4483 (13) A
-
3, T = 293 (2) K, Z = 4, reflections collected/unique: 15 200/5383 (R(int) = 0.1430). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632770.
-
-
-
-
18
-
-
35048866014
-
-
Crystal data for compound 2d: C34H36O 4, MW, 508.63, triclinic, space group P1, final R indices [I > 2σ(I, R1, 0.0900, wR2, 0.2104, R indices (all data, R1, 0.2184, wR2, 0.2722, a, 8.6809 (14) Å, b, 15.504 (2) Å, c, 21.838 (3) Å, α, 93.347°, β, 92.725°, γ, 94.441°, V, 2921.4(8) Å3, T, 293 (2) K, Z, 4, reflections collected/unique: 15 521/10707 (R(int, 0.1336, Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647587. Crystal data for compound epi-2d: C 34H36O4, MW, 508.63, orthorhombic, space group Pca2(1, final R indices [I > 2σ(I, R1, 0.0765, wR2, 0.1711, R indices all data, R1, 0.1616, wR2, 0.2112, a, 28.9
-
3, T = 293 (2) K, Z = 8, reflections collected/unique: 29 213/5646 (R(int) = 0.1745). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647588.
-
-
-
-
19
-
-
35048847163
-
-
Crystal data for compound 3f: C22H20O 2, MW, 316.38, orthorhombic, space group P2(1)2(1)2(1, final R indices [I > 2σ(I, R1, 0.0592, wR2, 0.1473, R indices (all data, R1, 0.0629, wR2, 0.1500, a, 6.0205 (7) Å, b, 16.6705 (18) Å, c, 17.5656 (19) Å, α, 90°, β, 90°, γ, 90°, V, 1763.0(3) Å3, T, 293 (2) K, Z, 4, reflections collected/unique: 10 498/2238 (Rint, 0.1078, Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632769
-
3, T = 293 (2) K, Z = 4, reflections collected/unique: 10 498/2238 (R(int) = 0.1078). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 632769.
-
-
-
-
23
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77955911241
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-
For Rh(I)-catalyzed cleaving C-O bond of allylic esters, see: Evans, P. A. Modern Rhodium-Catalyzed Organic Reactions; Wiley-VCH: 2005; pp 191-214.
-
For Rh(I)-catalyzed cleaving C-O bond of allylic esters, see: Evans, P. A. Modern Rhodium-Catalyzed Organic Reactions; Wiley-VCH: 2005; pp 191-214.
-
-
-
-
24
-
-
35048888156
-
-
For Pd(0)-catalyzed cleaving C-O bond of propargyl carbonates, see: Tsuji, J. Palladium Reagents and Catalysts; Wiley: Chichester, 2004; pp 543-563.
-
For Pd(0)-catalyzed cleaving C-O bond of propargyl carbonates, see: Tsuji, J. Palladium Reagents and Catalysts; Wiley: Chichester, 2004; pp 543-563.
-
-
-
-
25
-
-
35048842420
-
-
3, T = 293 (2) K, Z = 4, reflections collected/unique: 10 456/3915 (R(int) = 0.1458). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647589.
-
3, T = 293 (2) K, Z = 4, reflections collected/unique: 10 456/3915 (R(int) = 0.1458). Supplementary crystallographic data have been deposited at the Cambridge Crystallographic Data Center. CCDC: 647589.
-
-
-
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26
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0000551283
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