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Volumn , Issue 15, 2007, Pages 2442-2444

Novel and efficient synthesis of 1-iodoalkynes

Author keywords

(Diacetoxyiodo)benzene; 1 iodoalkynes; Copper(I) iodide; Potassium iodide

Indexed keywords

(DIACETOXYIODO)BENZENE; 1 IODOALKYNE; ALKYNE DERIVATIVE; BENZENE DERIVATIVE; COPPER IODIDE; IODINE DERIVATIVE; POTASSIUM IODIDE; UNCLASSIFIED DRUG;

ARTICLE; CHEMICAL REACTION; DIMERIZATION; DRUG SYNTHESIS;

EID: 34948815023 PISSN: 09365214 EISSN: None Source Type: Journal
DOI: 10.1055/s-2007-985608 Document Type: Article

Times cited : (47)

References (26)

1
- 33845374372
- (a) Boutin, R. H.; Rapoport, H. J. Org. Chem. 1986, 51, 5320.
- (1986) J. Org. Chem , vol.51 , pp. 5320
- Boutin, R.H.¹ Rapoport, H.²

2
- 0004942615
- (b) Bjorkling, F.; Norin, T.; Unelius, R. Synth. Commun. 1985, 15, 463.
- (1985) Synth. Commun , vol.15 , pp. 463
- Bjorkling, F.¹ Norin, T.² Unelius, R.³

3
- 84985580906
- (c) Hofmeister, H.; Annen, K.; Laurent, H.; Wiechert, R. Angew. Chem., Int. Ed. Engl. 1984, 23, 727.
- (1984) Angew. Chem., Int. Ed. Engl , vol.23 , pp. 727
- Hofmeister, H.¹ Annen, K.² Laurent, H.³ Wiechert, R.⁴

4
- 0001545629
- (d) Roush, W. R.; Peseckis, S. M.; Walts, A. E. J. Org. Chem. 1984, 49, 3429.
- (1984) J. Org. Chem , vol.49 , pp. 3429
- Roush, W.R.¹ Peseckis, S.M.² Walts, A.E.³

5
- 37049074616
- and references cited therein
- (a) Jeffery, T. J. Chem. Soc., Chem. Commun. 1988, 909; and references cited therein,
- (1988) J. Chem. Soc., Chem. Commun , pp. 909
- Jeffery, T.¹

6
- 0034025417
- (b) Kabalka, G. W.; Shoup, T. M.; Goodman, M. M. Nucl. Med. Biol. 2000, 27, 279.
- (2000) Nucl. Med. Biol , vol.27 , pp. 279
- Kabalka, G.W.¹ Shoup, T.M.² Goodman, M.M.³

7
- 0000959738
- (a) Cohen, M. J.; McNelis, E. J. Org. Chem. 1984, 49, 515.
- (1984) J. Org. Chem , vol.49 , pp. 515
- Cohen, M.J.¹ McNelis, E.²

8
- 0013491256
- (b) Ricci, A.; Taddei, M.; Dembech, P.; Guerrini, A.; Seconi, G. Synthesis 1989, 461.
- (1989) Synthesis , pp. 461
- Ricci, A.¹ Taddei, M.² Dembech, P.³ Guerrini, A.⁴ Seconi, G.⁵

9
- 0029006004
- (c) Rao, M. L. N.; Periasamy, M. Synth. Commun. 1995, 25, 2295.
- (1995) Synth. Commun , vol.25 , pp. 2295
- Rao, M.L.N.¹ Periasamy, M.²

10
- 0002813615
- (d) Barluenga, J.; Gonzalez, J. M.; Rodriguez, M. A.; Campos, P. G.; Asensio, G. Synthesis 1987, 661.
- (1987) Synthesis , pp. 661
- Barluenga, J.¹ Gonzalez, J.M.² Rodriguez, M.A.³ Campos, P.G.⁴ Asensio, G.⁵

11
- 1642538440
- (e) Kabalka, G. W.; Mereddy, A. R. Tetrahedron Lett. 2004, 45, 1417.
- (2004) Tetrahedron Lett , vol.45 , pp. 1417
- Kabalka, G.W.¹ Mereddy, A.R.²

12
- 0001633473
- (a) Nishikawa, T.; Shibaya, S.; Hosokowa, S.; Isobe, M. Synlett 1994, 485.
- (1994) Synlett , pp. 485
- Nishikawa, T.¹ Shibaya, S.² Hosokowa, S.³ Isobe, M.⁴

13
- 0025797346
- (b) Casarini, A.; Dembech, P.; Reginato, G.; Ricci, A. Tetrahedron Lett. 1991, 32, 2169.
- (1991) Tetrahedron Lett , vol.32 , pp. 2169
- Casarini, A.¹ Dembech, P.² Reginato, G.³ Ricci, A.⁴

14
- 33751157394
- (c) Simonot, B.; Rousseau, G. J. Org. Chem. 1994, 59, 5912.
- (1994) J. Org. Chem , vol.59 , pp. 5912
- Simonot, B.¹ Rousseau, G.²

