Synthesis and X-ray crystal structure of [(C5Ph 5)CrCl(μ-Cl)2Tl]2: An example of the rare M-X-Tli linkage (X = halide)

Organometallics

Volumn 26, Issue 19, 2007, Pages 4843-4845

  Davis, K Brian ^a   Harris, T David ^a   Castellani, Michael P ^a   Golen, James A ^b   Rheingold, Arnold L ^b  

^a MARSHALL UNIVERSITY   (United States)

^b UNIVERSITY OF CALIFORNIA   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

COMPLEXATION; SOLVENTS; SYNTHESIS (CHEMICAL);

DIMERIC COMPLEX; STERIC BASIS;

DIMERS;

EID: 34748843999     PISSN: 02767333     EISSN: None     Source Type: Journal    
DOI: 10.1021/om070231f     Document Type: Article

References (25)

1. (a) Bruce, M. R. M.; Tyler, D. R. Organometallics 1985, 4, 528-533.
2. (b) Filippou, A. C.; Grünleiter, W. J. Organomet. Chem. 1989, 378, 387-399.
3. (c) Antiñolo, A.; Carrillo, F.; Chaudret, B.; Fajardo, M.; García-Yuste, S.; Lahoz, F. J.; Lanfranchi, M.; López, J. A.; Otero, A.; Pellinghelli, M. A. Organometallics 1995, 14, 1297-1301.
4. (d) Kuang, S.-M.; Fanwick, P. E.; Walton, R. A. Inorg. Chem. 2002, 41, 147-151.
5. 2]: Schmidbaur, H.; Bublak, W.; Riede, J.; Müller, G. Angew. Chem., Int. Ed. Engl. 1985, 24, 414-415) and
6. 4: Schüpp, B.; Keller, H.-L. Z. Anorg. Allg. Chem. 1999, 625, 379-381).
7. Ezomo, O. J.; Mingos, D. M. P.; Williams, I. D. J. Chem. Soc., Chem. Commun. 1987, 924-925.
8. Blake, A. J.; Christie, R. M.; Roberts, Y. V.; Sullivan, M. J.; Schröder, M.; Yellowlees, L. J. J. Chem. Soc., Chem. Commun. 1992, 848-849.
9. Bianchini, C.; Masi, D.; Linn, K.; Mealli, C.; Peruzzini, M.; Zanobini, F. Inorg. Chem. 1992, 31, 4036-4037.
10. Kahwa, I. A.; Miller, D.; Mitchel, M.; Fronczek, F. R.; Goodrich, R. G.; Williams, D. J.; O'Mahoney, C. A.; Slawin, A. M.; Ley, S. V.; Groombridge, C. J. Inorg. Chem. 1992, 31, 3963-3970.
11. Barthazy, P.; Togni, A.; Mezzetti, A. Organometallics 2002, 21, 3472.
12. Becker, C.; Kieltsch, I.; Broggini, D.; Mezzetti, A. Inorg. Chem. 2003, 42, 8417-8429.
13. Kunrath, F. A.; Casagrande, O. L., Jr.; Toupet, L.; Carpentier, J.-F. Eur. J. Inorg. Chem. 2004, 4803-4806.
14. Drouin, S. D.; Foucault, H. M.; Yap, G. P. A.; Fogg, D. E. Organometallics 2004, 23, 2583-2590.
15. Szymczak, N. K.; Han, F.; Tyler, D. R. Dalton Trans. 2004, 3941-3942.
16. Devic, T.; Batail, P.; Fourmigué, M.; Avarvari, N. Inorg. Chem. 2004, 43, 3136-3141.
17. Price, W.D.; Castellani, M. P. Unpublished results.
18. 3. Wei, P.; Stephan, D. W. Organometallics 2003, 22, 1712-1717.
19. Köhler, F. H.; de Cao, R.; Ackermann, K.; Sedlmair, J. Z. Naturforsch. 1993, 38b, 1406-1411.
20. Richeson, D. S.; Mitchell, J. F.; Theopold, K. H. Organometallics 1989, 8, 2570-2577.
21. Hutton, M. A.; Durham, J. C.; Grady, R. W.; Harris, B. E.; Jarrell, C. S.; Mooney, J. M.; Castellani, M. P.; Rheingold, A. L.; Kölle, U.; Korte, B. J.; Sommer, R. D.; Yee, G. T. Yee; Boggess, J. M.; Czernuszewicz, R. S. Organometallics 2001, 20, 734-740.
22. 2 and the starting chromium dimer, then the material recovered for R = H would contain less than 4% of the thallium complex, while R = Me would contain less than 1.5% thallium complex.
23. Hoobler, R. J.; Hutton, M. A.; Dillard, M. M.; Castellani, M. P.; Rheingold, A. L.; Rieger, A. L.; Rieger, P. H.; Richards, T. C.; Geiger, W. E. Organometallics 1993, 12, 116-123.
24. Köhler, F. H.; de Cao, R.; Ackermann, K.; Sedlmair, J. Z. Naturforsch. 1983, 38B, 1406-1411.
25. Köhler, F. H.; Lachmann, J.; Müller, G.; Zeh, H.; Brunner, H.; Pfauntsch, J.; Wachter, J. J. Organomet. Chem. 1989, 365, C15-C18.