Development and validation of gas chromatography-mass spectroscopy method for determination of prilocaine HCl in human plasma using internal standard methodology

Biomedical Chromatography

Volumn 21, Issue 10, 2007, Pages 1077-1082

  Kadioglu, Yucel ^a   Atila, Alptug ^a  

^a ATATÜRK UNIVERSITY   (Turkey)

Author keywords

GC MS; Method validation; Prilocaine HCl

Indexed keywords

GAS CHROMATOGRAPHY; MASS SPECTROMETRY; SPECTROSCOPIC ANALYSIS;

GAS CHROMATOGRAPHY-MASS SPECTROSCOPIES; GC-MS; HUMAN PLASMAS; INTERNAL STANDARDS; METHEMOGLOBINEMIA; METHOD VALIDATIONS; O-TOLUIDINE; PRILOCAINE; PRILOCAINE HCL; VALIDATION PARAMETERS;

CHLORINE COMPOUNDS;

LIDOCAINE; PRILOCAINE;

ACCURACY; ANALYTIC METHOD; ARTICLE; CONTROLLED STUDY; DRUG BLOOD LEVEL; DRUG DETERMINATION; DRUG STRUCTURE; GAS CHROMATOGRAPHY; HUMAN; MASS SPECTROMETRY; QUANTITATIVE ANALYSIS; SENSITIVITY AND SPECIFICITY; VALIDATION PROCESS;

EID: 34848826540     PISSN: 02693879     EISSN: 10990801     Source Type: Journal    
DOI: 10.1002/bmc.857     Document Type: Article

References (24)

1. Adams HA, Biscoping J, Ludof K, Borgmann A, Beckman-MB and Hempelmann G. The quantitative analysis of amide local anesthetics using high pressure liquid chromatography and ultraviolet detection (HPLC/UV). Regional Anaesthesia 1989;, 12: 53-57.
2. Ariens EJ. Chiral Separation in HPLC, Applications to Pharmaceutical Compounds, Krstulovic AM (ed.). Ellis Horwood: Chichester, 1989; 31.
3. Asada A. Gas chromatographic determination of local anesthetics in blood. Osaka City Medical Journal 1979; 25: 91-122.
4. Bjork M, Petterson KJ and Osterlof G. Capillary gas chromatographic method for simultaneous determination of local anesthetics in plasma samples. Journal of Chromatography 1990, 533: 229-234.
5. Cameron JD. The gas chromatographic determination of plasma concentrations of some local anesthetics using a nitrogen detector. Clinical Chemica Acta 1974; 56: 307-309.
6. Cawson RA and Curson DR. The hazards of dental local anesthetics in children. British Dental Journal 1983; 154: 253-256.
7. Jastak JY, Yagela JA and Donaldson D. Local anesthesia in the oral cavity. In: Pharmacology of Local Anesthesia and Clinical Preparations and Drug Selection. W.B. Saunders: Philadelphia, PA, 1995; 23-26.
8. Keenaghan JB. The determination of lidocaine and prilocaine in whole blood by gas chromatography. Journal of Pharmacy Science 1967; 56: 1645-1646.
9. Klein J, Fernandes D, Gazarian M, Kent G and Koren G. Simultaneous determination of lidocaine, prilocaine and the prilocaine metabolite o-toluidine in plasma by high performance liquid chromatography. Journal of Chromatography B 1994; 655: 83-88.
10. Klimundova J, Satinsky D, Sklenarova H and Solich P. Automation of simultaneous release tests of two substances by sequential injection chromatography with Franz cell. Talanta 2006; 69: 730-735.
11. Koehler A, Oertel R and Kirch W. Simultaneous determination of bupivacaine, mepivacain, prilocaine and ropivacain in human serum by liquid chromatography-tandem mass spectrometry. Journal of Chromatography A 2005; 1088: 126-130.
12. Prat M and Bruguerolle B. Rapid simultaneous gas-liquid chromatographic determination of five local anesthetic drugs in serum. Clinical Chemistry 1986; 32: 2098-2100.
13. Rishiraj B, Epstein JB, Fine D, Nabi S and Wade NK. Permanent vision loss in one eye following administration of local anesthesia for a dental extraction. International Journal of Oral & Maxillofacial Surgery 2005; 34: 220-223.
14. Rudolf B, Durstewitz-Knierim D, Ridderskamp I, Scharenberg C and Brandt L. Increase of prilocaine-induced methemoglobinemia following anesthesia. Anaesthetist 1995; 44: 445-449.
15. Siluveru M and Stewart JT. Stereoselective determination of R-(-)- and S-(+)-prilocaine in human serum using a brush-type chiral stationary phase, solid-phase extraction and UV detection. Journal of Pharmaceutical and Biomedical Analysis 1996; 15: 389-392.
16. Siluvera M and Stewart JT. Stereoselective determination of R-(-)- and S-(+)-prilocaine in human serum by capillary electrophoresis using a derivatized cyclodextrin and ultraviolet detection. Journal of Chromatography B 1997; 693: 205-210.
17. Storms LM and Stewart JT. Stability-indicating HPLC assay for determination of prilocaine and procaine drug combinations. Journal of Pharmaceutical and Biomedical Analysis 2002; 30: 49-58.
18. Taddio A, Stevens B, Craig K, Rastogi P, Ben-David S and Shennan A. Efficacy and safety of lidocaine-prilocaine cream for pain during circumcision. New England Journal of Medicine 1997; 336: 1197-201.
19. Tucker GT, Mather LE, Lennard MS and Gregory A. Plasma concentrations of the stereoisomers of prilocaine after administration of racemate: implications for toxicity? British Journal of Anaesthesia 1990; 65: 333-336.
20. Warren RE, Van de Mark TB and Weinberg S. Methemoglobinemia induced by high doses of prilocaine. Oral Surgery Oral Medicine Oral Pathology 1974; 37: 866-871.
21. Watanabe T, Namera A, Yashiki M, Iwasaki Y and Kojima T. Simple analysis of local anesthetics in human blood using headspace solid-phase microextraction and gas chromatography-mass spectrometry-electron impact ionization selected ion monitoring. Journal of Chromatography B 1998; 709: 225-232.
22. Wieberg K and Jacobbsson SP. Paralel factor analysis of HPLC-DAD data for binary mixtures of lidocaine and prilocaine with different levels of chromatographic separation. Analytica Chimica Acta 2004; 514: 203-209.
23. Wieberg K, Andersson M, Hagman A and Jacobsson SP. Peak purity determination with principal component analysis of high-performance, liquid chromatography-diode array detection data. Journal of Chromatography A 2004; 1029: 13-20.
24. ICH. Validation of analytical procedures. In Proceedings of the International Conference on Harmonization. Commission of the European Communities: Brussels, 1996.