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Volumn 46, Issue 19, 2007, Pages 7710-7712

The highest D value for a MnII ion: Investigation of a manganese(II) polyoxometalate complex by high-field electron paramagnetic resonance

c CNRS (France)

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[No Author keywords available]

Indexed keywords

EID: 34948863835 PISSN: 00201669 EISSN: None Source Type: Journal
DOI: 10.1021/ic701193f Document Type: Article

Times cited : (35)

References (24)

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- Synthesis of 1: in a 10 mL beaker, 2.520 g (4.5 × 10 -4 mol) of Na14[As2W19O 67]·H2O, 0.147 g (4.5 · 10-4 mol) of Na2WO4· 2H2O, and 0.076 g (4.5 × 10-4 mol) of Mn(SO4) are dissolved in 5 mL of water at T, 70, 80°C. The pH of the mixture is adjusted to 2.2 with 1 M HCl, and the red solution is stirred for 15 min. After cooling to room temperature, 3 g (2.2 × 10-2 mol) of RbCl is added, and a few minutes later, the resulting orange precipitate is filtered and washed with 1 M KCl and dried with ethanol and ether. Yield: 2.1 g (85, A total of 0.7 g of the powder are then recrystallized in 5 mL of water with gentle heating. After 1 night, 0.210 g of orange parallelepipedic crystals of 1 suitable for X-ray diffraction are obtained. IR νmax/cm-1, 963s, 913sh
- -1). Anal. Calcd (found) for 1: W, 58.34 (58.10); Mn, 0.87 (0.85); As, 2.38 (2.61); Rb, 10.85 (10.11).

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