Application of unsymmetrical indirect covariance NMR methods to the computation of the13C↔15N HSQC-IMPEACH and 13C↔15N HMBC-IMPEACH correlation spectra

Magnetic Resonance in Chemistry

Volumn 45, Issue 10, 2007, Pages 883-888

  Martin, Gary E ^a   Hilton, Bruce D ^a   Irish, Patrick A ^a   Blinov, Kirill A ^b   Williams, Antony J ^c  

^a MERCK RESEARCH LABORATORIES   (United States)

^b Moscow Division   (Russian Federation)

^c Advanced Chemistry Development Inc   (Canada)

Author keywords

13C 15N heteronuclear correlation; 1H 13C GHMBC; 1H 13C GHSQC; 1H 15NIMPEACH MBC; Unsymmetrical indirect covariance

Indexed keywords

CARBON; CHEMICAL SHIFT; STEEL BEAMS AND GIRDERS;

13C-15N HETERONUCLEAR CORRELATION; 1H- 13C GHMBC; 1H-13C GHSQC; 1H-15NIMPEACH-MBC; CORRELATION SPECTRA; HETERONUCLEAR; HETERONUCLEAR CORRELATION; PROCESSING METHOD; SPECTRA'S; UNSYMMETRICAL INDIRECT COVARIANCE;

NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY;

EID: 34748840152     PISSN: 07491581     EISSN: 1097458X     Source Type: Journal    
DOI: 10.1002/mrc.2064     Document Type: Article

References (29)

1. Martin GE, Crouch RC, Andrews CW. J. Heterocycl. Chem. 1995; 32: 1665.
2. Koshino H, Uzawa J. Kagaku to Seibutsu 1995; 33: 252.
3. Martin GE, Hadden CE. J. Nat. Prod. 2000; 65: 543.
4. Marek R, Lyčka A. Curr. Org. Chem. 2002; 6: 35.
5. 15N 2D NMR methods. In Annual Reports on NMR Spectroscopy, vol. 55, Webb GA (ed). Elsevier: Amsterdam, 2005; 1.
6. Forgo P, Homann J, Dombi G, Máthé L. Advanced multidimensional NMR experiments as tools for structure determination of Amaryllidaceae alkaloids. In Poisonous Plants and Related Toxins, Acamovic T, Steward S, Pennycott TW (eds). Wallingford, 2004; 322.
7. 15N NMR in alkaloid chemistry. In Modern Alkaloids, Fattorusso E, Taglialatela-Scafati O (eds). Wiley-VCH: 2007 (in press).
8. Pérez-Trujillo M, Nolis P, Parella T. Org. Lett. 2007; 9: 29.
9. Kupče E, Freeman R. Magn. Reson. Chem. 2007; 45: 103.
10. Bruschweiler R, Zhang F. J. Chem. Phys. 2004; 120: 5253.
11. Zhang F, Bruschweiler R. J. Am. Chem. Soc. 2004; 126: 13180.
12. Blinov KA, Larin NI, Kvasha MP, Moser A, Williams AJ, Martin GE. Magn. Reson. Chem. 2005; 43: 999.
13. Blinov KA, Larin NI, Williams AJ, Zell M, Martin GE. Magn. Reson. Chem. 2006; 44: 107.
14. Blinov KA, Larin NI, Williams AJ, Mills KA, Martin GE. J. Heterocycl. Chem. 2006; 43: 163.
15. Martin GE, Blinov KA, Williams AJ. J. Nat. Prod. 2007 (in press).
16. Blinov KA, Williams AJ, Hilton BD, Irish PA, Martin GE. Magn. Reson. Chem. 2007; 45: 544.
17. Martin GE, Irish PA, Hilton BD, Blinov KA, Williams AJ. Magn. Reson. Chem. 2007; 45: 624.
18. Martin GE, Hilton BD, Irish PA, Blinov KA, Williams AJ. J. Heterocycl. Chem. 2007; 44: in press.
19. Martin GE. J. Heterocycl. Chem. 1997; 34: 695.
20. Hadden CE, Martin GE, Krishnamurthy W. Magn. Reson. Chem. 2000; 38: 143.
21. Kupče E. Methods Enzymol. 2001; 338: 82.
22. Boyer RD, Johnson R, Krishnamurthy K. J. Magn. Reson. 2003; 165: 253.
23. Bax A, Freeman R, Kempsell SP. J. Am. Chem. Soc. 1980; 102: 4849.
24. Köck M, Kerssebaum R, Bermel W. Magn. Reson. Chem. 2003; 41: 65.
25. Cavanaugh J, Fairbrother WJ, Palmer AG III, Skelton NJ, Ranee M. Protein NMR Spectroscopy: Principles and Practice (2nd edn). Academic Press: New York City, 2006.
26. Martin GE, Hadden CE. Magn. Reson. Chem. 2000; 38: 251.
27. Kupče E, Freeman R. J. Am. Chem. Soc. 2004; 126: 6429.
28. Kupče E, Freeman R. J. Am. Chem. Soc 2006; 128: 6020.
29. Kline M, Cheatham S. Magn. Reson. Chem. 2003; 41: 307.