15
- 0028922406
- (d) Brunei, Y.; Rousseau, G. Tetrahedron Lett. 1995, 36, 2619.
- (1995) Tetrahedron Lett , vol.36 , pp. 2619
- Brunei, Y.¹ Rousseau, G.²

16
- 0032886495
- (e) Nasker, D.; Roy, S. J. Org. Chem. 1999, 64, 6896.
- (1999) J. Org. Chem , vol.64 , pp. 6896
- Nasker, D.¹ Roy, S.²

17
- 0032913695
- (f) Abe, H.; Suzuki, H. Bull. Chem. Soc. Jpn. 1999, 72, 787.
- (1999) Bull. Chem. Soc. Jpn , vol.72 , pp. 787
- Abe, H.¹ Suzuki, H.²

18
- 34548172446
- Ochiai, M.; Uemura, K.; Masaki, Y. J. Am. Chem. Soc. 1993, 115, 2528.
- (1993) J. Am. Chem. Soc , vol.115 , pp. 2528
- Ochiai, M.¹ Uemura, K.² Masaki, Y.³

19
- 34447284254
- Yan, J.; Wu, J. L.; Yang, Z. P. J. Organomet. Chem. 2007, 692, 3636.
- (2007) J. Organomet. Chem , vol.692 , pp. 3636
- Yan, J.¹ Wu, J.L.² Yang, Z.P.³

20
- 34948889063
- General Procedure for the Iodination of Terminal Alkynes To MeCN (3 mL, alkyne 1 (0.5 mmol, DIB (0.5 mmol, Et3N (1.0 mmol, KI (1.0 mmol, and CuI (5.0 mol, were added. The mixture was stirred at r.t. for 0.3-0.5 h and then separated on a silica gel plate using PE as eluent, 1-iodoalkyne 2 was afforded in good to excellent yield. Compound 2a: Oil. 1H NMR (400 MHz, CDCl3, δ, 7.44-7.42 (m, 2 H, 7.32-7.29 (m, 3 H, 13C NMR (100 MHz, CDCl 3, δ, 132.3, 128.8, 128.2, 1234, 94.1, 6.1. IR (film, ν, 2175, 755, 690 cm-1. MS (EI, m/z, 228 (100, M, Compound 2b: Oil. 1H NMR (400 MHz, CDCl 3, δ, 7.32 (d, J, 8.4 Hz, 2 H, 7.11 (d, J, 8.0 Hz, 2 H, 2.35 (s, 3 H, 13C NMR (100 MHz, CDCl3, δ, 139.0, 132.2, 129.0, 120.3, 94.2, 21.5, 4.9. IR film, ν, 2170, 818 cm-1
- +].

21
- 37049073594
- (a) Kita, Y.; Okunaka, R.; Kondo, M.; Tohma, H.; Inagaki, M.; Hatanaka, K. J. Chem. Soc., Chem. Commun. 1992, 429.
- (1992) J. Chem. Soc., Chem. Commun , pp. 429
- Kita, Y.¹ Okunaka, R.² Kondo, M.³ Tohma, H.⁴ Inagaki, M.⁵ Hatanaka, K.⁶

22
- 34447253597
- (b) Yan, Y.; Zhong, L. R.; Chen, Z. C. J. Org. Chem. 1991, 56, 461.
- (1991) J. Org. Chem , vol.56 , pp. 461
- Yan, Y.¹ Zhong, L.R.² Chen, Z.C.³

23
- 0025914440
- Ochiai, M.; Uemura, K.; Oshima, K.; Masaki, Y.; Kunishima, M.; Tani, S. Tetrahedron Lett. 1991, 32, 4753.
- (1991) Tetrahedron Lett , vol.32 , pp. 4753
- Ochiai, M.¹ Uemura, K.² Oshima, K.³ Masaki, Y.⁴ Kunishima, M.⁵ Tani, S.⁶

24
- 0000807858
- (a) Stang, P. J.; Surber, B. W. J. Am. Chem. Soc. 1985, 107, 1452.
- (1985) J. Am. Chem. Soc , vol.107 , pp. 1452
- Stang, P.J.¹ Surber, B.W.²

25
- 0001600484
- (b) Stang, P. J.; Kitamura, T.; Boehshar, M.; Wingert, H. J. Am. Chem. Soc. 1989, 111, 2225.
- (1989) J. Am. Chem. Soc , vol.111 , pp. 2225
- Stang, P.J.¹ Kitamura, T.² Boehshar, M.³ Wingert, H.⁴

26
- 0000492218
- (c) Stang, P. J.; Boehshar, M.; Lin, J. J. Am. Chem. Soc. 1986, 108, 7832.
- (1986) J. Am. Chem. Soc , vol.108 , pp. 7832
- Stang, P.J.¹ Boehshar, M.² Lin, J.³

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